Production of flavor concentrates by osmosis

Patent metadata

Field	Value
Publication number	US-12268227-B2
Application number	US-201716762887-A
Country	US
Kind code	B2
Filing date	Nov 9, 2017
Priority date	Nov 9, 2017
Publication date	Apr 8, 2025
Grant date	Apr 8, 2025

Abstract

The present invention relates to a process for preparing of a food concentrate in which an aqueous starting solution from a foodstuff is concentrated by osmosis with a semi-permeable biomimetic membrane. In addition, the present invention relates to a food concentrate which can be produced by the process according to the invention, a food concentrate which is free of disturbing aroma components with an OAV (odour activity value) ≥1 and which does not contain any solvent additives. Furthermore, the present invention relates to the use of the food concentrates and products comprising the food concentrate according to the invention.

First claim

The invention claimed is:

1. A process for preparing a food concentrate comprising:
preparing an aqueous starting solution from a food, wherein the aqueous starting solution is a vapor condensate obtained from a fruit or a vegetable,
concentrating the aqueous starting solution by forward osmosis with a semi-permeable biomimetic membrane, and
thereby forming a food concentrate as a retentate;
wherein the semipermeable biomimetic membrane comprises:
vesicles of liposomes comprising at least one aquaporin protein incorporated therein or vesicles of polymersomes comprising at least one aquaporin protein incorporated therein;
a thin film composite matrix in which the vesicles are embedded; and
a carrier layer;

wherein the osmosis is carried out at a temperature in a range of 10° C. to 40° C.; and
wherein the aqueous starting solution is concentrated by a factor of 20 to 1000.

2. A process according to claim 1 , wherein the liposome comprises lipids selected from DPhPC, DOPC, mixed soybean lipids, asolectin, mixed lipids of E. coli , or combinations thereof; and wherein the polymersome comprises: triblock copolymers of the hydrophilic-hydrophobic-hydrophilic-type (A-B-A, A-B-C, C-B-A, wherein A is PMOXA, B is PDMS and C is PEO), diblock copolymers of the hydrophilic-hydrophobic type (A-B, wherein A is PB and B is PEO), or combinations thereof.

3. A process according to claim 1 , wherein the aquaporin protein comprises at least one selected from the group consisting of AQP0, AqpZ, SoPIP2, AQP10, and their isoforms.

4. A process according to claim 1 , wherein the thin film composite matrix is prepared by polymerizing an aqueous solution of an amine with a solution of an acid chloride in an organic solvent.

5. A process according to claim 1 , comprising recovering in the retentate aroma substances having an OAV (odour activity value) ≥1 in the aqueous starting solution wherein a recovery rate of the aroma substances having an OAV ≥1 in the aqueous starting solution is >90% in the retentate, by weight relative to the aroma substances having an OAV ≥1 in the aqueous starting solution.

6. A process according to claim 1 , comprising recovering in the retentate aroma substances having a log-sensory recovery coefficient W>3 in the aqueous starting solution wherein the recovery rate of aroma substances having log-sensory recovery coefficient W of the aroma substances with W>−3, is ≥50%; by weight relative to the aroma substances having a log-sensory recovery coefficient W>−3 in the aqueous starting solution.

7. A process according to claim 1 , wherein the aqueous starting solution comprises ethanol, and wherein any remaining ethanol content in the retentate is reduced by at least 50%, by weight relative to the ethanol content in the aqueous starting solution.

Assignees

• Symrise Ag

Inventors

• Kiefl Johannes
• Utermöhle Claudia
• Brennecke Stefan

Classifications

• A61K2800/10

  General cosmetic use · CPC title

• A23V2002/00

  Food compositions, function of food ingredients or processes for food or foodstuffs · CPC title

• A61K47/46

  Ingredients of undetermined constitution or reaction products thereof, e.g. skin, bone, milk, cotton fibre, eggshell, oxgall or plant extracts · CPC title

• A61Q19/00

  Preparations for care of the skin · CPC title

• A61Q11/00

  Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses · CPC title