Method, data set and sensored mixer to sense a property of a liquid

Patent metadata

Field	Value
Publication number	US-12276629-B2
Application number	US-202118015784-A
Country	US
Kind code	B2
Filing date	Jul 14, 2021
Priority date	Jul 16, 2020
Publication date	Apr 15, 2025
Grant date	Apr 15, 2025

Abstract

Sensored mixer, comprising a mixing device for mixing two or more components to produce a mixed liquid at a mixer output, and a property sensor for determining a property of a liquid, the property sensor comprising a) a channel comprising a sensing zone through which the liquid flows; b) two electrodes for generating an electric field of one or more sensing frequencies in the sensing zone; c) a data storage device comprising a pre-stored set of calibration data representing calibration impedance responses measured previously at the one or more sensing frequencies and at different property values of the property of an identical liquid; and d) a device to repeatedly i) generate between the electrodes an electric field of in the sensing zone; ii) sense between the electrodes, a response impedance; iii) derive from the response impedance a property value of the property of the liquid, using the pre-stored set of calibration data representing calibration impedance responses, wherein the property sensor is in fluid communication with the mixer output such that the mixed liquid can flow from the mixer output through the sensing zone. A method for sensing a property of the liquid and a data set of calibration data representing calibration impedance responses usable with the sensor and the method are also disclosed.

First claim

The invention claimed is:

1. A sensored mixer comprising a mixing device ( 120 ) for mixing two or more components (A, B) to produce a mixed liquid ( 10 ) at a mixer output ( 170 ), and a property sensor ( 1 ) for determining a property value of a property of the mixed liquid ( 10 ), the property sensor comprising a) a channel ( 20 ) comprising a sensing zone ( 50 ) through which-in use-the mixed liquid flows; b) two electrodes ( 30 , 40 ) for generating an electric field of one or more sensing frequencies in the sensing zone; c) a data storage device ( 230 ) comprising a pre-stored set of calibration data representing calibration impedance responses measured previously at the one or more sensing frequencies and at different property values of the property of an identical liquid; and d) a property value deriver ( 220 ), electrically connected to the electrodes ( 30 , 40 ), and operable to repeatedly i) generate, while the mixed liquid ( 10 ) flows through the sensing zone ( 50 ), between the electrodes ( 30 , 40 ) an electric field of the one or more sensing frequencies in the sensing zone; ii) sense between the electrodes ( 30 , 40 ), at the one or more sensing frequencies, while the mixed liquid ( 10 ) flows through the sensing zone ( 50 ) and while the electric field is present, a response impedance; iii) derive from the response impedance a property value of the property of the mixed liquid ( 10 ), using the pre-stored set of calibration data representing calibration impedance responses, wherein the property sensor ( 1 ) is in fluid communication with the mixer output ( 170 ) such that the mixed liquid ( 10 ) can flow from the mixer output ( 170 ) through the sensing zone ( 50 ).

2. The sensored mixer according to claim 1 , wherein the channel ( 20 ) comprises a first longitudinal section ( 180 ) having a first open cross section available for the flow of the mixed liquid ( 10 ), and a second longitudinal section ( 260 ), downstream from the first longitudinal section ( 180 ), having a second open cross section available for the flow of the mixed liquid ( 10 ), wherein the second open cross section is larger than the first open cross section, and wherein the sensing zone ( 50 ) is comprised in the second longitudinal section ( 260 ).

3. The sensored mixer according to claim 1 , wherein one or both of the electrodes ( 30 , 40 ) is/are arranged such as to be in contact with the mixed liquid ( 10 ) when the liquid flows through the sensing zone ( 50 ).

4. The sensored mixer according to claim 1 , wherein the sensing zone ( 50 ) is arranged between the electrodes ( 30 , 40 ).

5. The sensored mixer according to claim 1 , wherein the channel ( 20 ) comprises a bypass ( 290 , 310 ), arranged such that a first portion ( 270 ) of the mixed liquid ( 10 ) flows through the sensing zone ( 50 ), and a second portion ( 280 , 300 ) of the liquid flows through the bypass ( 290 , 310 ) bypassing the sensing zone.

6. The sensored mixer according to claim 5 , wherein one of the electrodes ( 30 , 40 ) is arranged between the sensing zone ( 50 ) and the bypass ( 290 , 310 ).

