Powder containing carboxymethylated cellulose nanofibers

US12049522B2 · US · B2

Patent metadata
FieldValue
Publication numberUS-12049522-B2
Application numberUS-201917058207-A
CountryUS
Kind codeB2
Filing dateMay 28, 2019
Priority dateMay 29, 2018
Publication dateJul 30, 2024
Grant dateJul 30, 2024

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  1. Title

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  2. Abstract

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  3. Assignees and inventors

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  4. Key dates

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  5. First independent claim

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  6. CPC / IPC classifications

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  7. Citations and related patents

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Abstract

Official abstract text for this publication.

A powder that contains carboxymethylated cellulose nanofibers, said carboxymethylated cellulose nanofibers having a degree of carboxymethyl substitution of 0.50 or less and a cellulose type I crystallinity of 60% or more, and has a median diameter of 10.0 μm to 150.0 μm. This powder is suitable usable as an additive.

First claim

Opening claim text (preview).

The invention claimed is: 1. A powder comprising carboxymethylated cellulose nanofibers, wherein the powder has a median diameter of from 10.0 μm to 150.0 μm, wherein the carboxymethylated cellulose nanofibers have a degree of carboxymethyl substitution of 0.50 or less and a degree of crystallization of cellulose I type of 60% or more and wherein the carboxymethylated cellulose nanofibers exhibit a transmittance to light at a wavelength of 660 nm of 70% or more when the carboxymethylated cellulose nanofibers are dispersed in water to form a water dispersion having a solid content of 1% (w/v). 2. The powder according to claim 1 , wherein the powder has an angle of repose in the range from 30.0° to 60.0°. 3. The powder according to claim 2 , comprising the carboxymethylated cellulose nanofibers and 5% by mass to 300% by mass of a water-soluble polymer based on an absolute dry mass of the carboxymethylated cellulose nanofibers. 4. The powder according to claim 3 , wherein the carboxymethylated cellulose nanofibers are produced by mercerizing a cellulose in a solvent containing mainly water to produce a mercerized cellulose, then carboxymethylating the mercerized cellulose in a mixed solvent of water and an organic solvent to produce a carboxymethylated cellulose, and then defibrating the carboxymethylated cellulose to provide the carboxymethylated cellulose nanofibers. 5. The powder according to claim 4 , wherein the solvent containing mainly water is a solvent containing more than 50% by mass of water. 6. The powder according to claim 5 , wherein the carboxymethylated cellulose nanofibers have an average fiber diameter of from 3 nm to 500 nm. 7. The powder according to claim 1 , comprising the carboxymethylated cellulose nanofibers and 5% by mass to 300% by mass of a water-soluble polymer based on an absolute dry mass of the carboxymethylated cellulose nanofibers. 8. The powder according to claim 1 , wherein the carboxymethylated cellulose nanofibers are produced by mercerizing a cellulose in a solvent containing mainly water to produce a mercerized cellulose, then carboxymethylating the mercerized cellulose in a mixed solvent of water and an organic solvent to produce a carboxymethylated cellulose, and then defibrating the carboxymethylated cellulose to provide the carboxymethylated cellulose nanofibers. 9. The powder according to claim 8 , wherein the solvent containing mainly water is a solvent containing more than 50% by mass of water. 10. The powder according to claim 1 , wherein the carboxymethylated cellulose nanofibers have an average fiber diameter of from 3 nm to 500 nm. 11. The powder according to claim 1 , wherein the water dispersion has a transmittance to light at 660 nm of 80% or more. 12. The powder according to claim 1 , wherein the water dispersion has a transmittance to light at 660 nm of 90% or more.

Assignees

Inventors

Classifications

  • C08L1/286Primary

    substituted with acid radicals, e.g. carboxymethyl cellulose [CMC] (C08L1/282 takes precedence) · CPC title

  • Alkyl ethers · CPC title

  • Powdering or granulating · CPC title

  • C08B11/12Primary

    substituted with carboxylic radicals {, e.g. carboxymethylcellulose [CMC]} · CPC title

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What does patent US12049522B2 cover?
A powder that contains carboxymethylated cellulose nanofibers, said carboxymethylated cellulose nanofibers having a degree of carboxymethyl substitution of 0.50 or less and a cellulose type I crystallinity of 60% or more, and has a median diameter of 10.0 μm to 150.0 μm. This powder is suitable usable as an additive.
Who is the assignee on this patent?
Jujo Paper Co Ltd
What technology area does this patent fall under?
Primary CPC classification C08L1/286. Mapped technology areas include Chemistry & Metallurgy.
When was this patent published?
Publication date Tue Jul 30 2024 00:00:00 GMT+0000 (Coordinated Universal Time) (B2). Legal status and post-grant events are not shown on this page.
What related patents are in patentsdb?
We list 3 related publications on this page (citations in our corpus or others sharing the same primary CPC).