Method for degreasing shaped ceramic molded body and method for manufacturing ceramic fired body

Patent metadata

Field	Value
Publication number	US-12221386-B2
Application number	US-202017005781-A
Country	US
Kind code	B2
Filing date	Aug 28, 2020
Priority date	Mar 1, 2018
Publication date	Feb 11, 2025
Grant date	Feb 11, 2025

Abstract

A ceramic molded body including a ceramic powder and an organic binder includes an oxidizable ceramic powder as the ceramic powder, includes an oxidizable metal or metal compound, or is in contact with a solid body including an oxidizable metal or metal compound. In a hydrogen atmosphere, the ceramic molded body is heated to a maximum temperature set within a range of 1,100° C. to 1,400° C. at a heating rate of more than 25° C./h, is degreased at the maximum temperature, and is then cooled at a cooling rate of more than 25° C./h.

First claim

What is claimed is:

1. A method for degreasing a ceramic molded body, comprising degreasing a ceramic molded body including a ceramic powder and an organic binder,
wherein the ceramic molded body includes an oxidizable ceramic powder as the ceramic powder, includes an oxidizable metal or metal compound, or is in contact with a solid body including an oxidizable metal or metal compound, and
in an atmosphere of hydrogen gas alone or in an atmosphere of a mixture of an inert gas and hydrogen gas with a hydrogen gas concentration of 20% by volume or more, the ceramic molded body is heated to a maximum temperature set within a range of 1,100° C. to 1,400° C. at a heating rate of more than 25° C./h, is degreased at the maximum temperature, and is then cooled at a cooling rate of more than 25° C./h, and
wherein the ceramic molded body is degreased without oxidizing the oxidizable ceramic powder and the oxidizable metal or metal compound, and without forming cracks in the ceramic molded body.

2. A method for degreasing a ceramic molded body, comprising degreasing a ceramic molded body including a ceramic powder and an organic binder,
wherein the ceramic molded body includes an oxidizable ceramic powder as the ceramic powder, includes an oxidizable metal or metal compound, or is in contact with a solid body including an oxidizable metal or metal compound, and
in an atmosphere of hydrogen gas alone or in an atmosphere of a mixture of an inert gas and hydrogen gas with a hydrogen gas concentration of 20% by volume or more, the ceramic molded body is heated to an intermediate temperature set within a range of 600° C. to 1,100° C. at a heating rate of more than 25° C./h, is held at the intermediate temperature for a predetermined period of time, is heated to a maximum temperature set above the intermediate temperature within a range of 1,100° C. to 1,400° C. at a heating rate of more than 25° C./h, is degreased at the maximum temperature, and is then cooled at a cooling rate of more than 25° C./h, and
wherein the ceramic molded body is degreased without oxidizing the oxidizable ceramic powder and the oxidizable metal or metal compound, and without forming cracks in the ceramic molded body.

3. The method for degreasing a ceramic molded body according to claim 1 ,
wherein the oxidizable ceramic powder is aluminum nitride, silicon nitride, or silicon carbide.

4. The method for degreasing a ceramic molded body according to claim 1 ,
wherein the oxidizable metal is Ni, W, or Mo, and the oxidizable metal compound is WC or MoC.

5. The method for degreasing a ceramic molded body according to claim 1 ,
wherein the heating and cooling rates are 50° C./h to 500° C./h.

6. The method for degreasing a ceramic molded body according to claim 1 ,
wherein the ceramic molded body has a porosity of 20% by volume to 70% by volume.

7. A method for manufacturing a ceramic fired body, comprising:
a degreasing step of degreasing a ceramic molded body including a ceramic powder and an organic binder; and
a firing step of firing the degreased ceramic molded body,
wherein the method for degreasing a ceramic molded body according to claim 1 is employed in the degreasing step.

8. The method for degreasing a ceramic molded body according to claim 2 ,
wherein the oxidizable ceramic powder is aluminum nitride, silicon nitride, or silicon carbide.

9. The method for degreasing a ceramic molded body according to claim 2 ,
wherein the oxidizable metal is Ni, W, or Mo, and the oxidizable metal compound is WC or MoC.

10. The method for degreasing a ceramic molded body according to claim 2 ,
wherein the heating and cooling rates are 50° C./h to 500° C./h.

11. The method for degreasing a ceramic molded body according to claim 2 ,
wherein the ceramic molded body has a porosity of 20% by volume to 70% by volume.

12. A method for manufacturing a ceramic fired body, comprising:
a degreasing step of degreasing a ceramic molded body including a ceramic powder and an organic binder; and
a firing step of firing the degreased ceramic molded body,
wherein the method for degreasing a ceramic molded body according to claim 2 is employed in the degreasing step.

Assignees

• Ngk Insulators Ltd

Inventors

• Onogi Tetsuya

Classifications

• B22F1/10

  Metallic powder containing lubricating or binding agents; Metallic powder containing organic material · CPC title

• C04B2235/6582

  Hydrogen containing atmosphere · CPC title

• C04B2235/6562

  Heating rate · CPC title

• C04B35/64

  Burning or sintering processes (C04B33/32 takes precedence {; powder metallurgy B22F}) · CPC title

• C04B35/638 Primary

  Removal thereof · CPC title