Fine particle manufacturing apparatus and fine particle manufacturing method

Patent metadata

Field	Value
Publication number	US-12161986-B2
Application number	US-201917272882-A
Country	US
Kind code	B2
Filing date	Sep 2, 2019
Priority date	Sep 3, 2018
Publication date	Dec 10, 2024
Grant date	Dec 10, 2024

Abstract

Provided are a fine particle manufacturing apparatus and a fine particle manufacturing method, which manufacture smaller fine particles. The fine particle manufacturing apparatus has: a raw material supply unit that supplies raw materials for producing fine particles into a thermal plasma flame; a plasma torch in which the thermal plasma flame is generated and the raw materials supplied by the raw material supply unit is evaporated by the thermal plasma flame to form a mixture in a gaseous state; a plasma generation unit that generates the thermal plasma flame inside the plasma torch; and a gas supply unit that supplies quenched gas to the thermal plasma flame, wherein the gas supply unit supplies the quenched gas with time modulation of the supply amount of the quenched gas.

First claim

The invention claimed is:

1. A fine particle manufacturing apparatus comprising:
a feedstock supply section configured to supply feedstock for fine particle manufacturing into a thermal plasma flame;
a plasma torch configured to allow the thermal plasma flame to be generated therein and, by use of the thermal plasma flame, evaporate the feedstock supplied by the feedstock supply section to convert the feedstock into a mixture in a gas phase state;
a plasma generation section configured to generate the thermal plasma flame inside the plasma torch; and
a gas supply section configured to supply quenching gas to the thermal plasma flame,
wherein the gas supply section supplies the quenching gas while time-modulating an amount of supply of the quenching gas.

2. The fine particle manufacturing apparatus according to claim 1 , wherein the feedstock supply section supplies the feedstock into the thermal plasma flame while time-modulating an amount of supply of the feedstock into the thermal plasma flame.

3. The fine particle manufacturing apparatus according to claim 1 , wherein the plasma generation section supplies a high frequency current that is amplitude-modulated to a coil for generating the thermal plasma flame and generates, as the thermal plasma flame, a modulated induction thermal plasma flame whose temperature state is time-modulated, and
wherein the high frequency current has an ON time during which a current amplitude has a high value and an OFF time during which the current amplitude has a low value.

4. The fine particle manufacturing apparatus according to claim 3 , wherein, during the ON time of the high frequency current, the feedstock supply section increases the amount of supply of the feedstock.

5. The fine particle manufacturing apparatus according to claim 1 , wherein the feedstock supply section supplies the feedstock into the thermal plasma flame with the feedstock being dispersed in a particulate form.

6. The fine particle manufacturing apparatus according to claim 1 , wherein the feedstock supply section disperses the feedstock in liquid to obtain a slurry and converts the slurry into droplets to supply the droplets into the thermal plasma flame.

7. A fine particle manufacturing method comprising:
a first step of supplying feedstock for fine particle manufacturing to a thermal plasma flame; and
a second step of evaporating the feedstock by use of the thermal plasma flame to convert the feedstock into a mixture in a gas phase state and supplying quenching gas to the thermal plasma flame,
wherein in the second step, the quenching gas is supplied while an amount of supply of the quenching gas is time-modulated.

8. The fine particle manufacturing method according to claim 7 , wherein in the first step, the feedstock is supplied into the thermal plasma flame while an amount of supply of the feedstock into the thermal plasma flame is time-modulated.

9. The fine particle manufacturing method according to claim 7 , wherein in the first step, the feedstock is supplied into the thermal plasma flame with the feedstock being dispersed in a particulate form.

10. The fine particle manufacturing method according to claim 7 , wherein in the first step, the feedstock is dispersed in liquid to obtain a slurry, the slurry is converted into droplets, and the droplets are supplied into the thermal plasma flame.

11. The fine particle manufacturing apparatus according to claim 3 , wherein during the OFF time of the high frequency current, the gas supply section increases the amount of supply of the quenching gas.

12. The fine particle manufacturing method according to claim 7 , wherein a high frequency current that is amplitude-modulated is supplied to a coil for generating the thermal plasma flame, and a modulated induction thermal plasma flame is generated as the thermal plasma flame, and
wherein the high frequency current has an ON time during which a current amplitude has a high value and an OFF time during which the current amplitude has a low value.

13. The fine particle manufacturing method according to claim 12 , wherein in the second step, during the OFF time of the high frequency current, the amount of supply of the quenching gas is increased.

14. The fine particle manufacturing method according to claim 12 , wherein in the first step, during the ON time of the high frequency current, the amount of supply of the feedstock is increased.

15. The fine particle manufacturing apparatus according to claim 2 , wherein the plasma generation section supplies a high frequency current that is amplitude-modulated to a coil for generating the thermal plasma flame and generates, as the thermal plasma flame, a modulated induction thermal plasma flame whose temperature state is time-modulated, and
wherein the high frequency current has an ON time during which a current amplitude has a high value and an OFF time during which the current amplitude has a low value.

16. The fine particle manufacturing apparatus according to claim 15 , wherein during the OFF time of the high frequency current, the gas supply section increases the amount of supply of the quenching gas.

17. The fine particle manufacturing apparatus according to claim 11 , wherein during the ON time of the high frequency current, the feedstock supply section increases the amount of supply of the feedstock.

18. The fine particle manufacturing method according to claim 8 , wherein a high frequency current that is amplitude-modulated is supplied to a coil for generating the thermal plasma flame, and a modulated induction thermal plasma flame is generated as the thermal plasma flame, and
wherein the high frequency current has an ON time during which a current amplitude has a high value and an OFF time during which the current amplitude has a low value.

19. The fine particle manufacturing method according to claim 18 , wherein in the second step, during the OFF time of the high frequency current, the amount of supply of the quenching gas is increased.

20. The fine particle manufacturing method according to claim 13 , wherein in the first step, during the ON time of the high frequency current, the amount of supply of the feedstock is increased.

Assignees

• Univ Nat Corp Kanazawa
• Nisshin Seifun Group Inc

Inventors

• Tanaka Yasunori
• Shimizu Kotaro
• SUEYASU Shiori
• Watanabe Shu
• Watanabe Tomoya
• Nakamura Keitaro

Classifications

• H05H1/30

  using applied electromagnetic fields, e.g. high frequency or microwave energy (H05H1/28 takes precedence) · CPC title

• C01B33/027 Primary

  by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material · CPC title

• B22F9/14

  using electric discharge · CPC title

• B01J2219/0898

  Hot plasma · CPC title

• B01J2219/089

  Liquid-solid · CPC title