Pellet production method

Patent metadata

Field	Value
Publication number	US-12109732-B2
Application number	US-202017622411-A
Country	US
Kind code	B2
Filing date	Jun 2, 2020
Priority date	Jun 27, 2019
Publication date	Oct 8, 2024
Grant date	Oct 8, 2024

Abstract

A pellet production method comprising: an operation in which a strand comprising a glass-fiber-reinforced polyamide resin composition containing 50 mass % to 80 mass % of glass fiber is extruded from an orifice at a die; an operation in which the strand is drawn into water within a tank and is cooled; and an operation in which the cooled strand is cut to obtain a pellet; wherein an angle of incidence at which the strand enters the water within the tank is not less than 70° but is less than 90°; and wherein a ratio of a diameter of the pellet to a diameter of the orifice (diameter of the pellet/diameter of the orifice) is 0.65 to 0.97.

First claim

The invention claimed is:

1. A pellet production method comprising:
an operation in which a strand comprising a glass-fiber-reinforced polyamide resin composition containing 50 mass % to 80 mass % of glass fiber is extruded from an orifice at a die;
an operation in which the strand is drawn into water within a tank and is cooled; and
an operation in which the cooled strand is cut to obtain a pellet;
wherein an angle of incidence at which the strand enters the water within the tank is not less than 70° but is less than 90°; and
wherein a ratio of a diameter of the pellet to a diameter of the orifice (diameter of the pellet/diameter of the orifice) is 0.65 to 0.97.

2. The pellet production method according to claim 1 wherein
at least one first guide roller for guiding the strand within the tank is provided within the tank; and
an angle made by portions of the strand that are ahead of and behind that first guide roller which is in an upstreammost location is not less than 90°.

3. The pellet production method according to claim 2 wherein the angle made by the portions of the strand that are ahead of and behind that first guide roller which is in the upstreammost location is not greater than 179°.

4. The pellet production method according to claim 2 wherein there is only one of the at least one first guide roller provided within the tank.

5. The pellet production method according to claim 2 wherein the angle made by the portions of the strand that are ahead of and behind that first guide roller which is in the upstreammost location is not greater than 120°.

6. The pellet production method according to claim 1 wherein the operation in which the strand is cooled comprises an operation in which the strand that was water-cooled within the tank is air-cooled.

7. The pellet production method according to claim 6 wherein
at least one second guide roller for causing the strand that was water-cooled within the tank to be guided through air is provided; and
an angle made by portions of the strand that are ahead of and behind that second guide roller which is in an upstreammost location is not less than 140°.

8. The pellet production method according to claim 1 wherein
the operation in which the strand is cooled comprises an operation in which the strand that was water-cooled within the tank is air-cooled;
at least one first guide roller for guiding the strand within the tank is provided within the tank;
at least one second guide roller for causing the strand that was water-cooled within the tank to be guided through air is provided; and
an angle made by portions of the strand that are ahead of and behind that second guide roller which is in an upstreammost location is greater than an angle made by portions of the strand that are ahead of and behind that first guide roller which is in an upstreammost location.

9. The pellet production method according to claim 1 wherein a standard deviation of an aspect ratio of the pellet is not greater than 0.20.

10. The pellet production method according to claim 1 wherein polyamide resin is present within 100 mass % of the glass-fiber-reinforced polyamide resin composition in an amount that is not less than 20 mass %.

11. The pellet production method according to claim 1 wherein average glass surface area per unit fiber as calculated based on residual glass fiber length at the pellet is not less than 1.1 times critical glass surface area.

12. The pellet production method according to claim 1 wherein polyamide resin comprised by the glass-fiber-reinforced polyamide resin composition comprises an aliphatic polyamide and a polyamide having an aromatic component.

13. The pellet production method according to claim 12 wherein the polyamide having the aromatic component comprises poly-meta-xylene adipamide for which concentration of terminal carboxy groups is not greater than 50 meq/kg and for which relative viscosity in 96% sulfuric acid solution is 1.4 to 1.8.

14. The pellet production method according to claim 12 wherein the aliphatic polyamide comprises polycaproamide for which concentration of terminal carboxy groups is 55 meq/kg to 95 meq/kg and for which relative viscosity in 96% sulfuric acid solution is 1.4 to 2.0.

15. The pellet production method according to claim 1 wherein the glass fiber comprises at least either glass fiber of circular cross-section of diameter not greater than 7 μm or glass fiber of flattened cross-section.

16. The pellet production method according to claim 1 wherein an extruder is used to extrude the strand.

17. The pellet production method according to claim 1 wherein, at the operation in which the strand is extruded, the strand is extruded in air.

Assignees

• Toyo Boseki
• Toyobo Mc Corp

Inventors

• Kon Sakito
• Ayuzawa Yoshitaka

Classifications

• B29B13/045

  of powders or pellets · CPC title

• B29B9/14

  fibre-reinforced · CPC title

• C08K7/14

  Glass · CPC title

• B29C48/04

  Particle-shaped (making granules B29B9/00) · CPC title

• B29C48/919

  using a bath, e.g. extruding into an open bath to coagulate or cool the material · CPC title