Alternating and continuous microwave fiber tow coating thermo-chemical reactor furnace

Patent metadata

Field	Value
Publication number	US-12000049-B2
Application number	US-202117558887-A
Country	US
Kind code	B2
Filing date	Dec 22, 2021
Priority date	Dec 22, 2021
Publication date	Jun 4, 2024
Grant date	Jun 4, 2024

Abstract

A reactor furnace for coating fiber tow includes an elongate reactor having a fiber tow inlet and a fiber tow outlet; a thermo-chemical reactor section positioned along the elongate reactor; a first microwave source for directing microwave energy along the reactor from a first end of the reactor toward a second end of the reactor; a second microwave source for directing microwave energy along the reactor from the second end of the reactor toward the first end of the reactor; a gas inlet upstream of the thermo-chemical reactor; and a gas outlet downstream of the thermo-chemical reactor.

First claim

What is claimed is:

1. A reactor furnace for coating fiber tow, comprising:
an elongate reactor having a fiber tow inlet and a fiber tow outlet;
a thermo-chemical reactor section positioned along the elongate reactor;
a first microwave source configured to direct microwave energy along the thermo-chemical reactor section in a direction from a first end of the elongate reactor toward a second end of the elongate reactor;
a second microwave source configured to direct microwave energy along the thermo-chemical reactor section in a direction from the second end of the elongate reactor toward the first end of the elongate reactor;
a gas inlet upstream of the thermo-chemical reactor section with respect to a direction of feed of fiber tow from the fiber tow inlet to the fiber tow outlet; and
a gas outlet downstream of the thermo-chemical reactor section with respect to the direction of feed of fiber tow from the fiber tow inlet to the fiber tow outlet;
a first circulator downstream of the thermo-chemical reactor section, the first circulator positioned to direct microwave energy from the first microwave source to a first termination point; and
a second circulator upstream of the thermo-chemical reactor section, the second circulator positioned to direct microwave energy from the second microwave source to a second termination point; wherein the second circulator isolates the first microwave source from the microwave energy of the second microwave source, and wherein the first circulator isolates the second microwave source from the microwave energy of the first microwave source.

2. The reactor furnace of claim 1 , further comprising a first fiber spool positioned to feed uncoated fiber to the fiber tow inlet of the elongate reactor, and a second fiber spool positioned to receive and coil a coated fiber produced in the thermo-chemical reactor.

3. The reactor furnace of claim 2 , wherein at least one of the first fiber spool and the second fiber spool is electrically grounded.

4. The reactor furnace of claim 1 , further comprising a control unit configured to receive input of temperature in the reactor and to alternate energy between the first microwave source and the second microwave source.

5. The reactor furnace of claim 1 , wherein the elongate reactor is a tube having a first end plate and a second end plate, and at least one opening in the first end plate defining an inlet for uncoated fiber in the first end plate, and at least one opening in the second end plate defining an outlet for coated fiber in the second end plate.

6. The reactor furnace of claim 5 , wherein the first end plate and the second end plate each have a plurality of openings whereby multiple fiber tows can be coated simultaneously.

7. The reactor furnace of claim 1 , wherein the elongate reactor defines an internal space, and further comprising an inert gas environment in the internal space.

8. The reactor furnace of claim 1 , wherein the elongate reactor comprises reactor tube materials selected from the group consisting of quartz, graphite and combinations thereof.

9. The reactor furnace of claim 1 , wherein the elongate reactor is between about 0.1 and 10 meters long.

10. A method for coating a fiber tow, comprising:
passing the fiber tow through the reactor furnace according to claim 1 in the presence of a coating gas; and
directing microwave energy from the first microwave source along a length of the fiber tow in the direction from the first end toward the second end; and
directing microwave energy from the second microwave source along the length of the fiber tow in the direction from the second end toward the first end;
receiving the microwave energy from the first microwave energy source in the first circulator to direct the microwave energy from the first microwave source away from the second microwave source; and receiving the microwave energy from the second microwave source in the second circulator to direct the microwave energy from the second microwave source away from the first microwave source, wherein the first circulator directs the microwave energy from the first microwave source to the first termination point, and wherein the second circulator directs the microwave energy from the second microwave source to the second termination point.

11. The method of claim 10 , wherein the microwave energy from the first microwave source is directed along the fiber tow in the direction of feed of the fiber tow, and wherein the microwave energy from the second microwave source is directed along the fiber tow in a direction opposite to the direction of feed.

12. The method of claim 10 , further comprising determining an amount of energy received in each of the first termination point and the second termination point, and adjusting power to the first microwave source and the second microwave source based on the amount of energy received.

13. The method of claim 10 , further comprising recovering energy from the first termination point and the second termination point as heat and using the heat to preheat the coating gas.

14. The method of claim 10 , further comprising alternating between directing the microwave energy from the first microwave source along the fiber tow and directing the microwave energy from the second microwave source along the fiber tow.

15. The method of claim 10 , further comprising feeding the fiber tow to the reactor furnace from a first fiber spool, and receiving coated fiber from the reactor furnace onto a second fiber spool, wherein at least one of the first fiber spool and the second fiber spool is electrically grounded.

16. The method of claim 10 , wherein gas is introduced to the reactor furnace to flow through the thermo-chemical reactor section of the reactor furnace in a gas flow direction, and wherein one of the microwave energy from the first microwave source and the microwave energy from the second microwave source is directed in the same direction as the gas flow direction, and the other of the microwave energy from the first microwave source and the microwave energy from the second microwave source is directed opposite to the gas flow direction.

Assignees

• Raytheon Tech Corp
• Rtx Corp

Inventors

• Gangloff Jr John J
• Holowczak John E
• She Ying
• Smith Kenneth David
• Cordatos Haralambos
• Gok Gurkan
• Dardas Zissis A

Classifications

• C23C16/545 Primary

  for coating elongated substrates · CPC title

• C23C16/511

  using microwave discharges · CPC title

• H01J37/32192

  Microwave generated discharge (H01J37/32357, H01J37/32366, H01J37/32394, H01J37/32403 take precedence) · CPC title

• H01J37/3277

  of continuous material · CPC title

• F27B9/062 Primary

  electrically heated · CPC title