Liquid oils without unwanted contaminants

Patent metadata

Field	Value
Publication number	US-12152218-B2
Application number	US-201916966564-A
Country	US
Kind code	B2
Filing date	Feb 7, 2019
Priority date	Feb 7, 2018
Publication date	Nov 26, 2024
Grant date	Nov 26, 2024

Abstract

The present invention relates to a process for preparing purified vegetable liquid oil, and the process is comprising contacting a vegetable liquid oil, which has not been subjected to a deodorization step, with an adsorbent comprising alumina oxide and wherein the adsorbent has a content of alumina oxide of not more than 9.5% and the obtained deodorized vegetable liquid oils.

First claim

The invention claimed is:

1. A process for preparing purified vegetable liquid oil, comprising contacting a vegetable liquid oil, which has not been subjected to a deodorization step, with an adsorbent comprising alumina oxide in an amount of not more than 9.5 wt % based on total adsorbent weight.

2. The process according to claim 1 wherein the adsorbent is non-chemically activated.

3. The process according to claim 1 , wherein the adsorbent has a content of earth alkali oxides of from 12 to 27 wt % based on total adsorbent weight.

4. The process according to claim 1 , wherein the adsorbent has a content of magnesium oxide of from 11 to 25 wt % based on total adsorbent weight.

5. A process for preparing purified vegetable liquid oil, comprising contacting a vegetable liquid oil, which has not been subjected to a deodorization step, with an adsorbent comprising alumina oxide in an amount of not more than 9.5 wt % based on total adsorbent weight, wherein the adsorbent is contacted with the vegetable liquid oil by adding the adsorbent to the vegetable liquid oil in an amount of not more than 1% (w/w) and subsequently removed from the vegetable liquid oil by filtration.

6. The process according to claim 5 , wherein the adsorbent is contacted with the vegetable liquid oil by adding the adsorbent to the vegetable liquid oil in an amount of not more than 0.6% (w/w).

7. The process according to claim 5 , wherein the adsorbent is contacted with the vegetable liquid oil by adding the adsorbent to the vegetable liquid oil in an amount of not more than 0.6% (w/w).

8. The process according to claim 5 , wherein the adsorbent is contacted with the vegetable liquid oil by adding the adsorbent to the vegetable liquid oil in an amount of not more than 0.5% (w/w).

9. The process according to claim 5 , wherein the adsorbent is contacted with the vegetable liquid oil by adding the adsorbent to the vegetable liquid oil in an amount of not more than 0.4% (w/w).

10. The process according to claim 1 , wherein the process comprises a treatment of the vegetable liquid oil in presence of a base.

11. The process according to claim 1 , wherein the process comprises the sequence of the following steps:
a) degumming of the vegetable liquid oil to form a degummed oil,
b) neutralising the degummed oil in presence of alkali to form an alkali treated oil,
c) bleaching the alkali treated oil in presence of an adsorbent comprising alumina oxide in an amount less than 9.5 wt % based on total adsorbent weight and the content of earth alkali metal oxides is from 12 to 27 wt % to provide a bleached oil,
d) deodorizing the bleached oil at a deodorization temperature below 265° ° C. to form a deodorized oil.

12. The process according to claim 11 , further comprising the step of
e) re-bleaching the deodorized oil in presence of an acid-activated bleaching agent to form a re-bleached oil.

13. The process according to claim 12 , further comprising the step of
f) re-deodorizing the re-bleached oil at a deodorization temperature below 200° C.

14. The process according to claim 11 , further comprising the step of
f) re-deodorizing the deodorized oil at a deodorization temperature below 200° C.

15. The process according to claim 1 wherein the adsorbent is contacted with the vegetable liquid oil by adding the adsorbent to the vegetable liquid oil in an amount of not more than 0.3% (w/w).

Assignees

• Cargill Inc

Inventors

• Brüse Falk

Classifications

• A23B20/30

  Preservation of other edible oils or fats, e.g. shortenings or cooking oils · CPC title

• C11B3/001

  by a combination of two or more of the means hereafter · CPC title

• B01J20/08

  comprising aluminium oxide or hydroxide; comprising bauxite · CPC title

• A23V2002/00

  Food compositions, function of food ingredients or processes for food or foodstuffs · CPC title

• A23D9/04

  Working-up · CPC title