Physical property measurement method, physical property measurement device, and probe

Patent metadata

Field	Value
Publication number	US-12253449-B2
Application number	US-202218051012-A
Country	US
Kind code	B2
Filing date	Oct 31, 2022
Priority date	May 1, 2020
Publication date	Mar 18, 2025
Grant date	Mar 18, 2025

Abstract

Provided are a physical property measurement method, a physical property measurement device, and a probe that can simply measure physical properties of a surface layer portion of an object. A physical property measurement method includes a step of bringing a probe into contact with a surface layer portion of a liquid or gel-like object and maintaining a contact state, a step of measuring a height of the object rising along the probe in contact with the object, and a step of calculating viscous properties or elastic properties of the surface layer portion of the object using the measured height of the object rising along the probe.

First claim

What is claimed is:

1. A physical property measurement method comprising:
a step of bringing a probe into contact with a surface layer portion of a liquid or gel-like object and maintaining a contact state;
a step of measuring a height of the object rising along the probe in contact with the object; and
a step of calculating a viscosity or an elastic property of the surface layer portion of the object using the measured height of the object rising along the probe and based on one of the following expressions:

σ
·
2

⁢
π
⁢
R

≈

G
·

h
R

·
π

⁢

R
2

⁢

and
⁢

η

≈

σ
⁢

R
2

h
2

⁢
k

⁢
t

,

where σ represents a surface tension of the object, G represents a shear modulus of the surface layer portion of the object, R represents a diameter of a tip portion of the probe at the height of the object rising along the probe, h represents the height of the object as measured, κ represents a meniscus curvature of the surface layer portion of the object, η represents the viscosity, and t represents time in seconds.

2. The physical property measurement method according to claim 1 ,
wherein the probe extends linearly and has a base portion and the tip portion,
the tip portion is thinner than the base portion, and
the tip portion of the probe is brought into contact with the surface layer portion of the object.

3. The physical property measurement method according to claim 1 ,
wherein a diameter of a thickest part in a portion of the probe which is in contact with the object is equal to or less than ⅓ of a thickness of the surface layer portion of the object.

4. The physical property measurement method according to claim 2 ,
wherein, in the probe, a diameter of the tip portion decreases toward a side opposite to the base portion.

5. The physical property measurement method according to claim 2 ,
wherein, in the probe, the base portion and the tip portion have a cylindrical shape, and the tip portion is thinner than the base portion.

6. The physical property measurement method according to claim 2 ,
wherein a diameter of a thickest part in a portion of the probe which is in contact with the object is equal to or less than ⅓ of a thickness of the surface layer portion of the object.

7. The physical property measurement method according to claim 3 ,
wherein, in the probe, a diameter of the tip portion decreases toward a side opposite to a base portion.

8. The physical property measurement method according to claim 3 ,
wherein, in the probe, a base portion and the tip portion have a cylindrical shape, and the tip portion is thinner than the base portion.

9. A physical property measurement device that measures a viscosity or an elastic property of a surface layer portion of a liquid or gel-like object, the physical property measurement device comprising:
a stage on which the object is placed;
a probe that is configured to come into contact with the surface layer portion of the object;
a driving unit that is configured to bring the probe into contact with the surface layer portion of the object and maintain a contact state, or separates the probe from the surface layer portion;
a measurement unit that is configured to measure a height of the object rising along the probe in contact with the object; and
a calculation unit that is configured to calculate the viscosity or the elastic property of the surface layer portion of the object using the height of the object rising along the probe measured by the measurement unit and based on one of the following expressions:

σ
·
2

⁢
π
⁢
R

≈

G
·

h
R

·
π

⁢

R
2

⁢

and
⁢

η

≈

σ
⁢

R
2

h
2

⁢
k

⁢
t

,

where σ represents a surface tension of the object, G represents a shear modulus of the surface layer portion of the object, R represents a diameter of a tip portion of the probe at the height of the object rising along the probe, h represents the height of the object as measured, κ represents a meniscus curvature of the surface layer portion of the object, η represents the viscosity, and t represents time in seconds,
wherein the tip portion of the probe has a part whose diameter is equal to or less than 33 μm.

10. The physical property measurement device according to claim 9 ,
wherein the probe extends linearly and has a base portion that is provided continuously with the tip portion, and
a diameter of the tip portion decreases toward a side opposite to the base portion.

11. The physical property measurement device according to claim 9 ,
wherein the probe extends linearly and has a base portion that is provided continuously with the tip portion,
the base portion and the tip portion have a cylindrical shape, and
the tip portion is thinner than the base portion.

Assignees

• Fujifilm Corp

Inventors

• Kajiya Tadashi
• Sawai Daisuke
• Miyata Koji
• Noda Hiroyuki

Classifications

• G01N2013/0283

  methods of calculating surface tension · CPC title

• G01N13/02

  Investigating surface tension of liquids · CPC title

• G01N11/10 Primary

  by moving a body within the material · CPC title

• G01N2011/006

  Determining flow properties indirectly by measuring other parameters of the system · CPC title

• G01N11/00 Primary

  Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties · CPC title