High purity tungsten hexachloride and method for making same
US-10100406-B2 · Oct 16, 2018 · US
US12195351B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-12195351-B2 |
| Application number | US-201916979021-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 24, 2019 |
| Priority date | Oct 25, 2018 |
| Publication date | Jan 14, 2025 |
| Grant date | Jan 14, 2025 |
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A molybdenum oxychloride or a tungsten oxychloride, wherein the molybdenum oxychloride or the tungsten oxychloride has a moisture content of less than 1 wt %. A method of producing a molybdenum oxychloride or a tungsten oxychloride, wherein a molybdenum oxide or a tungsten oxide as a raw material is subject to dehydration treatment at 400° C. or higher and 800° C. or less, and the raw material that underwent dehydration treatment is thereafter reacted with a chlorine gas to synthesize a molybdenum oxychloride or a tungsten oxychloride. An object of the present invention is to provide a molybdenum oxychloride or a tungsten oxychloride having a low moisture content, as well as a production method thereof.
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The invention claimed is: 1. A method of producing a molybdenum oxychloride or a tungsten oxychloride, wherein a molybdenum oxide or a tungsten oxide as a raw material is subject to dehydration treatment at 400° C. or higher and 800° C. or less while flowing inert gas, or inert gas mixed with oxygen, or air (O 2 +N 2 ), wherein the dehydration treatment time is set to be 3 hours or longer, and the raw material that underwent dehydration treatment is thereafter reacted with a chlorine gas to synthesize a molybdenum oxychloride or a tungsten oxychloride. 2. The method of producing a molybdenum oxychloride or a tungsten oxychloride according to claim 1 , wherein the dehydration treatment is at a temperature of 500° C. or higher and 750° C. or less.
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