Apparatus and method for granulating low viscosity materials

Patent metadata

Field	Value
Publication number	US-12070876-B2
Application number	US-201917272338-A
Country	US
Kind code	B2
Filing date	Aug 27, 2019
Priority date	Aug 30, 2018
Publication date	Aug 27, 2024
Grant date	Aug 27, 2024

Abstract

An apparatus to batch or continuously form solid polymer particles, the apparatus comprising the following components: A) at least one pastillation unit comprising a pastillation head, said unit used to form discrete molten polymer particles from a polymer melt; B) a moving belt to receive and transfer the discrete molten polymer particles from the pastillation head; C) a means to transfer water onto the moving belt, such that the water comes into contact with the discrete molten polymer particles on the moving belt to form the solid polymer particles; and wherein the water of component C is sprayed onto the discrete molten polymer particles, such that the ratio of “the rate of water spray” to “the discharge rate” is ≥3.0; and wherein the belt residence time is ≤50 seconds.

First claim

What is claimed is:

1. A process to form solid polymer particles from a polymer melt, said process comprising pastillating the polymer melt using an apparatus to batch or continuously form solid polymer particles, the apparatus comprising the following components:
A) at least one pastillation unit comprising a pastillation head, said unit used to form discrete molten polymer particles from a polymer melt comprising ≥95 wt % of an olefin-based with a melt viscosity (177° C.) from 50 cP to 20,000 cP;
B) a moving belt to receive and transfer the discrete molten polymer particles from the pastillation head;
C) a means to transfer water over the moving belt, such that the water comes into contact with the discrete molten polymer particles on the moving belt at a rate of water spray to form the solid polymer particles at a discharge rate with a belt residence time of ≤50 seconds; and
wherein the water of component C is sprayed onto the discrete molten polymer particles, such that the ratio of the rate of water spray to the discharge rate is ≥3.0.

2. The process of claim 1 , wherein the specific capacity of the pastillation unit of ≥12 lbs/hr/ft 2 .

3. The process of claim 1 , wherein the temperature of the polymer melt at the pastillation head is from 80° C. to 275° C.

4. The process of claim 1 , wherein the olefin based polymer has a number average molecular weight from 500 g/mole to 50,000 g/mole.

5. The process of claim 1 , wherein the olefin based polymer has a density of 0.860 g/cc to 0.960 g/cc.

6. The process of claim 1 , wherein the olefin-based polymer has a molecular weight distribution (MWD) from 1.8 to 4.0.

7. The process of claim 1 , wherein the olefin-based polymer is a propylene-based polymer.

8. The process of claim 7 , wherein the propylene-based polymer is a propylene/alpha-olefin interpolymer.

9. The process of claim 7 , wherein the propylene-based polymer is a propylene/ethylene interpolymer.

10. The process of claim 1 , wherein the olefin-based polymer is an ethylene-based polymer.

11. The process of claim 10 , wherein the ethylene-based polymer is an ethylene/alpha-olefin interpolymer.

Assignees

• Dow Global Technologies Llc

Inventors

• Bawiskar Santosh S
• Zogg Jr Michael J
• Li Guang Ming
• Jin Yi
• Schilhab Lonnie

Classifications

• C08J3/12

  Powdering or granulating · CPC title

• C08F210/16

  Copolymers of ethene with alpha-alkenes, e.g. EP rubbers · CPC title

• B29K2995/0088

  Molecular weight · CPC title

• B29K2995/0063

  Density · CPC title

• B29K2023/12

  PP, i.e. polypropylene · CPC title