Piston system and high pressure homogenizer using the piston system

Patent metadata

Field	Value
Publication number	US-12084532-B2
Application number	US-202217879941-A
Country	US
Kind code	B2
Filing date	Aug 3, 2022
Priority date	Nov 7, 2017
Publication date	Sep 10, 2024
Grant date	Sep 10, 2024

Abstract

The invention relates to a piston system ( 1 ) for use in a homogenizer, comprising a piston ( 2 ) that is configured and arranged to make a reciprocating movement in use of the piston system, a cylinder ( 3 ) that is configured and arranged to receive and guide at least a first part of the piston, a first supply channel ( 8 ) that is configured and arranged to supply a lubricating medium ( 9 ) to a portion ( 10 ) of the first part of the piston that in use is arranged inside the cylinder, and a second supply channel ( 13 ) that is configured and arranged to, in use, supply a cooling medium ( 14 ) to a second part of the piston outside the cylinder. Also disclosed is a process for the production of an elastomer agglomerate composition forcing a slurry comprising elastomeric particles through an aperture to obtain the elastomer agglomerate composition using the piston system.

First claim

What is claimed is:

1. A piston system for use in a homogenizer, comprising:
a piston that is configured and arranged to make a reciprocating movement in use of the piston system,
a cylinder that is configured and arranged to receive and guide at least a first part of the piston,
a first supply channel that is configured and arranged to supply a lubricating medium to a portion of the first part of the piston that, in use, is arranged inside the cylinder, and
a second supply channel that is configured and arranged to, in use, supply a cooling medium to a second part of the piston while the second part of the piston is outside the cylinder,
wherein the cooling medium comprise water.

2. The piston system of claim 1 , further comprising a chamber in communication with a third part of the piston, wherein the piston is configured to force a slurry out of an aperture of the chamber.

3. The piston system of claim 1 , further comprising a supply configured and arranged to supply elastomeric particles to a chamber of the piston system in communication with a third part of the piston, wherein, in use, movement of the piston into the chamber forces the slurry out of an aperture of the chamber.

4. The piston system of claim 3 , wherein the elastomeric particles are selected from the group consisting of polybutadiene particles, poly(styrene butadiene) particles, poly(acrylonitrile butadiene) particles and polybutylacrylate particles and combinations thereof.

5. The piston system of claim 4 , wherein the elastomeric particles comprise polybutadiene particles.

6. The piston system of claim 3 , wherein the slurry comprises at least 20 wt % of elastomeric particles, based upon a total weight of the slurry.

7. The piston system of claim 6 , wherein the slurry comprises at least 30 wt % and at most 50 wt % of elastomeric particles, based upon a total weight of the slurry.

8. The piston system of claim 3 , wherein the elastomeric particles have an average particle size of at most 150 nm, wherein the average particle size, D50, is determined in accordance with ISO 9276-2:2014.

9. The piston system of claim 8 , wherein the elastomeric particles have an average particle size of 80 to 120 nm, wherein the average particle size, D50, is determined in accordance with ISO 9276-2:2014.

10. The piston system of claim 1 , wherein the first supply channel comprises at least two inlet branches and wherein a first inlet branch of the at least two inlet branches is connected with a first lubricant supply system that is configured and arranged to enable manual supply of the lubricating medium.

11. The piston system of claim 10 , wherein a second inlet branch of the at least two inlet branches is connected with a second lubricant supply system that is configured and arranged to enable automatic supply of the lubricating medium.

12. The piston system of claim 1 , wherein the lubricating medium comprises grease.

13. The piston system of claim 1 , wherein the cooling medium is not part of a closed system.

14. The piston system of claim 1 , wherein the lubricating medium is grease.

15. The piston system of claim 1 , wherein both the lubricating medium and cooling medium comprise water.

16. A high-pressure homogenizer comprising at least one piston system of claim 1 .

17. A process for increasing a particle size of elastomeric particles, the process comprising:
providing a slurry comprising the elastomeric particles in water; and
forcing the slurry through an aperture in a piston system to obtain the elastomer agglomerate composition,
wherein the piston system comprises:
a piston that is configured and arranged to make a reciprocating movement in use of the piston system,
a cylinder that is configured and arranged to receive and guide at least a first part of the piston,
a first supply channel that is configured and arranged to supply a lubricating medium to a portion of the first part of the piston that, in use, is arranged inside the cylinder, and
a second supply channel that is configured and arranged to, in use, supply a cooling medium to a second part of the piston while the second part of the piston is outside the cylinder.

18. The process according to claim 17 , wherein the elastomeric particles have an average particle size D50 as determined in accordance with ISO 9276-2:2014, and wherein the elastomer agglomerate composition has agglomerates having a larger average particle size than the elastomeric particles average particle size.

Assignees

• Sabic Global Technologies Bv

Inventors

• Ferraris Dane M
• Legg Richard
• Youssef Ahmed Abouelfetouh
• Lowry Vern

Classifications

• F04B53/162

  Adaptations of cylinders · CPC title

• B01F25/4512

  with reciprocating pistons · CPC title

• B01F2101/2805

  Mixing plastics, polymer material ingredients, monomers or oligomers · CPC title

• B01F25/44

  Mixers in which the components are pressed through slits · CPC title

• F04B53/18

  Lubricating · CPC title