Wood template-supported phase change composite for thermal energy applications

Patent metadata

Field	Value
Publication number	US-12280518-B2
Application number	US-202217936925-A
Country	US
Kind code	B2
Filing date	Sep 30, 2022
Priority date	Sep 30, 2021
Publication date	Apr 22, 2025
Grant date	Apr 22, 2025

Abstract

Wood template-supported phase change material (PCM) composite having thermal energy storage applications. A wood template-supported PCM may include a wood template that has had at least a portion of its xylan and/or lignin removed and saturated with a PCM. The PCM may be stabilized with a cross linkable network for improved infiltration into the wood template. The wood template-supported PCM composite may be formed by extracting xylan and/or lignin from the wood to create a wood template, densifying at least a portion of the wood template, and inserting a PCM into the wood template.

First claim

The invention claimed is:

1. A method of forming a wood template-supported phase change composite, the method comprising:
extracting a xylan from a wood, resulting in a wood template;
densifying at least a portion of the wood template; and
inserting a phase change material into the wood template, wherein:
the phase change material comprises a material that can absorb or release heat when changing phase, and
the phase change material comprises polyethylene glycol and the stabilizing agent comprises poly(ethylene glycol) diacrylate.

2. The method of claim 1 , wherein the extracting comprises:
soaking at least a portion of the wood in a first solution;
removing the wood from the first solution;
applying a heat and a pressure to the wood; and
washing the wood with a second solution.

3. The method of claim 2 , wherein:
the first solution comprises water, and
the second solution comprises at least one of water or methanol.

4. The method of claim 2 , wherein:
the heat is in the range of about 100° F. to about 250° F.

5. The method of claim 4 , wherein:
the heat is in the range of about 140° F. to about 190° F.

6. The method of claim 1 , wherein the densifying comprises:
wetting at least a portion of the wood template, and
compressing the wood template.

7. The method of claim 6 , wherein the wetting comprises:
soaking the at least a portion of the wood template in water.

8. The method of claim 6 , wherein the compressing comprises:
positioning a first plate on a first side of the wood template,
positioning a second plate on a second side of the wood template, and
applying a pressure the wood template through the first plate and the second plate.

9. The method of claim 8 , wherein:
the pressure comprises a displacement rate of approximately 1 mm/min.

10. The method of claim 1 , wherein the inserting comprises:
soaking the wood template in a solution comprising the phase change material and a stabilizing agent.

11. The method of claim 1 , wherein:
the phase change material and the stabilizing agent are cross-linkable.

12. The method of claim 1 , wherein:
the wood comprises at least one of pine, balsa, cedar, spruce, firwood, hemlock timber, teak wood, oak, maple, cherry, walnut, beech, mahogany, mango wood, sal wood, or ash.

13. The method of claim 1 , further comprising:
using the wood-template supported phase change composite for thermal energy storage.

14. A wood template-supported phase change composite device comprising:
a wood template; and
a phase change material and a stabilizing agent inserted in the wood template; wherein:
the wood template comprises a wood that has had a xylan removed and at least a portion of the wood template is densified, and
the phase change material comprises polyethylene glycol and the stabilizing agent comprises poly(ethylene glycol) diacrylate.

15. The device of claim 14 , wherein:
the phase change material comprises a material that can absorb or release heat when changing phase.

16. The device of claim 14 , wherein:
the phase change material and the stabilizing agent are cross-linkable.

17. The device of claim 14 , wherein:
the wood comprises at least one of pine, balsa, cedar, spruce, firwood, hemlock timber, teak wood, oak, maple, cherry, walnut, beech, mahogany, mango wood, sal wood, or ash.

Assignees

• Alliance Sustainable Energy
• Univ Texas

Inventors

• Cui Shuang
• BOOTEN Charles William
• Vidal Judith Cecilia
• Li Yudong
• Foster Kyle Edward O'Neil
• Chen Xiaowen
• Lynch Kelsey Mary
• Lu Hongbing
• Magalindan Bernadette Karen
• Perruci Gustavo Felicio

Classifications

• B27K5/001

  Heating · CPC title

• B27K2240/60

  Improving the heat-storage capacity · CPC title

• B27K2240/10

  Extraction of components naturally occurring in wood, cork, straw, cane or reed · CPC title

• F28D20/023 Primary

  the latent heat storage material being enclosed in granular particles or dispersed in a porous, fibrous or cellular structure · CPC title

• F28D2020/0017

  the heat storage material being enclosed in porous or cellular or fibrous structures · CPC title