Electrosorptive cavitation devices and methods for phase separation

Patent metadata

Field	Value
Publication number	US-12017155-B2
Application number	US-201816494189-A
Country	US
Kind code	B2
Filing date	Mar 13, 2018
Priority date	Mar 14, 2017
Publication date	Jun 25, 2024
Grant date	Jun 25, 2024

Abstract

Provided herein are phase separation devices and methods for performing phase separation of an aqueous mixture. Said devices and methods may include a cavitation component for cavitating the aqueous mixture to produce a cavitated aqueous mixture; and an electrosorption component for performing an electrosorptive phase separation of the cavitated aqueous mixture. Such devices and methods may be used for phase separation of aqueous mixtures including algal aqueous mixtures and/or mining or waste water aqueous mixtures, for example.

First claim

What is claimed is:

1. A phase separation device for performing continuous phase separation of an aqueous mixture, said device comprising:
a cavitation assembly for cavitating the aqueous mixture to produce a cavitated aqueous mixture; wherein the cavitation assembly comprises a tangential flow aqueous mixture inlet, a vortex stabilizer in communication with the tangential flow aqueous mixture inlet, and a nozzle in communication with the vortex stabilizer, wherein the nozzle comprises a restriction flow channel and a divergent outlet in communication with the electrosorption assembly; and
an electrosorption assembly for receiving the cavitated aqueous mixture and performing an electrosorptive phase separation of the cavitated aqueous mixture; the electrosorption assembly comprising a non-sacrificial cathode and a non-sacrificial anode.

2. The device of claim 1 , wherein the nozzle comprises the restriction flow channel having a length L and a diameter d, wherein the restriction flow channel receives the aqueous mixture and directs the aqueous mixture to the divergent outlet; wherein the cavitated aqueous mixture comprises cavitation voids comprising vapour, and wherein the electrosorptive phase separation of the cavitated aqueous mixture includes electrosorptive vapour bubble generation.

3. The device of claim 2 , wherein the restriction flow channel has a d/L ratio of 0.005-0.02.

4. The device of claim 2 , wherein d is 0.03-0.0625 inches.

5. The device of claim 1 , wherein the vortex stabilizer comprises a vortex stabilizer insert comprising a conical portion having a longitudinal slit for allowing vortexing aqueous mixture to exit the vortex stabilizer and enter the nozzle.

6. The device of claim 1 , wherein the divergent outlet comprises a conical channel which progressively widens toward the electrosorption assembly with a divergent angle of 30°-45°.

7. The device of claim 1 , wherein the divergent outlet has a diameter to length ratio of 0.1875-0.3.

8. The device of claim 1 , wherein the cathode comprising a conductive spiral tube with a central core and the anode comprising a conductive member disposed within the central core.

9. The device of claim 8 , wherein the cathode comprises a carbon-based conductive material, TiO 2 , copper, brass, aluminum, or stainless steel.

10. The device of claim 8 , wherein the conductive spiral tube of the cathode comprises two or more turns, wherein each turn, in combination with the anode, forms a distinct electrochemical cell.

11. The device of claim 1 , wherein the device is configured vertically or on an incline, such that the electrosorption assembly receives the cavitated aqueous mixture at a bottom end thereof and performs electrosorptive phase separation of the cavitated aqueous mixture as the cavitated aqueous mixture moves toward a top end of the electrosorption assembly, the top end being elevated relative to the bottom end.

12. The device of claim 1 , wherein the cathode forms an outer shell defining an interior core, and the anode is disposed within the core.

13. The device of claim 12 , wherein the cathode comprises a continuous conductive member, or a plurality of individual conductive members longitudinally aligned in series.

14. The device of claim 13 , wherein the cathode comprises a tube, spiral, or coil.

Assignees

• Nat Res Council Canada

Inventors

• Kirpalani Deepak M

Classifications

• C11B1/10

  by extracting · CPC title

• C02F2103/16

  from metallurgical processes, i.e. from the production, refining or treatment of metals, e.g. galvanic wastes · CPC title

• C02F2103/10

  from quarries or from mining activities · CPC title

• C02F2001/46171

  Cylindrical or tubular shaped · CPC title

• C02F1/465

  by electroflotation · CPC title