Vanadium oxide-doped laser-induced graphene multi-parameter sensor to decouple soil nitrogen loss and temperature
US-2024393305-A1 · Nov 28, 2024 · US
US12092602B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-12092602-B2 |
| Application number | US-202117206935-A |
| Country | US |
| Kind code | B2 |
| Filing date | Mar 19, 2021 |
| Priority date | Mar 20, 2020 |
| Publication date | Sep 17, 2024 |
| Grant date | Sep 17, 2024 |
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An electrode includes an electrically conductive substrate with a coating containing boron-doped diamond (BDD) nanoparticles. Fabricating the electrode can include dispersing BDD nanoparticles in a solvent to yield a suspension, coating a conductive substrate with the suspension, and drying the suspension to yield the electrode. In some cases, fabricating the electrode includes combining BDD nanoparticles with a polymeric resin precursor to yield a mixture including a metal oxide, coating a conductive substrate with the mixture to yield a coated substrate, and calcining the coated substrate to yield a metal oxide coating including BDD nanoparticles. In certain cases, fabricating the electrode includes combining powdered activated carbon with polymeric linkers to yield a polymeric precursor solution, combining BDD nanoparticles with the polymeric precursor solution to yield a mixture, coating a conductive substrate with the mixture to yield a coated substrate, and crosslinking the polymeric linkers to yield the electrode.
Opening claim text (preview).
What is claimed is: 1. An electrode comprising: an electrically conductive substrate; and a coating on the electrically conductive substrate, wherein the coating comprises a polymer, powdered activated carbon, and boron-doped diamond nanoparticles comprising between about 10 and about 80,000 ppm boron. 2. The electrode of claim 1 , wherein the boron-doped diamond nanoparticles have a diameter in a range between about 10 nm and about 200 nm. 3. The electrode of claim 2 , wherein the boron-doped diamond nanoparticles have a diameter in a range between about 50 nm and about 60 nm. 4. The electrode of claim 1 , wherein a thickness of the coating is in a range between one nanoparticle and five nanoparticles. 5. The electrode of claim 1 , wherein the polymer further comprises polypyrrole. 6. The electrode of claim 1 , wherein the polymer comprises polyaniline. 7. The electrode of claim 1 , wherein the polymer comprises polyphenylene vinylene. 8. The electrode of claim 1 , wherein the polymer comprises polyvinyl alcohol. 9. The electrode of claim 8 , wherein the polymer further comprises glutaraldehyde linkers.
Electrodes · CPC title
Diamond coating · CPC title
Water · CPC title
at least partially made of carbon · CPC title
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