Apparatus and method for preparing aerogel blanket

Patent metadata

Field	Value
Publication number	US-12053753-B2
Application number	US-202017416619-A
Country	US
Kind code	B2
Filing date	Jun 10, 2020
Priority date	Sep 3, 2019
Publication date	Aug 6, 2024
Grant date	Aug 6, 2024

Abstract

Provided is an apparatus for preparing an aerogel blanket, the apparatus comprising: a bobbin around which a blanket is wound; a body provided with a gelling tank in which the bobbin is accommodated; a driving member configured to allow the bobbin accommodated in the gelling tank to rotate; and a silica sol supply member configured to gelate the blanket as silica sol is injected into the gelling tank to impregnate the blanket rotating by the bobbin.

First claim

The invention claimed is:

1. An apparatus for preparing an aerogel blanket, the apparatus comprising:
a bobbin around which a blanket is wound;
a main body provided with a gelling tank enclosing a gelling chamber inside the gelling tank in which the bobbin is accommodated, the gelling tank having a U-shaped cross-sectional shape of which an upper portion is covered by a cover that can be opened, a lower portion having a curvature corresponding to the blanket wound around the bobbin, and having a first wall and an opposite second wall;
a driving member configured to transmit power to the bobbin accommodated in the gelling tank to rotate the bobbin; and
a silica sol supply tank in which a precursor solution and a catalyst solution are mixed to prepare a silica sol, the silica sol supply tank connected to the gelling tank to deliver the silica sol into the gelling tank via an inflow inlet at an upper end of the gelling tank to the blanket and lower portion of the gelling tank to impregnate the blanket rotating by the bobbin,
wherein the bobbin comprises:
a winding rod around which the blanket is wound in a roll shape; and
a support plate coupled to each end of the winding rod to support a side portion of the blanket wound around the winding rod, each support plate comprising a plurality of opening holes through which the silica sol delivered to the gelling tank can be introduced into the side portion of the blanket wound around the winding rod,
wherein the winding rod comprises:
an inner portion comprising a hollow;
a plurality of connection holes in an outer circumferential surface of the winding rod and connected to the hollow through which the silica sol injected into the gelling tank is introduced into the hollow; and
an outer portion comprising a plurality of connection holes, through which the silica sol introduced into the hollow is discharged to the outside of the winding rod so as to impregnate the inside of the blanket wound around the winding rod.

2. The apparatus of claim 1 , wherein the gelling tank further comprises a discharge outlet provided at an outer lower end of the gelling tank.

3. The apparatus of claim 1 , wherein the gelling tank further comprises a first rotator provided on the first wall and a second rotator provided on the second wall of the gelling tank, and the first rotator is coupled to one end of the bobbin and the second rotator is coupled to the other end of the bobbin so that the bobbin is rotatably installed in the gelling chamber.

4. The apparatus of claim 3 , wherein a coupling groove is defined in each of both ends of the bobbin, and a coupling protrusion is disposed on each of the first and second rotators, and
the bobbin and the first and second rotators are interlocked with each other to rotate by coupling of the coupling groove and the coupling protrusion.

5. The apparatus of claim 3 , wherein the driving member transmits power to the first rotator to allow the bobbin to be rotated.

6. The apparatus of claim 3 , wherein the gelling tank further comprises a rotation handle coupled to the second rotator to allow the bobbin to be manually rotated.

7. A method for preparing an aerogel blanket, the method using the apparatus of claim 6 and comprising:
winding a blanket around the bobbin of the apparatus as a winding step (S 10 );
rotatably installing the bobbin around which the blanket is wound inside the gelling tank of the apparatus, as an accommodation step (S 20 );
injecting a precursor solution and a catalyst solution into the silica sol supply tank of the apparatus to mix the precursor solution and the catalyst solution with each other, thereby preparing a silica sol, as a silica sol preparation step (S 30 );
rotating the bobbin, around which the blanket is wound, via the driving member of the apparatus within the gelling tank of the apparatus, as a rotation step (S 40 ); and
injecting the silica sol mixed in the silica sol supply tank of the apparatus into the gelling tank of the apparatus to impregnate the silica sol into the blanket rotating by the bobbin, thereby gelating the blanket, as a gelation step (S 50 ).

8. The method of claim 7 , further comprising, after the gelation step (S 50 ), collecting the silica sol remaining in the gelling tank of the apparatus, as a collection step (S 60 ).

9. The method of claim 8 , further comprising, after the collection step (S 60 ), injecting an aging solution into the gelling tank of the apparatus to age the blanket rotating by the bobbin of the apparatus, and collecting the aging solution remaining in the gelling tank of the apparatus when the aging of the blanket is completed, as an aging step (S 70 ).

10. The method of claim 9 , further comprising, after the aging step (S 70 ), injecting a surface modifying solution into the gelling tank of the apparatus to modify a surface of the blanket rotating by the bobbin of the apparatus, and collecting the surface modifying solution remaining in the gelling tank of the apparatus when the surface modification of the blanket is completed, as a surface modifying step (S 80 ).

11. The method of claim 10 , further comprising, after the surface modifying step (S 80 ), drying the blanket to complete the aerogel blanket.

12. The method of claim 7 , wherein, in the accommodation step (S 20 ), rotatably installing the bobbin of the apparatus around which the blanket is wound in the gelling chamber of the gelling tank of the apparatus comprises coupling one end of the bobbin to the first rotator provided on the first wall of the gelling tank of the apparatus and coupling the other end of the bobbin to the second rotator provided on the second wall of the gelling tank of the apparatus.

Assignees

• Lg Chemical Ltd

Inventors

• Kang Tae Gyeong
• Kim Bong June
• Baek Se Won

Classifications

• B28B21/46

  by dipping · CPC title

• B28B1/525

  containing organic fibres, e.g. wood fibres (B28B1/526, B28B1/527 take precedence) · CPC title

• B28B1/52

  specially adapted for producing articles from mixtures containing fibres, {e.g. asbestos cement}(by wrapping on to mandrels B28B1/42) · CPC title

• C01B33/1585 Primary

  Dehydration into aerogels · CPC title

• C01B33/155

  Preparation of hydroorganogels or organogels · CPC title