Water sampling immersion probe

Patent metadata

Field	Value
Publication number	US-12287316-B2
Application number	US-201917632061-A
Country	US
Kind code	B2
Filing date	Aug 1, 2019
Priority date	Aug 1, 2019
Publication date	Apr 29, 2025
Grant date	Apr 29, 2025

Abstract

The present invention relates to a water sampling immersion probe ( 50 ) for continuously filtering a water sample from wastewater ( 14 ). The water sampling immersion probe ( 50 ) includes a distal coarse filter ( 60 ) with a porosity of 0.1 to 1.0 mm, a proximal fine filter ( 70 ) arranged downstream of the coarse filter ( 60 ) and having a porosity of less than 5.0 μm, and a sample suction opening ( 74 ) arranged downstream of the fine filter ( 70 ). The coarse filter ( 60 ) is arranged to not contact the fine filter ( 70 ).

First claim

The invention claimed is:

1. A water sampling immersion probe for continuously filtering a water sample from wastewater, the water sampling immersion probe comprising:
a distal coarse filter comprising a porosity of 0.1 to 1.0 mm;
a proximal fine filter arranged downstream of the distal coarse filter, the proximal fine filter comprising a porosity of less than 50 μm, the distal coarse filter and the proximal fine filter being arranged so as to not contact each other, wherein the distal coarse filter and the proximal fine filter define a venting chamber, wherein the venting chamber is vented at a bottom and the venting chamber is inclined with respect to vertical with an inclination angle between 5° and 80° degrees and completely submerged so that rising air bubbles remain in contact with a distal side of a membrane of the proximal fine filter over the entire height of the membrane; and
a sample suction opening arranged downstream of the proximal fine filter.

2. The water sampling immersion probe of claim 1 , wherein the venting chamber comprises at least one venting opening through which venting air can be blown into the venting chamber.

3. The water sampling immersion probe of claim 2 , wherein,
the water sampling immersion probe is generally cylindrical and comprises a cylinder axis, and
the cylinder axis of the immersion probe is inclined with respect to a horizontal (H) at an inclination angle (A′) of 10° to 80°.

4. The water sampling immersion probe of claim 1 , wherein the proximal fine filter is defined by a fine filter membrane which is air-impermeable comprising a porosity of less than 5.0 μm.

5. The water sampling immersion probe of claim 1 , wherein the distal coarse filter is defined by a coarse filter membrane which is self-supporting.

6. The water sampling immersion probe of claim 5 , wherein the coarse filter membrane of the distal coarse filter is substantially flat.

7. The water sampling immersion probe of claim 6 , wherein,
the coarse filter membrane of the coarse filter and the fine filter membrane of the fine filter are each flat and are arranged substantially parallel to each other, and
a general plane of each of the coarse filter membrane, the fine filter membrane, and the resulting venting chamber are inclined with respect to the vertical (V) at an inclination angle of 10° to 40°.

8. The water sampling immersion probe of claim 5 , wherein the proximal fine filter is defined by a fine filter membrane, wherein the coarse filter membrane and the fine filter membrane are each generally cylindrical in shape and are arranged coaxially with respect to each other.

9. The water sampling immersion probe of claim 8 , wherein,
the venting chamber is generally cylindrical, and
the venting opening is arranged at a vertically lowest region of the venting chamber.

10. The water sampling immersion probe of claim 1 , wherein the distal coarse filter is defined by a coarse filter membrane which is at least one of self-supporting and comprises a lipophilic surface.

11. The water sampling immersion probe of claim 1 , further comprising:
a suction chamber arranged downstream of the proximal fine filter; and
a separate stiff support body arranged in the suction chamber which mechanically supports the proximal fine filter and which is permeable to water.

12. The water sampling immersion probe of claim 1 , further comprising:
a protection fork comprising at least two fork tines, the protection fork being arranged distal of and at the outside of the coarse filter membrane, wherein,
a lateral tine distance (D) of two neighboring fork tines of the at least two fork tines is 5 to 50 mm.

13. The water sampling immersion probe of claim 12 , wherein,
each of the at least two fork tines comprise a free end and at least one closed end, and
the free end of each of the at least two fork tines are arranged downstream in a direction of a flowing wastewater, and
the free end of each of the at least two fork tines is arranged higher than the at least one closed end of the at least two fork tines in the direction of the flowing wastewater.

14. The water sampling immersion probe of claim 13 , further comprising:
a next upstream flow resistance structure, wherein,
a distance (X) between the at least one closed end of the at least two fork tines and the next upstream flow resistance structure is at least 50 mm.

15. A process water analysis arrangement for continuously analyzing a water sample of wastewater, the process water analysis arrangement comprising:
a water sampling immersion probe for continuously filtering a water sample from wastewater, the water sampling immersion probe comprising:
a distal coarse filter comprising a porosity of 0.1 to 1.0 mm;
a proximal fine filter arranged downstream of the distal coarse filter, the proximal fine filter comprising a porosity of less than 50 μm, the distal coarse filter and the proximal fine filter being arranged so as to not contact each other, wherein the distal coarse filter and the proximal fine filter define a venting chamber, wherein the venting chamber is vented at a bottom and the venting chamber is inclined with respect to vertical with an inclination angle between 5° and 80° degrees and completely submerged so that rising air bubbles remain in contact with a distal side of a membrane of the proximal fine filter over the entire height of the membrane; and
a sample suction opening arranged downstream of the proximal fine filter;

a control unit comprising a sample pump, and
a water analysis apparatus,
wherein, the water analysis apparatus is fluidically connected to the sample suction opening so that the water sample is pumped from the water sampling immersion probe by the sample pump to the water analysis apparatus.

Assignees

• Hach Lange Gmbh

Inventors

• Battefeld Manfred
• Steinhauer Frank
• Stellmach-Hanulok Aurelia
• Aleth Nina
• Brubaker Silke
• Leyer Axel
• Dräger Hartmut
• Goertz Sebastian
• Kussmann Michael
• Küppers Michael

Classifications

• G01N2001/1043

  from sewers · CPC title

• G01N1/14

  Suction devices, e.g. pumps; Ejector devices · CPC title

• C02F1/44

  by dialysis, osmosis or reverse osmosis {(general membrane separation processes B01D61/00, membrane modules B01D63/00, electrodialysis C02F1/4693, combination of membrane modules and bioreactors C02F3/1268)} · CPC title

• B01D2325/02

  Details relating to pores or porosity of the membranes · CPC title

• B01D2319/02

  Elements in series · CPC title