X-ray detector system with at least two stacked flat Bragg diffractors

Patent metadata

Field	Value
Publication number	US-12209977-B2
Application number	US-202418439625-A
Country	US
Kind code	B2
Filing date	Feb 12, 2024
Priority date	Feb 16, 2023
Publication date	Jan 28, 2025
Grant date	Jan 28, 2025

Abstract

An apparatus includes a plurality of stacked flat Bragg diffractors having at least a first flat Bragg diffractor and a second flat Bragg diffractor. The first and second flat Bragg diffractors are positioned sequentially along an x-ray propagation axis of an x-ray beam. The x-ray beam includes x-rays and has an angular beam divergence less than 30 mrad in at least one direction.

First claim

What is claimed is:

1. An apparatus comprising:
a plurality of flat Bragg diffractors comprising at least a first flat Bragg diffractor and a second flat Bragg diffractor, the first and second flat Bragg diffractors positioned sequentially along an x-ray propagation axis of an x-ray beam comprising x-rays and having an angular beam divergence less than 30 mrad in at least one direction, the first and second flat Bragg diffractors sequentially impinged by the x-rays and configured to reflect and diffract corresponding reflected and diffracted portions of the x-rays; and
an energy dispersive x-ray detector configured to receive and detect the reflected and diffracted portions from the plurality of flat Bragg diffractors.

2. The apparatus of claim 1 , wherein the first flat Bragg diffractor comprises a substantially flat multilayer, single crystal, or mosaic crystal configured to diffract at least some of the x-rays in accordance with Bragg's law.

3. The apparatus of claim 1 , wherein the first flat Bragg diffractor and the second flat Bragg diffractor are connected to one another and are configured to be sequentially impinged by the x-ray beam.

4. The apparatus of claim 1 , wherein the second flat Bragg diffractor is downstream from the first flat Bragg diffractor, the first flat Bragg diffractor configured to reflect and diffract a first reflected and diffracted portion of the x-rays and to transmit a first transmitted portion of the x-rays, the second flat Bragg diffractor configured to reflect and diffract a second reflected and diffracted portion of the first transmitted portion and to transmit a second transmitted portion of the first transmitted portion, the first reflected and diffracted portion having a first mean x-ray energy E 1 and a first energy resolution ΔE 1 and the second reflected and diffracted portion having a second mean x-ray energy E 2 and a second energy resolution ΔE 2 , the second x-ray energy E 2 different from the first x-ray energy E 1 .

5. The apparatus of claim 4 , wherein the first flat Bragg diffractor comprises a multilayer Bragg diffractor configured to reflect and diffract x-rays having x-ray energies less than 1 keV and the second flat Bragg diffractor comprises a single crystal and/or mosaic crystal and is configured to reflect and diffract x-rays having x-ray energies greater than 1 keV.

6. The apparatus of claim 5 , wherein the multilayer Bragg diffractor has a d-spacing in a range of 3 nanometers to 30 nanometers, the single crystal comprises a material selected from the group consisting of: diamond, quartz, graphite, stack of graphene layers, other materials comprising low atomic number elements, silicon (Si), germanium (Ge), lithium fluoride (LiF), mica, indium antimonide (InSb), polyethylene terephthalate (PET), ammonium dihydrophosphate (ADP), rubidium acid phtahalate (RAP), beryl, and thallium acid phthalate (TIAP), and the mosaic crystal comprises a material selected from the group consisting of: highly annealed pyrolitic graphite (HAPG) and highly oriented pyrolitic graphite (HOPG).

7. The apparatus of claim 4 , wherein the plurality of flat Bragg diffractors further comprises a third flat Bragg diffractor downstream from the second flat Bragg diffractor, the third flat Bragg diffractor configured to reflect and diffract a third reflected and diffracted portion of the second transmitted portion and to transmit a third transmitted portion of the second transmitted portion, the third reflected and diffracted portion having a third mean x-ray energy E 3 and a third energy resolution ΔE 3 , the third x-ray energy E 3 different from the first x-ray energy E 1 and from the second x-ray energy E 2 .

