Sacrificial substrates for silicon-carbon composite materials
US-2020381703-A1 · Dec 3, 2020 · US
US11969771B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11969771-B2 |
| Application number | US-202318359139-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 26, 2023 |
| Priority date | Jul 27, 2022 |
| Publication date | Apr 30, 2024 |
| Grant date | Apr 30, 2024 |
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A method of fabricating a film vibration device, including: photoetching a surface of a silicon wafer to form a circular-hole array; etching an aluminum layer on the silicon wafer; etching the silicon wafer to form a through-hole array to obtain a porous silicon wafer; attaching a polyethylene terephthalate (PET) sheet to a side of the porous silicon wafer; ablating the PET sheet to obtain a porous PET film; attaching a polyvinylidene fluoride (PVDF) film to a lower side of the porous silicon wafer; performing vacuumization above the porous silicon wafer, while heating the PVDF film below the porous silicon wafer to create dome micro-structures on the PVDF film; and laminating the porous PET film on each of two sides of the PVDF film to obtain the film vibration device. This application also provides a cleaning device having the film vibration device.
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What is claimed is: 1. A method of fabricating a film vibration device, comprising: (S 1 ) forming a circular-hole array on a surface of a silicon wafer by photoetching; (S 2 ) etching an aluminum layer on the silicon wafer; (S 3 ) etching the silicon wafer to form a through-hole array, so as to obtain a porous silicon wafer; (S 4 ) attaching a polyethylene terephthalate (PET) sheet to a side of the porous silicon wafer; and subjecting the PET sheet to breakdown with the porous silicon wafer as a mask to obtain a porous PET film; (S 5 ) attaching a polyvinylidene fluoride (PVDF) film to a lower side of the porous silicon wafer; performing vacuumization above the porous silicon wafer, and simultaneously heating the PVDF film below the porous silicon wafer such that a plurality of dome micro-structures are formed on the PVDF film; and (S 6 ) laminating the porous PET film on each of two sides of the PVDF film having the plurality of dome micro-structures to obtain the film vibration device; wherein in step (S 5 ), the heating is performed through three annealing-cooling operations, each comprising: heating a bottom of the PVDF film at 75-85° C. for 4-6 min; and cooling the PVDF film to room temperature while keeping vacuum above the PVDF film. 2. The method of claim 1 , wherein step (S 1 ) comprises: (S 1 - 1 ) depositing an aluminum film on the silicon wafer to form the aluminum layer on the surface of the silicon wafer; (S 1 - 2 ) applying a photoresist to a top of the aluminum film followed by soft baking to form a photoresist layer on the surface of the aluminum layer; and (S 1 - 3 ) subjecting the photoresist layer to patterning through photoetching followed by exposure and development with a developer. 3. The method of claim 1 , wherein step (S 2 ) comprises: (S 2 - 1 ) drying the silicon wafer after photoetched; and (S 2 - 2 ) immersing the silicon wafer in an aluminum etchant to etch an exposed part of the aluminum layer. 4. The method of claim 1 , wherein step (S 3 ) comprises: (S 3 - 1 ) etching the silicon wafer through a plasma reaction; (S 3 - 2 ) removing a photoresist layer; and (S 3 - 3 ) etching a remaining part of the aluminum layer with an aluminum etchant to obtain the porous silicon wafer. 5. The method of claim 1 , wherein step (S 4 ) comprises: (S 4 - 1 ) attaching the PET sheet to the side of the porous silicon wafer, wherein the PET sheet has a thickness of 45-55 μm; and (S 4 - 2 ) ablating the PET sheet by a laser grating with the porous silicon wafer as the mask; and separating an ablated PET sheet from the porous silicon wafer to obtain the porous PET film. 6. The method of claim 1 , wherein a thickness of the PVDF film is 8-12 μm. 7. The method of claim 1 , wherein each of two sides of the PVDF film is coated with a silver electrode layer having a thickness of 60-80 nm. 8. A film vibration device prepared by the method of claim 1 , comprising: a first porous PET film; a second porous PET film; and a PVDF film; wherein the PVDF film is sandwiched between the first porous PET film and the second porous PET film; the first porous PET film and the second porous PET film have the same structure; the first porous PET film is arranged above the PVDF film; and the second porous PET film is arranged below the PVDF film; and the PVDF film is provided with a plurality of dome micro-structures adapted to a through-hole array of the first porous PET film; the plurality of dome microstructures are embedded in the through-hole array of the first porous PET film; and two sides of the PVDF film are each coated with a silver electrode layer. 9. A cleaning device, comprising: a container; a control panel; and the film vibration device of claim 8 ; wherein the film vibration device is arranged on a bottom of the container, and is electrically connected with the control panel.
Using ultrasounds · CPC title
with foil-type piezoelectric elements, e.g. PVDF · CPC title
Foil type, e.g. PVDF · CPC title
Cleaning in a tank · CPC title
Treatment with inorganic or organometallic reagents after imagewise removal · CPC title
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