Process and apparatus for reduction in microbial growth in solutions of sugars extracted from waste materials

Patent metadata

Field	Value
Publication number	US-11965219-B2
Application number	US-201917055703-A
Country	US
Kind code	B2
Filing date	May 14, 2019
Priority date	May 17, 2018
Publication date	Apr 23, 2024
Grant date	Apr 23, 2024

Abstract

A process for reducing microbial growth in solutions of sugars extracted from waste materials, the process comprising monitoring indicators of microbial growth in the solution in situ and administering an antimicrobial; a sugar substrate obtained by concentrating a solution of sugar treated using the process; an apparatus for extracting sugars from waste materials, the apparatus comprising a reaction vessel ( 10 ), one or more sensors ( 15,20 ) for monitoring indicators of microbial growth in the reaction vessel, a software for analysing signals from the sensor and a source of antimicrobial.

First claim

The invention claimed is:

1. A process for reducing microbial growth in a solution of sugars extracted from waste materials, the process comprising:
a. monitoring one or more indicators of microbial growth in the solution in situ; and
b. administering one or more antimicrobials in response to microbial growth being detected based on the one or more indicators of microbial growth,
wherein the one or more indicators of microbial growth comprise dissolved oxygen.

2. A process according to claim 1 , wherein the one or more indicators of microbial growth further comprises pH.

3. A process according to claim 1 , wherein the one or more indicators of microbial growth is a concentration of dissolved oxygen in a range of 0-1 mg/L.

4. A process according to claim 1 , wherein the microbial growth is growth selected from bacterial growth, fungal growth, viral growth, protistal growth, archaeal growth and combinations thereof.

5. A process according to claim 4 , wherein the microbial growth is growth selected from bacterial growth, fungal growth, viral growth, and combinations thereof.

6. A process according to claim 1 , wherein the one or more antimicrobials are selected from antibiotics, disinfectants, antiseptics or combinations thereof.

7. A process according to claim 6 , wherein the one or more antimicrobials are selected from disinfectants, antiseptics or combinations thereof.

8. A process according to claim 1 , wherein the one or more antimicrobials are selected from ozone, sodium azide, chlorine dioxide, benzisothiazolinone (BIT) or combinations thereof.

9. A process according to claim 8 , wherein the one or more antimicrobials are administered at levels in a range of 0.005-0.015 wt % for sodium azide; 2.5×10 −4 -0.05 wt % for BIT; 0.01-0.35 wt % for chlorine dioxide or 0.002-0.05 wt % for virginiamycin.

10. A process according to claim 1 , wherein the one or more antimicrobials are administered when a gradient of a decrease of oxygen in the solution of sugars is in the range −0.025 to −0.030 mg/L.

11. An apparatus for extracting sugars from waste materials, the apparatus comprising:
a. a reaction vessel;
b. one or more sensors for monitoring one or more indicators of microbial growth in the reaction vessel, wherein the one or more indicators of microbial growth comprises dissolved oxygen;
c. software for analysing signals from the one or more sensors and controlling administering of an antimicrobial in response to signals from the one or more sensors; and
d. a source of the antimicrobial.

12. An apparatus according to claim 11 , wherein the one or more sensors are in contact with a solution of sugar extracted from waste materials.

13. An apparatus according to claim 11 , wherein the one or more sensors comprise one or more sensors selected from a pH sensor and/or an oxygen sensor.

14. An apparatus according to claim 11 , wherein the one or more sensors comprise an oxygen sensor.

15. An apparatus according to claim 11 , wherein the one or more sensors comprise an electrochemical sensor.

16. An apparatus according to claim 11 , wherein the software comprises closed-loop feedback control software.

17. An apparatus according to claim 11 , further comprising an actuator for administering the antimicrobial to the reaction vessel.

Assignees

• Univ Leeds Innovations Ltd

Inventors

• Blacker Andrew John
• Bourne Richard Anthony
• Reynolds William Robert

Classifications

• B09B3/80

  involving an extraction step · CPC title

• B09B3/60 Primary

  Biochemical treatment, e.g. by using enzymes · CPC title

• C13B20/005 Primary

  using chemicals not provided for in groups C13B20/02 - C13B20/14 · CPC title

• A23B2/70

  by treatment with chemicals · CPC title

• A01N43/80

  five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2 · CPC title