Porous ceramic structure for part made of CMC material and method for obtaining same

Patent metadata

Field	Value
Publication number	US-12115486-B2
Application number	US-202017618214-A
Country	US
Kind code	B2
Filing date	Jun 30, 2020
Priority date	Jul 10, 2019
Publication date	Oct 15, 2024
Grant date	Oct 15, 2024

Abstract

A porous ceramic structure intended to form the reinforcement of a ceramic matrix composite component, the structure having a connected porosity delimited by an internal surface which includes a plurality of first points, each first point being associated with a second point aligned with this first point along a normal to the internal surface taken at the first point, the structure being divisible into a plurality of unit volumes of a size less than or equal to 5 mm3 in each of which: a characteristic pore length, corresponding to the maximum of the distance separating each first point from its associated second point, is less than or equal to 0.5 mm; and a porosity ratio is greater than or equal to 50%.

First claim

The invention claimed is:

1. A porous ceramic structure intended to form a reinforcement of a ceramic matrix composite component, the structure having a connected porosity delimited by an internal surface which comprises a plurality of first points each first point being associated with a second point aligned with said first point along a normal to the internal surface taken at the first point, the structure being divisible into a plurality of unit volumes of a size less than or equal to 5 mm 3 in each of which:
a characteristic pore length, corresponding to a maximum of the distance separating each first point from its associated second point, is less than or equal to 0.5 mm; and
a porosity ratio is greater than or equal to 50%; and
comprising a plurality of interconnected structural elements which define the connected porosity, wherein in each unit volume a surface bridging ratio corresponding to a ratio between the sum of the surfaces connecting two structural elements to each other and the sum of the surfaces not connecting two structural elements to each other is less than or equal to 15%,
wherein the structural elements are beams, and
wherein the beams are oriented in four directions given by the diagonals of a cube.

2. The structure as claimed in claim 1 , wherein the structure is sintered.

3. The structure as claimed in claim 1 , wherein each unit volume has a size less than or equal to 1 mm 3 .

4. The structure as claimed in claim 1 , wherein the characteristic length is less than or equal to 0.2 mm.

5. The structure as claimed in claim 1 , wherein the porosity ratio of each unit volume is comprised between 60% and 80%.

6. The structure as claimed in claim 1 , wherein a standard deviation of a distribution of characteristic lengths of the unit volumes in the structure is less than 10% of a mean value of the distribution of characteristic lengths in the structure, and a standard deviation of a distribution of porosity ratios of unit volumes in the structure is less than 10% of a mean value of the distribution of porosity ratios in the structure.

7. A process for manufacturing a porous structure as claimed in claim 1 , comprising manufacturing the structure by additive manufacturing.

8. A process for manufacturing a ceramic matrix composite component comprising a matrix-densified porous reinforcement, the process comprising manufacturing a porous structure by a process as claimed in claim 7 and forming a ceramic matrix in the porosity of the porous structure.

9. The process as claimed in claim 8 , wherein the formation of the ceramic matrix is achieved by chemical vapor infiltration.

10. The process as claimed in claim 8 , wherein the porous structure comprises silicon carbide, and the formation of the ceramic matrix comprises introducing a carbon powder and/or a silicon carbide powder into the porosity of the porous structure, and then infiltrating the porosity of the porous structure with silicon or a molten silicon compound.

11. The process as claimed in claim 8 , wherein the formation of the ceramic matrix is achieved by injecting a matrix precursor polymer into the porosity of the porous structure and pyrolysis heat treatment to convert the precursor to the matrix.

Assignees

• Safran Ceram

Inventors

• Lacombe Benjamin
• Garnier Gildas

Classifications

• C04B2235/52

  Constituents or additives characterised by their shapes · CPC title

• C04B2235/422

  Carbon · CPC title

• C04B2235/3826

  Silicon carbides · CPC title

• C04B38/0074

  expressed as porosity percentage · CPC title

• C04B38/0051

  characterised by the pore size, pore shape or kind of porosity · CPC title