Air separation device

Patent metadata

Field	Value
Publication number	US-11959702-B2
Application number	US-202117192426-A
Country	US
Kind code	B2
Filing date	Mar 4, 2021
Priority date	Mar 5, 2020
Publication date	Apr 16, 2024
Grant date	Apr 16, 2024

Abstract

An air separation device can include: a first compressor and a second compressor for compressing feed air; a first refrigerator and a second refrigerator for cooling the feed air; a pre-purification unit for pre-purifying the feed air; a flow rate measuring unit for measuring the flow rate of the feed air; a main heat exchanger for subjecting the feed air to heat exchange; a purification portion into which the feed air led out from the main heat exchanger is fed, and which separates and purifies product nitrogen and/or product oxygen from the feed air; and a compressor control unit for controlling the feed quantity of the feed air in accordance with an increase or decrease in the production quantity of product nitrogen and/or product oxygen.

First claim

What is claimed is:

1. An air separation device comprising:
a first compressor configured to compress a feed air;
a second compressor installed in series or in parallel with the first compressor;
a first refrigerator configured to cool the feed air that has been compressed by the first compressor and/or the second compressor;
a second refrigerator in series or in parallel with the first refrigerator;
a pre-purification unit configured to pre-purify the feed air that has been cooled by the first refrigerator and/or the second refrigerator;
a flow rate measuring unit configured to measure the flow rate of the feed air that has been pre-purified by the pre-purification unit;
a main heat exchanger, into which the feed air that has been pre-purified by the pre-purification unit is introduced for heat exchange;
a purification portion into which the feed air led out from the main heat exchanger is fed, and which separates and purifies product nitrogen and/or product oxygen from the feed air; and
a compressor control unit configured to control the feed quantity of feed air in accordance with an increase or decrease in the production quantity of product nitrogen and/or product oxygen, wherein the compressor control unit comprises:
a pressure setting unit which determines a pressure setting value in accordance with the flow rate of the feed air fed to the purification portion;
a liquid level setting unit which, in accordance with the flow rate of the feed air fed to the purification portion, determines a liquid level setting value for oxygen-enriched liquid collected in the distillation portion; and
a compressor automatic drive unit which automatically starts the standby-side first compressor or second compressor if the flow rate of the feed air is at least equal to a first flow rate threshold, and automatically stops the compressor that is to be put on standby, selected from among the first compressor and the second compressor, if the flow rate of the feed air is at most equal to a second flow rate threshold lower than the first flow rate threshold.

2. The air separation device according to claim 1 , further comprising a refrigerator automatic drive unit which is configured to:
automatically operate the standby-side first refrigerator or second refrigerator if the temperature of the feed air introduced into the pre-purification unit is at or above a first temperature threshold for a first duration;
automatically stop the refrigerator that is to be put on standby, selected from among the first refrigerator and the second refrigerator, if the temperature of the feed air introduced into the pre-purification unit is maintained at or below a second temperature threshold lower than the first temperature threshold for a second duration; and
automatically stop the first refrigerator and the second refrigerator if the temperature of the feed air sent to the upstream-side first refrigerator or second refrigerator is equal to or less than a third temperature threshold and the temperature of the feed air introduced into the pre-purification unit is maintained at or below the second temperature threshold for the second duration.

3. The air separation device according to claim 1 , further comprising an adsorption processing time determining unit which:
calculates a quantity of moisture and a quantity of carbon dioxide in the feed air on the basis of the temperature of the feed air introduced into the pre-purification unit, the pressure of the feed air introduced into the pre-purification unit, and the flow rate of the feed air fed to the purification portion;
calculates a moisture adsorbable time during which moisture can be adsorbed by an adsorbent, and a carbon dioxide adsorbable time during which carbon dioxide can be adsorbed by the adsorbent, from the quantity of moisture and the quantity of carbon dioxide, and the filling amount of the adsorbent in the pre-purification unit; and
determines the value of the smaller of the moisture adsorbable time and the carbon dioxide adsorbable time to be an adsorption processing time.

4. The air separation device according to claim 3 , further comprising a regeneration processing time determining unit which:
calculates an adsorbed moisture total weight and an adsorbed carbon dioxide total weight that have been adsorbed, from the quantity of moisture, the quantity of carbon dioxide, and the adsorption processing time;
calculates a moisture desorption heat quantity for desorbing the adsorbed moisture total weight of moisture from the adsorbent, and a carbon dioxide desorption heat quantity for desorbing the adsorbed carbon dioxide total weight of carbon dioxide from the adsorbent;
calculates a total desorption heat quantity by adding the moisture desorption heat quantity and the carbon dioxide desorption heat quantity; and
calculates a regeneration processing time by dividing the total desorption heat quantity by an amount of heat in heated waste gas that has been heated by a heating unit.

Assignees

• Air Liquide

Inventors

• Kaneda Takuya
• Sugitani Tsuyoshi

Classifications

• F25J3/08 Primary

  Separating gaseous impurities from gases or gaseous mixtures {or from liquefied gases or liquefied gaseous mixtures}(cold traps B01D8/00) · CPC title

• B01D53/0438

  Cooling or heating systems · CPC title

• B01D53/0454

  Controlling adsorption (controlling temperature swing adsorption B01D53/0462, controlling pressure swing adsorption B01D53/047) · CPC title

• B01D2256/10

  Nitrogen · CPC title

• B01D2256/12

  Oxygen · CPC title