Corn protein retention during extraction

Patent metadata

Field	Value
Publication number	US-11985990-B2
Application number	US-201716335604-A
Country	US
Kind code	B2
Filing date	Oct 6, 2017
Priority date	Sep 23, 2016
Publication date	May 21, 2024
Grant date	May 21, 2024

Abstract

Disclosed herein is a method of maintaining corn protein yield during extraction and managing stickiness and viscosity comprising obtaining a corn material having a corn protein content and washing the corn material to remove non-protein components with an ethanol-water solvent comprising at least 85 wt % ethanol to obtain a corn protein isolate, wherein the loss of corn protein content during extraction is less than 10% of total corn protein.

First claim

The invention claimed is:

1. A method of maintaining corn protein yield during extraction of corn material to obtain a corn protein isolate, comprising:
obtaining a destarched corn gluten meal comprising at least 70 wt % corn protein on a dry weight basis; and
treating the destarched corn gluten meal to obtain a desolventized corn protein isolate by a method consisting essentially of
a) carrying out an extraction of non-protein solutes from the destarched corn gluten meal by washing the destarched corn gluten meal to extract the non-protein solutes with an ethanol-water solvent comprising at least 85 wt % ethanol to obtain a corn protein isolate;
b) collecting the corn protein isolate in the form of collected solids from the ethanol-water solvent extraction step a), wherein the collected solids comprises residue ethanol-water solvent; and
c) desolventizing the residue ethanol-water solvent from the collected solids of step b) by drying with heat to provide a desolventized corn protein isolate;

wherein the extraction occurs at temperatures ranging from about 5-50° C.,
wherein the amount of total water present in the ethanol-water solvent extraction step a) is limited such that less than 10% of the corn protein content is removed from the corn material by the ethanol-water solvent during the extraction, and
wherein the amount of water present in the collected solids collected in step b) is limited such that the collected solids comprising the residue ethanol-water solvent has a tack force ranging from −1.000 to 0 at 42.5° C.

2. The method of claim 1 , wherein the extraction occurs at temperatures ranging from about 20-30° C.

3. The method of claim 1 , wherein the ethanol-water solvent comprises at least 90 wt % ethanol.

4. The method of claim 1 , wherein the ethanol-water solvent comprises at least 95 wt % ethanol.

5. The method of claim 1 , wherein the corn protein isolate comprises 87-98 wt % corn protein on a dry weight basis.

6. The method of claim 1 , wherein the corn protein isolate has a viscosity ranging from 1500-3500 centipoise.

7. The method of claim 1 , wherein less than 5% of the corn protein content is removed from the corn material during the extraction.

8. The method of claim 1 , wherein the corn protein isolate has a maximum compressibility strain of 0.600.

9. The method of claim 1 , wherein the corn protein isolate comprises 55-98 wt % corn protein on a dry weight basis.

10. The method of claim 1 , wherein the corn protein isolate comprises 87-98 wt % corn protein on a dry weight basis.

11. The method of claim 1 , wherein the desolventizing is carried out by a rotary evaporator.

Assignees

• Cargill Inc

Inventors

• Frank christopher lawrence
• Huelsnitz Christopher Steven
• Mcconville Erika Lyn
• Porter Michael A
• Steinbach Adam John
• Yehia Hadi Nayef
• Zheng Guo-Hua

Classifications

• A23J1/12 Primary

  from cereals, wheat, bran, or molasses · CPC title

• A23L5/23

  by extraction with solvents · CPC title

• A23V2002/00

  Food compositions, function of food ingredients or processes for food or foodstuffs · CPC title