Apparatus for mixing based on oscillatory flow reactors provided with smooth periodic constrictions
US-2016250615-A1 · Sep 1, 2016 · US
US11944944B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11944944-B2 |
| Application number | US-201816760768-A |
| Country | US |
| Kind code | B2 |
| Filing date | Oct 24, 2018 |
| Priority date | Nov 7, 2017 |
| Publication date | Apr 2, 2024 |
| Grant date | Apr 2, 2024 |
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A mixing apparatus includes a mixer configured to mix a material including a rubber or a resin in the presence of a working fluid that is in a supercritical state or a subcritical state. The mixer includes a chamber that forms a flow passage for the working fluid and the material, and a mixing blade disposed in the chamber and fixed to the chamber.
Opening claim text (preview).
The invention claimed is: 1. A mixing apparatus comprising a mixer configured to mix a material including a rubber or a resin in the presence of a working fluid that is in a supercritical state or a subcritical state, wherein the mixer comprises: a chamber that forms a flow passage for the working fluid and the material; a mixing blade disposed in the chamber and fixed to the chamber, a mixer entrance pressure gauge configured to detect a pressure within an entrance-side portion of the mixer; a mixer exit pressure gauge configured to detect a pressure within an exit-side portion of the mixer; a mixer entrance thermometer configured to detect a temperature within an entrance-side portion of the mixer; and a mixer exit thermometer configured to detect a temperature within an exit-side portion of the mixer, and wherein the mixer is inclined with respect to a horizontal direction so that the material goes down from an upstream side to a downstream side of the mixer. 2. The mixing apparatus according to claim 1 , comprising a separator provided downstream of the mixer and configured to separate the working fluid from the material. 3. The mixing apparatus according to claim 2 , comprising a pressure adjustment valve configured to adjust a degree of opening of a flow passage through which the working fluid separated from the material is to pass. 4. The mixing apparatus according to claim 2 , wherein the separator comprises an opening portion configured to intermittently eject the material from which the working fluid has been separated. 5. The mixing apparatus according to claim 3 , wherein the separator comprises an opening portion configured to intermittently eject the material from which the working fluid has been separated. 6. The mixing apparatus according to claim 1 , comprising a degree-of-opening adjustment valve configured to adjust a degree of opening of a flow passage through which the working fluid and the material ejected from the mixer are to pass. 7. The mixing apparatus according to claim 1 , further comprising a controller configured to control a differential pressure between the pressure detected by the mixer entrance pressure gauge and the pressure detected by the mixer exit pressure gauge so that the differential pressure falls within a prescribed range. 8. The mixing apparatus according to claim 1 , wherein the mixer comprises: a mid-mixer pressure gauge configured to detect a pressure at a portion located downstream of the mixer entrance pressure gauge and upstream of the mixer exit pressure gauge; and a mid-mixer thermometer configured to detect a temperature at a portion located downstream of the mixer entrance thermometer and upstream of the mixer exit thermometer. 9. The mixing apparatus according to claim 1 , wherein the mixer comprises a mixing acceleration member, and wherein the mixing acceleration member is fixed to the chamber, blocks a part of the flow passage in the chamber, and is provided separately from the mixing blade. 10. The mixing apparatus according to claim 1 , wherein a sectional area of the chamber as viewed from an axial direction varies depending on a position in the axial direction. 11. The mixing apparatus according to claim 1 , wherein a line obtained by connecting centers of cross sections, as viewed from an axial direction of the chamber, of the chamber is shaped like a curved line or a polygonal line. 12. The mixing apparatus according to claim 1 , wherein the mixing blades are arranged at intervals in an axial direction of the chamber. 13. The mixing apparatus according to claim 1 , wherein the mixer comprises a heater configured to heat inside the chamber. 14. The mixing apparatus according to claim 1 , wherein the mixer comprises a cooler configured to cool inside the chamber. 15. The mixing apparatus according to claim 1 , comprising an auxiliary mixer disposed downstream of the mixer and configured to exert a pressure that is higher than atmospheric pressure on the material. 16. The mixing apparatus according to claim 1 , comprising a pump configured to send out the working fluid to the mixer, wherein a rotation speed of the pump is inverter-controlled.
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