Methods for producing a hollow-core fiber and for producing a preform for a hollow-core fiber

Patent metadata

Field	Value
Publication number	US-12189177-B2
Application number	US-202017619980-A
Country	US
Kind code	B2
Filing date	Jul 15, 2020
Priority date	Jul 17, 2019
Publication date	Jan 7, 2025
Grant date	Jan 7, 2025

Abstract

Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; providing a number of tubular anti-resonant element preforms; arranging the anti-resonant element preforms at target positions of the interior of the cladding tube wall, thereby forming a primary preform which has a hollow core region and an inner jacket region; and further processing the primary preform in order to form a secondary preform, including a process of elongating the primary preform in order to directly form the hollow-core fiber or to form the secondary preform. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that a primary preform with an outer diameter ranging from 20 to 70 mm is used for the elongation process.

First claim

The invention claimed is:

1. A method for producing an anti-resonant hollow-core fiber having a hollow core extending along a longitudinal axis of the hollow-core fiber and an inner sheath surrounding the hollow core, which inner sheath includes a plurality of anti-resonance elements, the method comprising the steps of:
(a) providing a cladding tube having an inner bore and a longitudinal axis, along which a cladding tube wall delimited by an inner side and an outer side extends;
(b) providing a plurality of tubular anti-resonance element preforms;
(c) arranging the anti-resonance element preforms at desired positions of the inner side of the cladding tube wall to form a primary preform having an outer diameter in the range of 20 to 70 mm;
(d) further processing of the primary preform into a secondary preform from which the hollow-core fiber is drawn, wherein the further processing includes elongating the primary preform and a single or repeated performance of one or more of the following hot-forming processes:
(i) collapsing additional sheath material,
(ii) collapsing additional sheath material and simultaneously elongating the primary preform, and

(e) drawing the secondary preform to form the hollow-core fiber, wherein the secondary preform resulting from further processing of the primary preform according to step (d) has an outside diameter in the range of 20 to 70 mm,
further comprising fixing and/or sealing using a sealing or bonding compound containing amorphous SiO 2 particles to arrange the anti-resonance element preforms and/or elongate the primary preform and/or draw the hollow-core fiber, and
wherein open ends of the anti-resonance element preforms and/or individual structural elements of the anti-resonance element preforms and/or any annular gap between tube elements of the anti-resonance element preforms are sealed by the sealing or bonding compound when the primary preform is elongated and/or when the hollow-core fibers are drawn.

2. The method according to claim 1 , further comprising, during the elongation of the primary preform, using a temperature-controlled heating element the temperature of which is kept precisely at +/−0.1° C.

3. The method according to claim 1 , further comprising, during the elongation of the primary preform, feeding the primary preform to a heating zone at a feed rate set to yield a throughput of at least 0.8 g/min and an average dwell time in the heating zone of less than 25 min.

4. The method according to claim 1 , wherein a draw-down ratio during the elongation of the primary preform is set to a value in the range of 1.05 to 10.

5. The method according to claim 1 , further comprising machining the inner side of the cladding tube and/or the outer side of the cladding tube.

6. The method according to claim 1 , further comprising machining at the desired positions to provide the inner side of the cladding tube with a longitudinal structure extending in the direction of the longitudinal axis of the cladding tube.

7. The method according to claim 1 , wherein, when the anti-resonance element preforms are arranged at desired positions on the inside of the cladding tube wall, upper ends of the anti-resonance element preforms are positioned at the desired positions using a positioning template.

8. The method according to claim 7 , wherein the cladding tube has a pair of end faces and the positioning template is used in the region of at least one of the end faces.

9. The method according to claim 3 , wherein the feed rate is set to yield a throughput in the range from 0.8 g/min to 85 g/min.

10. The method according to claim 9 , wherein the feed rate set to yield a throughput in the range from 3.3 g/min to 85 g/min.

11. The method according to claim 3 , wherein the average dwell time is in the range of 5 to 25 min.

12. The method according to claim 4 , wherein the draw-down ratio during the elongation of the primary preform is set to a value in the range of 1.05 to 5.

13. The method according to claim 5 , wherein the step of machining includes drilling, milling, grinding, honing, and/or polishing.

14. The method according to claim 8 , wherein the positioning template is used in the region of both of the end faces.

15. A method for producing a preform for an anti-resonant hollow-core fiber having a hollow core extending along a longitudinal axis of the hollow-core fiber and an inner sheath surrounding the hollow core, which inner sheath includes a plurality of anti-resonance elements, the method comprising the steps of:
(a) providing a cladding tube having an inner bore and a longitudinal axis, along which a cladding tube wall delimited by an inner side and an outer side extends;
(b) providing a plurality of tubular anti-resonance element preforms;
(c) arranging the anti-resonance element preforms at desired positions of the inner side of the cladding tube wall to form a primary preform having an outer diameter in the range of 20 to 70 mm; and
(d) further processing the primary preform into a secondary preform for the hollow-core fiber, wherein the further processing includes elongating the primary preform and
(i) collapsing additional sheath material,
(ii) collapsing additional sheath material and simultaneously elongating the primary preform such that the resulting secondary preform has an outside diameter in the range of 20 to 70 mm, further comprising fixing and/or sealing using a sealing or bonding compound containing amorphous SiO 2 particles to arrange the anti-resonance element preforms and/or elongate the primary preform and/or draw the hollow-core fiber, and
wherein open ends of the anti-resonance element preforms and/or individual structural elements of the anti-resonance element preforms and/or any annular gap between tube elements of the anti-resonance element preforms are sealed by the sealing or bonding compound when the primary preform is elongated and/or when the hollow-core fibers are drawn.

Assignees

• Heraeus Quarzglas

Inventors

• Rosenberger Manuel
• Trommer Martin
• Weimann Steffen
• Hünermann Michael
• Schuster Kay

Classifications

• G02B6/032

  with non solid core or cladding {(G02B6/02295 takes precedence)} · CPC title

• C03B2203/16

  Hollow core · CPC title

• C03B2201/02

  Pure silica glass, e.g. pure fused quartz · CPC title

• C03B37/02781

  Hollow fibres, e.g. holey fibres · CPC title

• C03B37/01262

  Depositing additional preform material as liquids or solutions, e.g. solution doping of preform tubes or rods · CPC title