Complex modality reactor for materials production and synthesis

Patent metadata

Field	Value
Publication number	US-12296312-B2
Application number	US-202318173322-A
Country	US
Kind code	B2
Filing date	Feb 23, 2023
Priority date	Jan 23, 2020
Publication date	May 13, 2025
Grant date	May 13, 2025

Abstract

A system for producing carbonaceous materials is disclosed that includes an energy source configured to emit microwave energy and a plasma reactor coupled to receive the microwave energy and configured to produce plasma in response to exposure of one or more process gases to the microwave energy. In some instances, the plasma reactor includes a first chamber having a rectangular cross-section and configured to receive the microwave energy from the energy source as sinusoidal waveform, a second chamber having a cylindrical cross-section and configured to receive microwave energy from the first chamber as a radial waveform having an energy maxima at a radial center of the cylindrical cross-section, the second chamber including an opening to receive one or more process gases and configured to ignite a plasma plume, and a gas-solid separator configured to separate solid materials from the plasma plume.

First claim

What is claimed is:

1. A plasma reactor comprising:
a first chamber having a rectangular cross-section and configured to receive microwave energy as a sinusoidal waveform;
a rectangular-to-cylindrical portion coupled to the first chamber and configured to convert the microwave energy from the sinusoidal waveform to a radial waveform;
a second chamber having a cylindrical cross-section coupled to the rectangular-to-cylindrical portion, the second chamber configured to produce a plasma plume in response to exposure of one or more process gases to the radial waveform of the microwave energy; and
a multi-flow nozzle including a first inlet and a second inlet arranged in a concentric configuration.

2. The plasma reactor of claim 1 , wherein the microwave energy has an energy maxima at a radial center of the second chamber.

3. The plasma reactor of claim 1 , wherein the second chamber is configured to contain the plasma plume.

4. The plasma reactor of claim 1 , further comprising a gas-solid separator to separate carbonaceous materials from the plasma plume.

5. The plasma reactor of claim 1 , further comprising a pressure controller configured to regulate the flow of the process gases into the plasma reactor.

6. The plasma reactor of claim 1 , wherein a location of ignition of the plasma plume within the plasma reactor is based at least in part on the microwave energy.

7. The plasma reactor of claim 1 , further comprising a reactor control unit configured to control an ignition point of the plasma plume.

8. The plasma reactor of claim 1 , wherein a center portion of the first chamber is aligned with a center portion of the second chamber along a common vertical axis.

9. The plasma reactor of claim 1 , wherein the first chamber is narrower than the second chamber.

10. The plasma reactor of claim 1 , wherein the multi-flow nozzle allows the one or more process gases to enter the second chamber.

11. The plasma reactor of claim 1 , wherein the first and second inlets flow first and second respective process gases into the second chamber.

12. The plasma reactor of claim 1 , wherein the multi-flow nozzle is configured to direct the one or more process gases into the second chamber at one or more respective flow rates.

13. The plasma reactor of claim 1 , wherein the multi-flow nozzle is configured to flow the one or more process gases into the second chamber in an adjacent configuration.

14. The plasma reactor of claim 1 , wherein the multi-flow nozzle is formed from a material permitting unimpeded transmission of the microwave energy.

15. The plasma reactor of claim 1 , wherein the multi-flow nozzle comprises a mechanical pressure barrier preventing the plasma plume from entering the first chamber.

16. The plasma reactor of claim 1 , wherein at least one of the one or more process gases includes a hydrocarbon gas.

17. The plasma reactor of claim 1 , wherein the first chamber and the rectangular-to-cylindrical portion are arranged in a linear manner relative to each other.

18. A plasma reactor comprising:
a first chamber having a rectangular cross-section and configured to receive microwave energy as a sinusoidal waveform;
a rectangular-to-cylindrical portion coupled to the first chamber and configured to convert the microwave energy from the sinusoidal waveform to a radial waveform;
a second chamber having a cylindrical cross-section coupled to the rectangular-to-cylindrical portion, the second chamber configured to produce a plasma plume in response to exposure of one or more process gases to the radial waveform of the microwave energy; and
a multi-flow nozzle that allows the one or more process gases to enter the second chamber, wherein the multi-flow nozzle is configured to flow the one or more process gases into the second chamber in a concentric configuration.

19. The plasma reactor of claim 18 , wherein the multi-flow nozzle is configured to direct the one or more process gases into the second chamber at one or more respective flow rates.

20. The plasma reactor of claim 18 , wherein the multi-flow nozzle is configured to flow the one or more process gases into the second chamber in an adjacent configuration.

Assignees

• Lyten Inc

Inventors

• Stowell Michael W
• Lanning Bruce
• Rogojina Elena

Classifications

• B01J37/346

  of microwave energy · CPC title

• B01J2219/0869

  Feeding or evacuating the reactor · CPC title

• B01D2259/806

  Microwaves · CPC title

• B01J2219/0894

  Processes carried out in the presence of a plasma · CPC title

• B01J2219/1218

  Multiple reactors · CPC title