Radio frequency heating for rapid curing of nanocomposite adhesives

Patent metadata

Field	Value
Publication number	US-12312507-B2
Application number	US-201816765424-A
Country	US
Kind code	B2
Filing date	Nov 21, 2018
Priority date	Nov 21, 2017
Publication date	May 27, 2025
Grant date	May 27, 2025

Abstract

A non-contact method of joining two components via direct heating of a thermoset adhesive includes applying the thermoset adhesive to at least a first component of the two components. The thermoset adhesive includes a susceptor to reacts in the presence of an electromagnetic field. The method includes placing the first component and a second component of the two components in proximity to an electromagnetic field. In some aspects, the method includes placing the first and second components in proximity to an electromagnetic field of a capacitor. The susceptor interacts with the electromagnetic field to heat the thermoset adhesive via resistive heating. In some aspects, a method of direct-contact heating of the thermoset adhesive includes attaching electrodes to a film comprising the adhesive. The components being joined together are not directly heated by the electromagnetic field, and as a result experience much lower temperatures than the thermoset adhesive.

First claim

What is claimed is:

1. A method of joining two components via direct heating of a thermoset adhesive, the method comprising:
applying the thermoset adhesive to at least a first component of the two components, the thermoset adhesive comprising a susceptor;
painting a first electrode on one end of the thermoset adhesive;
painting a second electrode on the opposite end of the thermoset adhesive from the first electrode;
contacting the first component with the first electrode;
contacting a second component of the two components with the second electrode;
contacting the second component with the thermoset adhesive;
creating an electromagnetic field by applying an RF signal across the first and second electrodes; and
wherein the susceptor interacts with the electromagnetic field to heat the thermoset adhesive via resistive heating.

2. The method of claim 1 , wherein the two components are not directly heated by the electromagnetic field.

3. The method of claim 1 , wherein the thermoset adhesive further comprises an epoxy.

4. The method of claim 3 , wherein the thermoset adhesive further comprises a urethane.

5. The method of claim 1 , wherein the susceptor comprises carbon nanotubes.

6. The method of claim 5 , wherein the carbon nanotubes comprise approximately 0.1 to 0.5 wt % of the thermoset adhesive.

7. The method of claim 5 , wherein the carbon nanotubes comprise approximately 1.0 to 10.0 wt % of the thermoset adhesive.

8. The method of claim 1 , wherein the susceptor comprises a graphene nanosheet.

9. The method of claim 1 , wherein the susceptor comprises carbon black particles.

10. The method of claim 1 , wherein the susceptor comprises inorganic nanomaterials.

11. The method of claim 1 , wherein the first electrode is connected to an output of an RF amplifier and the second electrode is grounded.

12. The method of claim 11 , wherein the applying the electromagnetic field comprises outputting, by the RF amplifier, an RF signal between approximately 3 kHz to approximately 300 MHz.

13. A structure manufactured by the process of claim 1 , the structure comprising the first component, the second component, and the thermoset adhesive.

Assignees

• Texas A & M Univ Sys

Inventors

• Sweeney Charles Brandon
• Green Micah J

Classifications

• B29K2105/002

  Agents changing electric characteristics · CPC title

• B29K2105/162

  Nanoparticles · CPC title

• B29K2105/0088

  Blends of polymers · CPC title

• B29K2301/10

  Thermosetting resins · CPC title

• B29K2509/00

  Use of inorganic materials not provided for in groups {B29K2503/00 - B29K2507/00,} as filler · CPC title