8. The apparatus of claim 7 , wherein the second flat Bragg diffractor is configured to diffract x-rays having x-ray energies in a range of 1 keV to 3 keV, and the third flat Bragg diffractor comprises a single crystal and/or mosaic crystal and is configured to reflect and diffract x-rays having x-ray energies greater than 3 keV.

9. The apparatus of claim 7 , wherein the first flat Bragg diffractor has a first x-ray transmittance greater than 1% for x-rays having the second x-ray energy E 2 and a third x-ray transmittance greater than 1% for x-rays having the third x-ray energy E 3 , and the second flat Bragg diffractor has a second x-ray transmittance greater than 1% for x-rays having the third x-ray energy E 3 .

10. The apparatus of claim 1 , wherein the plurality of flat Bragg diffractors are positioned along the x-ray propagation axis within a region extending along the x-ray propagation axis by a distance less than 200 millimeters.

11. The apparatus of claim 1 , wherein at least two adjacent flat Bragg diffractors of the plurality of flat Bragg diffractors are positioned along the x-ray propagation axis spaced from one another along the x-ray propagation axis by less than 30 millimeters.

12. The apparatus of claim 1 , wherein at least two flat Bragg diffractors of the plurality of flat Bragg diffractors comprise the same material as one another.

13. The apparatus of claim 12 , wherein the at least two flat Bragg diffractors are configured to reflect and diffract x-rays with atomic planes having the same Miller indices as one another and the x-rays are incident to each of the at least two flat Bragg diffractors at different Bragg angles such that a spectral bandwidth overlap between diffracted x-rays from the at least two flat Bragg diffractors is substantially zero.

14. The apparatus of claim 12 , wherein the x-rays are incident to each of the at least two flat Bragg diffractors at substantially equal Bragg angles and diffracting atomic planes of the at least two flat Bragg diffractors have different d-spacings.

15. The apparatus of claim 1 , wherein at least two flat Bragg diffractors of the plurality of flat Bragg diffractors comprise different materials from one another.

16. The apparatus of claim 1 , further comprising:
a fixture comprising a rigid frame; and
a plurality of mounts affixed to the fixture, the plurality of mounts configured to hold the plurality of flat Bragg diffractors along the x-ray propagation axis, each mount comprising a first portion configured to be affixed to a corresponding flat Bragg diffractor of the plurality of flat Bragg diffractors and a second portion configured to be controllably moved to adjust an angle of the corresponding flat Bragg diffractor relative to the x-ray propagation axis.

17. An apparatus configured to receive an x-ray beam propagating along an x-ray propagation axis with an angular beam divergence less than 30 mrad in at least one direction substantially perpendicular to the x-ray propagation axis, the apparatus comprising:
a plurality of sequentially stacked flat Bragg diffractors that are rigidly connected to one another with a separation between adjacent flat Bragg diffractors less than 200 millimeters, the plurality of sequentially stacked flat Bragg diffractors configured to receive the x-ray beam, each flat Bragg diffractor of the plurality of sequentially stacked flat Bragg diffractors configured to diffract a corresponding diffracted portion of the x-ray beam with a spectral overlap between the diffracted portions from different flat Bragg diffractors less than 25%; and
at least one x-ray detector configured to receive and detect the diffracted portions.

18. The apparatus of claim 17 , wherein the diffracted portions diffracted by at least two flat Bragg diffractors of the plurality of sequentially stacked flat Bragg diffractors have different mean x-ray energies th

Assignees

• Sigray Inc

Inventors

• Yun Wenbing
• Kirz Janos

Classifications

• G01N2223/0563

  measure of energy-dispersion spectrum of diffracted radiation · CPC title

• G01N2223/0568

  spectro-diffractometry · CPC title

• G01N2223/041

  X-ray absorption fine structure [EXAFS] · CPC title

• G01N2223/315

  monochromators · CPC title

• G01N2223/1016

  X-ray · CPC title