High-Pressure Homogenizer and Method for Manufacturing Graphene Using the Same
US-2019284053-A1 · Sep 19, 2019 · US
US12194428B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-12194428-B2 |
| Application number | US-202117467377-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 6, 2021 |
| Priority date | Sep 16, 2020 |
| Publication date | Jan 14, 2025 |
| Grant date | Jan 14, 2025 |
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A multi-layered micro-channel mixer includes a base plate and a cover plate. Two inlet fluid reservoirs, two inlet channels, two groups of fluid distribution channel networks, two groups of process fluid channels, an impinging stream mixing chamber, a fluid mixing intensification channel and an outlet buffer reservoir are provided on the base plate. Two fluids are fed into the two inlet fluid reservoirs, respectively. The fluids then flow into the process fluid channels via the inlet channels and the multi-stage fluid distribution channel networks, respectively. Then the two fluid streams ejected from the opposing process fluid channels impinges upon each other in the impinging stream mixing chamber. The mixed fluid is subjected to vortex or secondary flow generated by the baffles or the internals in the impinging stream mixing chamber and fluid mixing intensification channel, and finally the mixed fluid is discharged through the outlet buffer reservoir.
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What is claimed is: 1. A multi-layered micro-channel mixer, comprising: a base plate; and a cover plate; wherein two inlet fluid reservoirs, two inlet channels, two groups of fluid distribution channel networks, two groups of process fluid channels, an impinging stream mixing chamber, a fluid mixing intensification channel and an outlet buffer reservoir are provided on the base plate; the cover plate is provided with three through-holes; two of the three through-holes are connected with the two inlet fluid reservoirs, respectively, and used as inlets of fluid materials to be mixed; the another one of the three through-holes is connected with the outlet buffer reservoir and used as an outlet of mixed fluid material; one end of each of the two inlet fluid reservoirs is connected with an external feed tube via a corresponding through-hole in the cover plate, and the other end of each of the two inlet fluid reservoirs is connected with one of the two inlet channels; each of the two inlet channels is connected with one group of process fluid channels via one group of fluid distribution channel network; each of the two groups of fluid distribution channel networks is composed of N stages of fluid distribution channels with different hydraulic diameters, wherein N is an integer ranging from 1-10; the first stage fluid distribution channels are directly connected with the two inlet channels, respectively; the N th stage fluid distribution channels have 2 N branch channels that are connected with 2 N next stage fluid distribution channels, or have 2 (N+1) branch channels that are connected with 2 (N+1) process fluid channels; each fluid distribution channel has two branch channels; each branch channel is connected with either a next stage fluid distribution channel or two process fluid channels; each branch channel of the last stage fluid distribution channels has two branches which are connected with two process fluid channels, respectively; one end of each of the process fluid distribution channels is connected with one branch channel of the last stage fluid distribution channels, and the other end of each of the process fluid channels is an outlet end and fixed inside the impinging stream mixing chamber; the two groups of process fluid channels are connected with the two inlet channels, respectively, and are symmetrically arranged on both sides of the impinging stream mixing chamber; the end of each of the process fluid channels inside the impinging stream mixing chamber is tapered; the impinging stream mixing chamber is directly connected with the fluid mixing intensification channel; internals or baffles are installed in the impinging stream mixing chamber; internals or baffles are installed in the fluid mixing intensification channel; the fluid mixing intensification channel is connected with the outlet buffer reservoir; and the outlet buffer reservoir is connected with an external discharge tube via the another one of the three through-holes; an angle α formed between each of the inlet channels and the corresponding first stage fluid distribution channel is 70°-130°; an angle β formed between each of the branch channels and the corresponding next stage fluid distribution channel is 70°-130°; an angle γ formed between two adjacent process fluid channels that are connected with the same branch channel is 95°-150°; each of the fluid distribution channels has a rectangular cross section; each of the first stage fluid distribution channels has a width of 0.1-30 mm, a depth of 0.1-15 mm and a length of 1-200 mm; the width, depth and length of the N th stage fluid distribution channel are 40%-90%, 40%-90% and 20%-80% of those of the (N−1) th stage fluid distribution channel, respectively, where N is an integer greater than or equal to 2; the baffles are installed in interval arrangement at both side walls of the impinging stream mixing chamber; an angle θ formed between each of the baffles and the side wall of the impinging stream mixing chamber is 20°-160°; the internals or baffles in the impinging stream mixing chamber are fixed away from the central axes of the process fluid channels, and are not in the same horizontal planes with the central axes of the process fluid channels; the distance between the central axis of the process fluid channel and its neighboring baffle or internal is 50-800 μm; a distance between two adjacent baffles or internals in the impinging stream mixing chamber is 50 μm-5 mm; the baffles are installed in interval arrangement at both side walls of the fluid mixing intensification channel; an angle φ formed between the baffle and the side wall of the fluid mixing intensification channel is 20°-160°; a distance between two adjacent baffles or internals in the fluid mixing intensification channel is 50 μm-5 mm; an outlet of each of the process fluid channels inside the impinging stream mixing chamber is tapered, and has a width of 1-500 μm; the process fluid channels are symmetrically arranged on both sides of the impinging stream mixing chamber; and a distance between the two tapered outlets of two process fluid channels symmetrically arranged with respect to the impinging stream mixing chamber is 10-500 μm. 2. The micro-channel mixer of claim 1 , wherein each of the two inlet channels has a rectangular cross section; each of the two inlet channels has a width of 50 μm-10 mm, a depth of 50 μm-10 mm and a length of 1-500 mm; and the two inlet channels are symmetrically arranged on both sides of the impinging stream mixing chamber. 3. The micro-channel mixer of claim 1 , wherein a cross section of each of the process fluid channels is rectangular; and each of the process fluid channels has a width of 50-1000 μm, a depth of 50-1000 μm and a length of 1-200 mm. 4. The micro-channel mixer of claim 1 , wherein a cross section of the impinging stream mixing chamber is rectangular; and the impinging stream mixing chamber has a width of 50 μm-10 mm, a depth of 50 μm-10 mm and a length of 1-500 mm. 5. The micro-channel mixer of claim 1 , wherein a cross section of each process fluid channel is rectangular; and each process fluid channel has a width of 50 μm-10 mm, a depth of 50 μm-10 mm and a length of 1-1000 mm. 6. The micro-channel mixer of claim 4 , wherein a height of the baffles or internals is equal to a depth of the impinging stream mixing chamber; a width of the baffles is 0.1-0.9 times that of the impinging stream mixing chamber; a length of the baffles is 0.1-2.0 times the width of the impinging stream mixing chamber; a width of the internals is 0.1-0.9 times that of the impinging stream mixing chamber; and a length of the internals is 0.1-2.0 times the width of the impinging stream mixing chamber. 7. The micro-channel mixer of claim 5 , wherein a height of the baffles or internals is equal to a depth of the fluid mixing intensification channel; a width of the baffles is 0.1-0.9 times that of the fluid mixing intensification channel; a length of the baffles is 0.1-2.0 times the width of the fluid mixing intensification channel; a width of the internals is 0.1-0.9 times that of the fluid mixing intensification channel; and a length of the internals is 0.1-2.0 times the width of the fluid mixing intensification channel. 8. The micro-channel mixer of claim 1 , wherein the internals in the impinging stream mixing chamber or the fluid mixing intensification channel are independently asterisk-shaped, X-shaped and Y-shaped. 9. A method of mixing fluids using the micro-channel mixer of claim 1 , comprising: simultaneously pumping two fluids into the two inlet fluid reservoirs, respectively; allowing the two fluids to flow into the two groups of process fluid channels sequentially through the two inlet channels and
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