Manufacturing apparatus and manufacturing method of porous glass base material for optical fiber

Patent metadata

Field	Value
Publication number	US-12043564-B2
Application number	US-202217872407-A
Country	US
Kind code	B2
Filing date	Jul 25, 2022
Priority date	Jun 11, 2019
Publication date	Jul 23, 2024
Grant date	Jul 23, 2024

Abstract

A manufacturing method of a porous glass base material for optical fiber includes: controlling a flow rate of a raw material liquid of an organic siloxane by a liquid mass flow controller; introducing raw material liquid to a raw material liquid nozzle of a vaporizer by a raw material liquid pipe; ejecting raw material liquid into the vaporizer; mixing raw material liquid and carrier gas to vaporize raw material liquid to form mixed gas; supplying mixed gas to a burner; combusting mixed gas together with a combustible gas and a combustion supporting gas in the burner to produce SiO2 particles; depositing SiO2 particles on a starting core base material to form the porous glass base material; and closing an open/close valve on a flow path of the raw material liquid pipe to stop supply of raw material liquid, while continuing to supply carrier gas, combustible gas, and combustion supporting gas.

First claim

What is claimed is:

1. A manufacturing method of a porous glass base material for optical fiber comprising:
controlling a flow rate of a raw material liquid of an organic siloxane by a liquid mass flow controller;
introducing the raw material liquid supplied from the liquid mass flow controller to a raw material liquid nozzle of a vaporizer by a raw material liquid pipe;
ejecting the raw material liquid from the raw material liquid nozzle into the vaporizer;
mixing the raw material liquid ejected in the vaporizer and a carrier gas to vaporize the raw material liquid to form a mixed gas in which the raw material gas and the carrier gas are mixed;
supplying the mixed gas to a burner;
combusting the mixed gas together with a combustible gas and a combustion supporting gas in the burner to produce SiO 2 particles;
depositing SiO 2 particles on a starting core base material to form the porous glass base material for optical fiber;
closing an open/close valve provided on a flow path of the raw material liquid pipe to stop the supply of the raw material liquid from the liquid mass flow controller, while continuing to supply the carrier gas, combustible gas, and combustion supporting gas; and
supplying a purge gas from a purge gas supply pipe that joins the raw material liquid pipe between the open/close valve and the raw material liquid nozzle to the raw material liquid pipe after the closing of the open/close valve.

2. The manufacturing method according to claim 1 further comprises additionally mixing oxygen gas into the mixed gas such that the mixed gas includes raw material gas, carrier gas, and oxygen gas, and supplying the mixed gas to the burner.

3. The manufacturing method according to claim 2 , wherein when a flow rate of the purge gas supplied from the purge gas supply pipe is L P and a flow rate of the oxygen gas additionally mixed is L O2 , in the supplying the purge gas to the raw material liquid pipe, the purge gas and the oxygen gas are respectively supplied so that L O2 /L P >14 is satisfied.

4. The manufacturing method according to claim 1 , wherein when a flow rate of the purge gas supplied from the purge gas supply pipe is L P and a flow rate of the carrier gas supplied to the vaporizer is L C , in the supplying the purge gas to the raw material liquid pipe, the purge gas and the carrier gas are respectively supplied so that L C /L P >10 is satisfied.

5. The manufacturing method according to claim 1 , wherein the carrier gas is any of nitrogen, argon, and helium.

6. The manufacturing method according to claim 1 , wherein the organic siloxane is octamethylcyclotetrasiloxane (OMCTS).

Assignees

• Shinetsu Chemical Co

Inventors

• Noda Naoto
• Iinuma Hitoshi

Classifications

• G02B1/046

  characterised by the core material · CPC title

• C03B37/07

  Controlling or regulating ({C03B37/0253 takes precedence } ; controlling or regulating in general G05) · CPC title

• C03B37/016

  by a liquid phase reaction process, e.g. through a gel phase · CPC title

• C03B37/01413

  Reactant delivery systems (C03B37/01807 takes precedence; devices therefor in general B01D1/00, B01J4/00) · CPC title

• G02B1/045

  Light guides · CPC title