Method for producing a composite element

Patent metadata

Field	Value
Publication number	US-12064839-B2
Application number	US-202016893458-A
Country	US
Kind code	B2
Filing date	Jun 5, 2020
Priority date	Jun 5, 2019
Publication date	Aug 20, 2024
Grant date	Aug 20, 2024

Abstract

A method for producing a composite element is provided. The method includes providing an outer frame comprising metal and having a first coefficient of thermal expansion in a first spatial direction and a second coefficient of thermal expansion in a second spatial direction, the first and second coefficient of thermal expansions differing from one another; providing an inner component comprising glass; heating the outer frame to an expanded state having the outer frame expanded with respect to the inner component in the first spatial direction in accordance with the first coefficient of thermal expansion and expanded along the second spatial direction in accordance with the second coefficient of thermal expansion; inserting the inner component in the outer frame when in the expanded state; and cooling the outer frame so that the outer frame contracts from the expanded state until the inner component is fitted in outer frame under compressive stress.

First claim

What is claimed is:

1. A method for producing a composite element, comprising
providing structural parts consisting of an outer frame and an inner component;
wherein the outer frame comprises metal and has a first coefficient of thermal expansion in a first spatial direction and a second coefficient of thermal expansion in a second spatial direction, the first and second coefficient of thermal expansions differing from one another;
wherein the inner component comprises a material selected from a group consisting of glass, quartz, sapphire, glass ceramic, ceramic, laser glass, and crystal;

heating the outer frame to an expanded state to have the outer frame expanded with respect to the inner component in the first spatial direction in accordance with the first coefficient of thermal expansion and expanded along the second spatial direction in accordance with the second coefficient of thermal expansion;
inserting the inner component in the outer frame when in the expanded state; and
cooling the outer frame so that the outer frame contracts from the expanded state until the inner component is fitted in outer frame under compressive stress.

2. The method of claim 1 , wherein the inner component is fitted in the outer frame under a first compressive stress along the first spatial direction and a second compressive stress along the second spatial direction, and wherein the first and second compressive stresses differ from one another.

3. The method of claim 1 , further comprising bringing about a phase transition in the metal of the outer frame from one crystal phase to a different crystal phase.

4. The method of claim 3 , further comprising changing the first and/or second coefficient of thermal expansion to a predefined value.

5. The method of claim 4 , wherein the first coefficient of thermal expansion is changed to a predefined value between −142·10 −6 K −1 and +181·10 6 K −1 , and/or
wherein the second coefficient of thermal expansion is changed to a predefined value between −11·10 6 K −1 and +24·10 −6 K −1 .

6. The method of claim 1 , wherein the metal of the outer frame comprises titanium-niobium alloy having a weight percent of niobium that lies between 10% and 25%.

7. The method of claim 6 , further comprising causing the titanium-niobium alloy to undergo a phase transition so that, in the titanium-niobium alloy, an α phase, a β phase, or an ω phase; or an α phase and a β phase, an α phase and an ω phase or a β phase and an ω phase; or an α phase and a β phase and an ω phase is or are formed.

8. The method of claim 7 , wherein the heating step comprises heating the outer frame at a condition selected from a group consisting of: heating with a heating rate of 0.01° C/s to 1° C/s, heating with a heating rate of 0.1° C/s to 0.3° C/s, heating with a heating rate of 0.18° C/s, heating at a temperature between 700 and 950 ° C., heating at a maximum temperature of 760° C., heating for a holding time of 0.1 to 10 hours, heating for a holding time of 0.5 to 4.75 hours, and any combinations thereof.

9. The method of claim 1 , wherein the inner component is transparent, and wherein the inner component comprises a transparent ceramic comprising yttrium-doped zirconium dioxide.

10. The method of claim 1 , wherein the inner component comprises further comprises a coating comprising Y 2 O 3 .

11. The method of claim 1 , wherein the inner component has a compressive stress tolerance that is less than 585 MPa.

12. The method of claim 1 , wherein the inner component has a compressive stress tolerance that is less than 8 MPa.

13. The method of claim 1 , wherein the inner component has a cross sectional shape that is non-circular and is a shape selected from a group consisting of oval, polygonal, and rounded polygonal.

14. The method of claim 1 , wherein the inner component has at least convex surface or concave surface that protrudes out of the outer frame.

15. The method of claim 1 , further comprising a conductor feedthrough arranged in the inner component.

16. The method of claim 1 , wherein the outer frame has a third coefficient of thermal expansion for a third spatial direction, wherein the third spatial direction is different from the first and second spatial directions, and wherein the third coefficient of thermal expansion has a value of less than 1·10 −6 K −1 .

17. The method of claim 16 , wherein the third coefficient of thermal expansion is configured so that shear stresses on the inner component are minimized or prevented along the third spatial direction.

18. The method of claim 1 , wherein the outer frame is produced by an additive manufacturing method.

19. A composite element produced according to the method of claim 1 .

Assignees

• Schott Ag

Inventors

• Ott Christian

Classifications

• Y10T29/49155

  Manufacturing circuit on or in base · CPC title

• H01B19/00 Primary

  Apparatus or processes specially adapted for manufacturing insulators or insulating bodies {(manufacture of porcelain for electric insulation C04B33/26)} · CPC title

• H01B17/26

  Lead-in insulators; Lead-through insulators · CPC title

• B23P11/025

  by using heat or cold · CPC title

• F16B2200/97

  having differing thermal expansion coefficients · CPC title