Apparatus and method for particulate capture from gas streams and a method of removing soluble particulate from a gas

Patent metadata

Field	Value
Publication number	US-12083468-B2
Application number	US-202217684716-A
Country	US
Kind code	B2
Filing date	Mar 2, 2022
Priority date	Nov 15, 2013
Publication date	Sep 10, 2024
Grant date	Sep 10, 2024

Abstract

Disclosed is a method for the removal of soluble particulate matter from a gas stream, such as urea dust from the off-gas of a finishing section of a urea production plant. The method comprises subjecting the off-gas to at least two quenching stages an aqueous quenching liquid. The quenching liquid used in a first, upstream quench stage, is allowed to have a higher concentration of dissolved particulate matter than the quenching liquid in the second, downstream quench stage. The quenched gas is led through a particle capture zone, typically comprising one or more of a wet scrubber, a Venturi scrubber, and a wet electrostatic precipitator.

First claim

The invention claimed is:

1. A particle capture system comprising, in series, a gas inlet, a first quenching zone, a particle capture zone, and a gas outlet, the first quenching zone comprising a liquid inlet for the distribution of a first quenching liquid, downstream thereof a gas flow-line to the particle capture zone, and a liquid outlet for the first quenching liquid, said liquid inlet and liquid outlet forming part of a first recirculation loop comprising an upstream reservoir for the first quenching liquid, wherein downstream of the first quenching zone, and upstream of the gas outlet of the particle capture zone, at least a second quenching zone is provided, said second quenching zone having a liquid inlet and a liquid outlet for a second quenching liquid, wherein the liquid inlet and liquid outlet of the second quenching zone form part of a second recirculation loop comprising a second reservoir, wherein the second recirculation loop can be operated independently of said first recirculation loop, the term downstream being defined with reference to the flowing direction of a gas stream from the gas outlet, and wherein the particle capture zone comprises a Venturi scrubber.

2. A finishing equipment for a urea plant, said finishing equipment comprising a urea finishing device comprising an inlet for liquid urea, an inlet for cooling gas, a collector for solid urea, an outlet for off-gas and at least one particle capture system, wherein the particle capture system is the system of claim 1 , said outlet for off-gas being in fluid communication with the gas inlet of the particle capture device.

3. The finishing equipment of claim 2 , wherein the urea finishing device is a fluid bed granulation unit.

4. The finishing equipment of claim 2 , further comprising an acid scrubber for the removal of ammonia.

5. The finishing equipment of claim 2 , wherein the particle capture system comprises one or more Venturi scrubbers comprising a plurality of parallel Venturi tubes each comprising a throat, the one or more Venturi scrubbers further comprising a plurality of single phase nozzles disposed to spray liquid in the throats of the Venturi tubes co-current with the gas stream.

6. A urea plant comprising a synthesis and recovery section; said section being in fluid connection with an evaporation section, said evaporation section being in fluid communication with a finishing section and having a gas flow line to a condensation section; and said finishing section having a gas flow line to a dust scrubbing section, wherein the finishing section comprises the finishing equipment of claim 2 .

7. A method of modifying an existing urea plant, said existing plant comprising a synthesis and recovery section; said section being in fluid communication with an evaporation section, said evaporation section being in fluid communication with a finishing section and having a gas flow line to a condensation section; said finishing section having a gas flow line to a dust scrubbing section, wherein the method comprises installing a first quenching system between the finishing section and the dust scrubbing section, said quenching system being in fluid communication with the gas flow line between the finishing section and the dust scrubbing section, and installing at least one second quenching system downstream of the first quenching system, wherein the first and second quenching systems each comprises a reservoir and each forms part of a recirculation loop that can be operated independently of the other, the term downstream being defined with reference to the intended flowing direction of a gas stream from the finishing section to the dust scrubbing section, and wherein the second quenching system comprises a Venturi scrubber.

Assignees

• Stamicarbon

Inventors

• Higgins Brian Sayre

Classifications

• B03C3/013

  Conditioning by chemical additives, e.g. with SO3 · CPC title

• B01D47/05

  by condensation of the separating agent · CPC title

• B01D2251/506

  Sulfuric acid · CPC title

• B01D53/58

  Ammonia · CPC title

• B01D2252/103

  Water · CPC title