Method for coating short fibres

Patent metadata

Field	Value
Publication number	US-12269780-B2
Application number	US-202118012121-A
Country	US
Kind code	B2
Filing date	Jun 21, 2021
Priority date	Jul 1, 2020
Publication date	Apr 8, 2025
Grant date	Apr 8, 2025

Abstract

A method for coating fibres includes coating short fibres having an average length less than or equal to 5 mm by chemical vapour deposition in a fluidised bed, the short fibres treated being made of ceramic material or carbon and being mixed with spacer particles distinct from the short fibres, the spacer particles having an average diameter greater than or equal to 20 μm.

First claim

The invention claimed is:

1. A method for coating fibres, comprising:
coating short fibres having an average length less than or equal to 5 mm by chemical vapour deposition in a fluidised bed, the short fibres treated being made of ceramic material or carbon and being mixed with spacer particles distinct from the short fibres, said spacer particles having an average diameter greater than or equal to 20 μm, the spacer particles belonging to Geldart groupings A or B and the content by volume of spacer particles in the mixture with the short fibres being between 25% and 95%.

2. The method according to claim 1 , wherein the spacer particles are present at a level between 50% and 95% by volume in the mixture with the short fibres.

3. The method according to claim 1 , wherein the average diameter of the spacer particles is greater than or equal to 50 μm.

4. The method according to claim 3 , wherein the average diameter of the spacer particles is greater than or equal to 100 μm.

5. The method according to claim 1 , wherein, during the coating, the mixture of short fibres and spacer particles is stirred using a stirring member.

6. The method according to claim 1 , wherein the short fibres and the spacer particles are present in a reactor during the coating, and wherein a vibratory motion is imposed on said reactor during the coating, using a vibrating member.

7. The method according to claim 1 , wherein the short fibres are made of silicon carbide, and wherein, on the short fibres, is deposited at least one layer of: pyrolytic carbon, boron nitride, silicon-doped boron nitride, silicon nitride or boron-doped carbon.

8. The method according to claim 1 , wherein the method comprises:
introducing short fibres and spacer particles into a reactor, the short fibres being coated with a sizing,
desizing so as to remove all or part of the sizing of the short fibres in the reactor, and then
coating the short fibres in the reactor as defined in claim 1 .

9. A method for manufacturing a composite material part, comprising:
implementing a method according to claim 1 in order to obtain coated short fibres,
separating the coated short fibres from at least a portion of the spacer particles,
moulding the coated short fibres thus separated from the spacer particles so as to form a porous preform of the part to be obtained, and
forming a matrix in the pores of the preform in order to obtain the composite material part.

10. A method for manufacturing a composite material part, comprising:
implementing a method according to claim 1 , in order to obtain coated short fibres,
separating the coated short fibres from at least a portion of the spacer particles,
mixing the coated short fibres thus separated from the spacer particles with the matrix material or with a matrix precursor, and
introducing the mixture thus obtained into a mould and the heat treatment of the introduced mixture, in order to obtain the composite material part.

Assignees

• Safran Ceram
• Centre Nat Rech Scient
• Univ Bordeaux

Inventors

• Delehouze Arnaud
• Bouillon Eric
• Bertrand Nathalie Dominique
• Guette Alain Jean-Michel
• El Mansouri Armine

Classifications

• C23C16/442

  using fluidised bed process · CPC title

• C23C16/345

  Silicon nitride · CPC title

• C23C16/342

  Boron nitride · CPC title

• C23C16/26

  Deposition of carbon only · CPC title

• C23C16/045

  Coating cavities or hollow spaces, e.g. interior of tubes; Infiltration of porous substrates · CPC title