Purification process for polyether-carbonate polyols

US12146027B2 · US · B2

Patent metadata
FieldValue
Publication numberUS-12146027-B2
Application numberUS-202017424259-A
CountryUS
Kind codeB2
Filing dateJan 6, 2020
Priority dateJan 31, 2019
Publication dateNov 19, 2024
Grant dateNov 19, 2024

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  1. Title

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  2. Abstract

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  4. Key dates

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  5. First independent claim

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Abstract

Official abstract text for this publication.

Alkylene carbonates are removed from polyether-carbonate polymers by contacting the polyether-carbonate with an absorbent at a temperature of 30 to 150° C. The process is effective and inexpensive. The purified polyether-carbonate is useful for making polyurethanes as well as in many other applications.

First claim

Opening claim text (preview).

What is claimed is: 1. A process for removing an alkylene carbonate from a polyether-carbonate, comprising contacting a starting polyether-carbonate that contains at least 0.25 weight-%, based on the weight of the starting polyether carbonate, of one or more alkylene carbonates, with a solid absorbent that contains pores having an average pore size of at least 1 nm up to 100 nm at a temperature of 30 to 150° C. and at which temperature the starting polyether-carbonate is a liquid, wherein the solid absorbent has a pore volume of 0.25 to 2 mL/g and is selected from the group consisting of an unfunctionalized, crosslinked porous polymer that lacks ion exchange capacity in the form of a particulate solid and a crosslinked porous polymer which which crosslinking porous polymer is is a crosslinked porous anion exchange resin in the form of a particulate solid. 2. The process of claim 1 wherein the starting polyether-carbonate contains 0.5 to 15% by weight of the alkylene carbonate, based on the combined weight of polyether carbonate and alkylene carbonate. 3. The process of claim 1 wherein the alkylene carbonate includes propylene carbonate, ethylene carbonate or both propylene carbonate and ethylene carbonate. 4. The process of claim 1 wherein 40 to 100 weight % of the alkylene carbonate is removed. 5. The process of claim 1 wherein the temperature is 60 to 85° C.

Assignees

Inventors

Classifications

  • C08G64/34Primary

    and cyclic ethers · CPC title

  • Post-polymerisation treatment, e.g. recovery, purification, drying · CPC title

  • and cyclic ethers · CPC title

  • saturated · CPC title

  • Cross-linked polymers · CPC title

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What does patent US12146027B2 cover?
Alkylene carbonates are removed from polyether-carbonate polymers by contacting the polyether-carbonate with an absorbent at a temperature of 30 to 150° C. The process is effective and inexpensive. The purified polyether-carbonate is useful for making polyurethanes as well as in many other applications.
Who is the assignee on this patent?
Dow Global Technologies Llc
What technology area does this patent fall under?
Primary CPC classification C08G64/34. Mapped technology areas include Chemistry & Metallurgy.
When was this patent published?
Publication date Tue Nov 19 2024 00:00:00 GMT+0000 (Coordinated Universal Time) (B2). Legal status and post-grant events are not shown on this page.
What related patents are in patentsdb?
We list 3 related publications on this page (citations in our corpus or others sharing the same primary CPC).