Process of producing high-quality lube base oil by using refined oil fraction of waste lubricant

Patent metadata

Field	Value
Publication number	US-12227705-B2
Application number	US-202318456321-A
Country	US
Kind code	B2
Filing date	Aug 25, 2023
Priority date	Aug 17, 2021
Publication date	Feb 18, 2025
Grant date	Feb 18, 2025

Abstract

Proposed is a process of producing a high-quality lube base oil using a refined oil fraction obtained from waste lubricant as a feedstock. The process includes purifying waste lubricant to obtain a refined oil fraction, pretreating the refined oil fraction, and blending the pretreated refined oil fraction with unconverted oil (UCO), before or after vacuum distillation and catalytic dewaxing of the unconverted oil, or between the vacuum distillation and the catalytic dewaxing of the unconverted oil.

First claim

What is claimed is:

1. A recycled oil product comprising:
a lube base oil prepared from a waste lubricant, wherein the recycled oil product has
a specific gravity ranging from 0.8 to 0.9,
a kinematic viscosity at 100° C. ranging from 3 to 8 cSt,
a viscosity index greater than or equal to 110,
a pour point ranging from −39° C. to −12° C., and
an aromatic content ranging from less than 1% to greater than 0%,
wherein the recycled oil product exhibits a UV 260-350 nm absorbance of 2.5 or less and a UV 325 nm absorbance of 0.7 or less, as measured by ASTM D 2008.

2. The recycled oil product of claim 1 , wherein the recycled oil product has a sulfur content ranging from less than 20 ppm to greater than 0 ppm.

3. The recycled oil product of claim 1 , wherein the recycled oil product has a nitrogen content ranging from less than 5 ppm to greater than 0 ppm.

4. The recycled oil product of claim 1 , wherein the recycled oil product has a chlorine content ranging from less than 1 ppm to greater than 0 ppm.

5. The recycled oil product of claim 1 , wherein the specific gravity is 0.84, the kinematic viscosity at 100° C. is 7.3 cSt, the viscosity index is 129, and the pour point is −12° C.

6. The recycled oil product of claim 5 , wherein the recycled oil product has a content of each of sulfur, nitrogen, and chlorine which is less than 1 ppm and greater than 0 ppm.

7. The recycled oil product of claim 1 , wherein the recycled oil product has a saturation degree of 90% or more.

8. The recycled oil product of claim 1 , wherein the recycled oil product has a saturation degree of 99% or more.

9. The recycled oil product of claim 1 , wherein the recycled oil product has a Saybolt color value of 27 or more, measured according to ASTM D 156.

10. The recycled oil product of claim 1 , wherein the recycled oil product has no solid impurities.

11. The recycled oil product of claim 1 , wherein the recycled oil product comprises a Group III grade lube base oil.

12. The recycled oil product of claim 1 , wherein the recycled oil product is produced by the following process of:
preparing a refined oil fraction by refining a waste lubricant;
pretreating the refined oil fraction; and
blending the pretreated refined oil fraction with unconverted oil before vacuum distillation and catalytic dewaxing of the unconverted oil, or between the vacuum distillation and the catalytic dewaxing,
wherein the vacuum distillation is performed before the catalytic dewaxing, and
wherein the unconverted oil refers to a heavy fraction remaining without being converted to fuel oil through a fuel oil hydrocracking process.

13. The recycled oil product of claim 12 , wherein the process comprises:
centrifuging the waste lubricant;
performing atmospheric distillation;
performing vacuum distillation; or
performing combinations thereof.

14. The recycled oil product of claim 12 , wherein, in the process, the amount of the refined oil fraction blended with the unconverted oil is 3% or more and 50% or less by volume.

Assignees

• Sk Innovation Co Ltd
• Sk Enmove Co Ltd

Inventors

• Jeon Young Wook
• Ok Jin Hee
• Noh Kyung Seok
• Kim Do Woan

Classifications

• C10N2070/00

  Specific manufacturing methods for lubricant compositions · CPC title

• C10N2030/20

  Colour, e.g. dyes · CPC title

• C10N2030/02

  Pour-point; Viscosity index · CPC title

• C10M2203/1006

  used as base material · CPC title

• C10M175/005

  using extraction processes; apparatus therefor · CPC title