Combination of carrier-magnetic-separation and a further separation for mineral processing

Patent metadata

Field	Value
Publication number	US-11998929-B2
Application number	US-201917268160-A
Country	US
Kind code	B2
Filing date	Aug 6, 2019
Priority date	Aug 13, 2018
Publication date	Jun 4, 2024
Grant date	Jun 4, 2024

Abstract

A process for concentrating desired particles containing a carrier-magnetic-separation with the following steps, providing a feedstock which contains the desired particles; adding hydrophobic magnetic particles to the feedstock which results in a loaded feedstock containing agglomerates of the magnetic particles and the desired particles or of the magnetic particles and the undesired material; separating the agglomerates from the loaded feedstock by a separation method which results in isolated agglomerates, breaking up the isolated agglomerates to obtain a suspension having magnetic particles in de-agglomerated form; and separating the magnetic particles from the suspension obtained in step d) by a separation method and provided that at least one separation method is a magnetic separation, and where the process has at least one further separation and where the further separation is s sorting, electric separation, screening, classification, gravity concentration, and flotation.

First claim

The invention claimed is:

1. A process for concentrating desired particles comprising a carrier-magnetic-separation comprising the following steps,
a) providing a feedstock which contains the desired particles and an undesired material;
b) adding hydrophobic magnetic particles to the feedstock which results in a loaded feedstock containing agglomerates of the magnetic particles and the desired particles or of the magnetic particles and the undesired material;
c) separating the agglomerates from the loaded feedstock by a separation method which results in isolated agglomerates, where the separation method magnetic separation;
d) breaking up the isolated agglomerates to obtain a suspension comprising the magnetic particles in de-agglomerated form; and
e) separating the magnetic particles from the suspension obtained in step d) by a separation method selected from sorting, electric separation, magnetic separation, screening, classification, gravity concentration, and flotation; and
f) optionally re-introducing the magnetic particles obtained in step e) to step b);
g) provided that at least one separation method of steps c) or e) is a magnetic separation, and where the process comprises at least one further separation before or after the steps a), b), c), d) or e),
wherein the at least one further separation is made before the agglomeration step b),
and where the further separation is selected from the group consisting of sorting, electric separation, screening, classification, gravity concentration, and flotation

wherein the flotation is achieved with
mechanical flotation machines,
pneumatic flotation machines,
hybrid flotation machines,
flotation columns,
reactor/separator flotation machines,
flash flotators,
Hydrofloat separator, or
Stack cells.

2. The process according to claim 1 , wherein the gravity concentration is achieved with
jigs,
spiral concentrators,
shaking tables,
centrifugal concentrators,
sluices,
cones,
fluidized bed separators,
dense medium separators or
elutriators.

3. The process according to claim 1 , wherein the gravity concentration is achieved with
jigs selected from the group consisting of Harz jig, IHC radial jig, in line pressure jig, Denver mineral jig and air-pulsated jig,
spiral concentrators selected from the group consisting of Humpreys spiral, soluble start and spiral concentrator,
shaking tables selected from the group consisting of sand tables, slime tables, Duplex concentrator, and Mozley laboratory separator,
centrifugal concentrators selected from the group consisting of Kelsey centrifugal jig, Knelson concentrator, Falcon concentrator and multi-gravity separator,
pinched sluiced,
Reichert cone,
fluidized bed separators selected from the group consisting of Cross Flow separator, and Reflux Classifier,
dense medium separators selected from the group consisting of gravitational vessels like drum separators, Wemco cone separator, Drewboy bath, Norwalt washer; centrifugal separators like dense medium cyclones, water-only cyclones, Vorsyl separator, large coal dense medium separator, Dyna whirlpool separator, and Tri-Flo separator, or
elutriators selected from the group consisting of teetered bed separator, Floatex density separator, HydroFloat separator, and allflux separator.

4. The process according to claim 1 , wherein the sorting is achieved by hand or sensor based sorting, where the sensor type is selected from color in visible light, ultraviolet, gamma radiation, neutron radiation, conductivity, X-ray fluorescence, X-ray luminescence, infrared, Raman, or microwave attenuation.

5. The process according to claim 1 , wherein the electric separation is achieved by charging via ion or electron bombardment, conductive induction, or triboelectric charging.

6. The process according to claim 1 , wherein the magnetic separation is achieved by low-intensity, high-intensity, high-gradient, or superconducting magnetic separators.

7. The process according to claim 1 , wherein the classification is achieved with centrifugal classifiers or gravitational classifier, such as sedimentation classifier, counter flow classifier, or air classifier.

8. The process according to claim 1 , wherein the screening is achieved with vibrating screens, static grizzlies, Mogensen Divergators, trommes, bradford breaker, roller screens, flip-flow screen, rotaspiral, Pansep screen, sieve bends, or tumbler screens.

9. The process according to claim 1 , where in case the further separation is flotation then the flotation is not made in step c) or not between step c) and step d).

10. The process according to claim 1 , wherein the further separation is made before the step b), and in between the step b) and the step d), or after the step d).

11. The process according to claim 1 , wherein the further separation is gravity concentration, which is made
i) before the agglomeration step b),
ii) after the separation step e), or
iii) after step b), and
optionally the gravity concentration is excluding elutriation.

12. The process according to claim 1 , wherein the further separation is screening, which is made
i) before the agglomeration step b),
ii) after the separation step e) or
iii) after step b).

13. The process according to claim 1 , wherein the further separation is classification, which is made
i) before the agglomeration step b),
ii) after the separation step e), or
iii) after step b).

14. The process according to claim 1 , wherein the further separation is sorting and is made before step b).

15. The process according to claim 1 , wherein the further separation is classification and is made before step b).

16. The process according to claim 1 , wherein the further separation is made before step a).

17. The process according to claim 1 , wherein the further separation is selected from the group consisting of sorting and electric separation and is made in dry state before step a).

Assignees

• Basf Se

Inventors

• Rohde Wolfgang
• Gilbert David Johann
• Schuler Bernhard
• Kuhn Oliver
• Mentges Michael

Classifications

• B03C1/30 Primary

  Combinations with other devices, not otherwise provided for · CPC title

• B03B9/00

  General arrangement of separating plant, e.g. flow sheets · CPC title

• B03C1/002

  High gradient magnetic separation (acting directly on the substance being separated B03C1/025; acting on the medium containing the substance being separated B03C1/32) · CPC title

• B03C1/01 Primary

  by addition of magnetic adjuvants · CPC title

• B03D1/023

  Carrier flotation; Flotation of a carrier material to which the target material attaches · CPC title