7. The sensored mixer according to claim 1 , further comprising a temperature sensor ( 350 ) for sensing a temperature of the mixed liquid ( 10 ) in the channel ( 20 ) or in the sensing zone ( 50 ).

8. The sensored mixer according to claim 1 , further comprising a flow speed sensor ( 360 ) for sensing a flow speed of the mixed liquid ( 10 ) through the channel ( 20 ) or through the sensing zone ( 50 ).

9. A process of determining a property value of a property of a liquid ( 10 ), comprising the steps, in this sequence, of i) providing a liquid ( 10 ) and a property sensor ( 1 ) for determining a property value of a property of the liquid ( 10 ), the property sensor comprising a) a channel ( 20 ) comprising a sensing zone ( 50 ) through which-in use-the liquid flows; b) two electrodes ( 30 , 40 ) for generating an electric field of one or more sensing frequencies in the sensing zone; c) a data storage device ( 230 ) comprising a pre-stored set of calibration data representing calibration impedance responses measured previously at the one or more sensing frequencies and at different property values of the property of an identical liquid; and d) a property value deriver ( 220 ), electrically connected to the electrodes ( 30 , 40 ), and operable to repeatedly 1 ) generate, while the liquid ( 10 ) flows through the sensing zone ( 50 ), between the electrodes ( 30 , 40 ) an electric field of the one or more sensing frequencies in the sensing zone; 2 ) sense between the electrodes ( 30 , 40 ), at the one or more sensing frequencies, while the liquid ( 10 ) flows through the sensing zone ( 50 ) and while the electric field is present, a response impedance; 3 ) derive from the response impedance a property value of the property of the liquid ( 10 ), using the pre-stored set of calibration data representing calibration impedance responses, and having the liquid ( 10 ) flow through the sensing zone ( 50 ); ii) generating, while the liquid ( 10 ) flows through the sensing zone ( 50 ), between the electrodes ( 30 , 40 ) an electric field of the one or more sensing frequencies in the sensing zone ( 50 ); iii) sensing between the electrodes ( 30 , 40 ), at the one or more sensing frequencies, while the liquid ( 10 ) flows through the sensing zone ( 50 ) and while the electric field is present, a response impedance; iv) deriving from the response impedance a property value of the property of the liquid ( 10 ), using the pre-stored set of calibration data representing calibration impedance responses.

10. The process according to claim 9 , wherein at least one of the one or more sensing frequencies is a frequency of between 1 Hertz and 10000 Hertz, and wherein the amplitude of the electric field is between 100 Volt per meter and 20000 Volt per meter.

11. The process according to claim 9 , wherein the liquid ( 10 ) is an adhesive or a curable adhesive or a two-component adhesive or a multi-component adhesive or a curable two-component adhesive.

12. The process according to claim 9 , wherein the liquid ( 10 ) has a dynamic viscosity of between 10 Pascalseconds and 40,000.0 Pascalseconds, measured at 25° C. according to standard ASTM D7042-12a in its version in force on 1 Jul. 2020.

13. A method comprising forming a set of calibration data representing calibration impedance responses for use in the process according to claim 9 , wherein the set of calibration data further represents a property value of a property of a calibration liquid at which property value one of the calibration impedance response was sensed.

14. The method according to claim 13 , wherein the set of calibration data further represents a sensing frequency at which sensing frequency one of the calibration impedance responses was sensed, and/or wherein the set of calibration data further represents a temperature of the liquid ( 10 ) in the sensing zone ( 50 ) at which temperature one of the calibration impedance responses was sensed.

Assignees

• 3M Innovative Properties Company

Inventors

• Münstermann Benjamin
• Schumacher Knut
• Zilligen Günter
• Stottmeister Martin
• Bialluch Robert
• Bahners Michael
• Keller Thomas
• Orda Peter
• Hahn Jörg
• Westkamp Harald
• Backes Andreas
• Wischnepolski Waleri
• Rudek David

Classifications

• G01N27/226

  Construction of measuring vessels; Electrodes therefor · CPC title

• G01N27/07

  Construction of measuring vessels; Electrodes therefor · CPC title

• G05D11/136

  by sensing the viscosity · CPC title

• G01N27/08

  which is flowing continuously · CPC title

• G01N27/10 Primary

  Investigation or analysis specially adapted for controlling or monitoring operations or for signalling · CPC title