Device and method for the continuous high-pressure treatment of bulk material and use thereof

Patent metadata

Field	Value
Publication number	US-11980832-B2
Application number	US-201917415942-A
Country	US
Kind code	B2
Filing date	Dec 20, 2019
Priority date	Dec 22, 2017
Publication date	May 14, 2024
Grant date	May 14, 2024

Abstract

An apparatus and method of high pressure treatment of bulk material by extraction and/or impregnation may involve treating bulk material in an internal volume of a pressure vessel apparatus at a high pressure level in a range from 40 to 1000 bar under isolation from the environment. The high pressure treatment may be performed charge-wise in a closed system in the pressure vessel apparatus in that the bulk material is supplied charge-wise to the internal volume with the pressure vessel apparatus closed and is positioned in at least one treatment plane. Upon completion of the high pressure treatment, the bulk material is discharged charge-wise from the internal volume with the pressure vessel apparatus closed. This also gives advantages in terms of handling, especially also with regard to material flow, and with regard to operational reliability.

First claim

What is claimed is:

1. A method for high pressure treatment of bulk material by extraction, wherein the bulk material is positioned in a high pressure treatment volume of a pressure vessel apparatus and is treated at a high pressure level in a range from 40 to 1000 bar under isolation from the environment, wherein the method comprises:
pressurizing the high pressure treatment volume;
high pressure treating the bulk material in a continuous manner at the high pressure level in the high pressure treatment volume, with continuity of the high pressure treating being assured solely by way of the high pressure treatment volume, wherein the high pressure treatment volume or the pressure vessel apparatus is in a fixed arrangement while the high pressure treating occurs, wherein during the high pressure treating discontinuous gravitational force-driven displacement of the bulk material occurs through the high pressure treatment volume by multiple discontinuous rotational or translational actuating movements, wherein the bulk material is disposed in a predefined first high pressure treatment plane and is then displaced continuously or between additional high pressure treatment planes within the high pressure treatment volume during the high pressure treating by virtue of the rotational or translational actuating movements, and wherein the bulk material is selected from polymers configured as superinsulators or aerogels;
depressurizing the high pressure treatment volume; and
wherein the high pressure treating comprises a continuous extraction.

2. The method of claim 1 wherein during the high pressure treating, continuous displacement or cyclical discontinuous batchwise displacement of the bulk material establishes a dwell time or a high pressure treatment time for the bulk material in the high pressure treatment volume.

3. The method of claim 1 wherein during the high pressure treating, bulk material displacement is controlled based on a size and/or cyclical supply of batches and/or charges while the bulk material is displaced continuously or in individual discontinuous batches in the high pressure treatment volume by way of the rotational actuating movements.

4. The method of claim 1 wherein the continuous extraction takes place above a critical temperature and above a critical pressure of a solvent used in the extraction.

5. The method of claim 1 comprising flowing a high pressure medium through the bulk material.

6. The method of claim 1 wherein the high pressure treating is performed at a constant high pressure or with fluctuations of pressure in a range of three to five bar inclusive.

7. The method of claim 1 wherein the translational actuating movements establish a displacement speed or cyclical discontinuous batchwise displacements that establish a dwell time or a high pressure treatment time for the bulk material in the high pressure treatment volume.

8. The method of claim 1 wherein the high pressure treating comprises discontinuous batchwise displacement of the bulk material by multiple discontinuous translational actuating movements.

9. The method of claim 1 wherein the bulk material is displaced at predefined times in the high pressure treatment volume in batches between individual ones of the high pressure treatment planes.

10. A method for high pressure treatment of bulk material by extraction, wherein the bulk material is positioned in a high pressure treatment volume of a pressure vessel apparatus and is treated at a high pressure level in a range from 40 to 1000 bar under isolation from the environment, wherein the method comprises: pressurizing the high pressure treatment volume; and high pressure treating the bulk material in a continuous manner at the high pressure level in the high pressure treatment volume, with continuity of the high pressure treating being assured solely by way of the high pressure treatment volume, wherein the high pressure treatment volume or the pressure vessel apparatus is in a fixed arrangement while the high pressure treating occurs, wherein during the high pressure treating discontinuous gravitational force-driven displacement of the bulk material occurs through the high pressure treatment volume by multiple discontinuous rotational or translational actuating movements, wherein the bulk material is disposed in a predefined first high pressure treatment plane and is then displaced continuously or between additional high pressure treatment planes within the high pressure treatment volume during the high pressure treating by virtue of the rotational or translational actuating movements, wherein the high pressure treating comprises at least one of:
continuous displacement of the bulk material in two different predefined material flow directions within the high pressure treatment volume, including in a first material flow direction defined by the rotational actuating movements and a second material flow direction defined by the translational actuating movements; or
continuous displacement of the bulk material counter to gravity by supplying potential energy to the bulk material by way of a rotational actuating movement; and
depressurizing of the high pressure treatment volume.

11. A high pressure treatment system configured for high pressure treatment of bulk material by extraction at a high pressure level in a range from 40 to 1000 bar, the high pressure treatment system comprising:
a pressurization device with pressurization generation means;
a pressure vessel apparatus coupled to the pressurization device by a high pressure-tight connection, the pressure vessel apparatus including a high pressure-resistant wall that surrounds a high pressure treatment volume for the high pressure treatment, wherein the pressure vessel apparatus includes an actuator being rotationally or translationally displaceable and configured for a rotational actuating movement or a translational actuating movement, each for gravitational force-driven displacement of the bulk material through the high pressure treatment volume during the high pressure treatment; and
a depressurization device coupled to the pressure vessel apparatus by a high pressure-tight connection,
wherein the high pressure vessel apparatus is in a fixed arrangement and is configured to a continuous high pressure treatment solely by way of the high pressure treatment volume being in a fixed arrangement and at the high pressure level,
wherein the actuator is configured to individually actuate a high pressure treatment plane of the pressure vessel apparatus or to simultaneously synchronously actuate multiple high pressure treatment planes of the pressure vessel apparatus, and wherein in the high pressure treatment volume multiple high pressure treatment planes are each defined by at least one gas-permeable plate with outflow chambers and with a passage segment.

12. The high pressure treatment system of claim 11 configured to:
supply individual batches of bulk material to the high pressure treatment volume during the high pressure treatment;
displace individual batches of bulk material within the high pressure treatment volume during the high pressure treatment; and
discharge individual batches of bulk material from the high pressure treatment volume during the high pressure treatment.

13. The high pressure treatment system of claim 11 wherein the actuator is coupled to multiple ones of the high pressure treatment planes, wherein each of the multiple high pressure treatment planes is defined by a pair of plates, wherein a first plate of the pair of plates is in a static arrangement at a fixed location and a second plate of the pair of plates is rotationally displaceable and

Assignees

• Uhde High Pressure Tech Gmbh
• Thyssenkrupp Ag

Inventors

• Steinhagen Volkmar
• Herber Ansgar

Classifications

• B01D11/0246 Primary

  comprising rotating means · CPC title

• B01D11/0203 Primary

  with a supercritical fluid · CPC title

• B01D11/0207

  Control systems · CPC title

• B01D11/0219

  Fixed bed of solid material · CPC title

• B01D11/0226

  with the general transport direction of the solids parallel to the rotation axis of the conveyor, e.g. worm · CPC title