Ferrite powder and method of producing the same

Patent metadata

Field	Value
Publication number	US-12119151-B2
Application number	US-202117795382-A
Country	US
Kind code	B2
Filing date	Jan 27, 2021
Priority date	Jan 27, 2020
Publication date	Oct 15, 2024
Grant date	Oct 15, 2024

Abstract

Provided are a ferrite powder capable of maintaining a high withstand voltage even when used in a resin composition having high magnetic properties and electrical resistivity and a high filling ratio, and a method for producing the same. A ferrite powder composed of spherical ferrite particles, wherein the ferrite powder contains iron (Fe): 55.0-70.0 mass % and manganese (Mn): 3.5-18.5 mass %, the ferrite powder containing more than 0.0 mass % to 7.5 mass % α-Fe 2 O 3 , and the ferrite powder has a volume average particle size (D50) of 15.0 μm or less.

First claim

The invention claimed is:

1. A ferrite powder comprising highly spherical ferrite particles,
wherein the ferrite powder contains 55.0 to 70.0 mass % iron (Fe) and 3.5 to 18.5 mass % manganese (Mn), the ferrite powder containing more than 0.0 mass % to 7.5 mass % α-Fe 2 O 3 ,
wherein the ferrite powder has a volume average particle size (D50) of 15.0 μm or less,
wherein the content of elements other than iron (Fe), manganese (Mn), and oxygen (O) in the ferrite powder is 0.5 mass % or less, and
wherein the ferrite powder has a carbon (C) content of from 0.001 mass % to 0.12 mass %.

2. The ferrite powder according to claim 1 , wherein the α-Fe 2 O 3 is contained in the ferrite powder in an amount of 3.0 mass % to 6.0 mass %.

3. The ferrite powder according to claim 1 , wherein the ferrite powder has a volume average particle size (D50) of 2.0 μm to 15 μm.

4. The ferrite powder according to claim 1 , wherein the ferrite powder has a mean shape factor SF-1 of 100 to 110.

5. The ferrite powder according to claim 1 , wherein the ferrite powder has a volume resistivity of 1.0×10 8 Ω·cm or more.

6. The ferrite powder according to claim 1 , wherein the ferrite powder contains 58.0 to 69.0 mass % iron (Fe) and 6.0 to 10.0 mass % manganese (Mn).

7. The ferrite powder according to claim 1 , wherein the ferrite powder has a volume average particle size (D50) of 2.5 to 7.0 μm.

8. The ferrite powder according to claim 1 , wherein the ferrite powder comprises one or more compounds selected from the group consisting of erucic acid amide (C 22 H 43 NO), butyl palmitate (C 20 H 40 O 2 ) and butyl stearate (C 22 H 44 O 2 ).

9. The ferrite powder according to claim 1 , wherein the α-Fe 2 O 3 is dispersed inside the highly spherical ferrite particles.

10. A process for producing the ferrite powder according to claim 1 , comprising the steps of:
mixing raw materials for ferrite to prepare a raw material mixture;
calcining the raw material mixture to form a calcined product;
pulverizing and granulating the calcined product to prepare a granular product; and
thermally spraying the granular product to produce a thermally sprayed product;
wherein the granular product has a carbon content of 0.001 to 0.095 mass %, and the feed rate of a raw material is 2.5 to 9.0 kg/hour, the flow rate of combustible gas is 3 to 10 m 3 /hour, and the flow rate of oxygen is 18 to 60 m 3 /hour in the step of thermally spraying.

Assignees

• Powdertech Co Ltd

Inventors

• Aga Koji
• Kojima Takashi
• Sugiura Takao
• KUWAHARA Sho
• KONNO Satomi
• Tsuduki Tadashi

Classifications

• C01P2006/80

  Compositional purity · CPC title

• C01P2006/42

  Magnetic properties · CPC title

• C01P2006/40

  Electric properties · CPC title

• C01P2004/61

  Micrometer sized, i.e. from 1-100 micrometer · CPC title

• C01P2004/32

  Spheres · CPC title