Fractionated stillage separation and feed products

Patent metadata

Field	Value
Publication number	US-11944109-B2
Application number	US-201816624811-A
Country	US
Kind code	B2
Filing date	Jun 19, 2018
Priority date	Jun 19, 2017
Publication date	Apr 2, 2024
Grant date	Apr 2, 2024

Abstract

This disclosure describes methods to separate solids from liquids in a production facility. A process separates components in the process stream by applying non-condensable media to create density differences and then using a mechanical device to separate the solids from the liquids based on the density difference. The process produces the liquids and solids, which may be further processed to create valuable animal feed products.

First claim

What is claimed is:

1. A method for separating components in a process stream, the method comprising:
receiving the process stream having a mixture of components of liquids and solids;
adding a non-condensable media to the mixture of components to change a density differential between the components;
separating the solids from the liquids in the mixture of components with a first separation device, to provide a separated solids stream and a separated liquids stream, wherein the separated solids stream is approximately 10% to approximately 40% total solids;
producing at least a portion of the separated solids stream as a feed product; and
processing the separated liquids stream with a membrane-based second separation device to recover suspended solids as a stream comprising protein.

2. The method of claim 1 , wherein the process stream comprises about 4% to about 12% total solids.

3. The method of claim 1 , wherein the process stream comprises a fractionated stillage.

4. The method of claim 1 , wherein the non-condensable media comprises at least one of air, carbon dioxide, nitrogen, or oxygen.

5. The method of claim 1 , wherein the first separation device comprises a sedicanter centrifuge, a decanter centrifuge, a disk stack centrifuge, a cyclone, an air floatation device, or a settling tank.

6. The method of claim 1 , wherein the separated solids stream comprises at least approximately 38% protein.

7. The method of claim 1 , further comprising evaporating at least a portion of the separated liquids stream to provide a condensed stream.

8. The method of claim 7 , further comprising drying the condensed stream to provide a dried product.

9. The method of claim 1 , wherein processing the separated liquids stream with the membrane-based separation device includes filtering using a plurality of membrane-enclosed open channels.

10. The method of claim 1 , wherein processing the separated liquids stream with the membrane-based separation device comprises using an open channel design having multiple channels.

11. The method of claim 1 , wherein processing the separated liquids stream includes recovering oil.

12. A method of producing a protein product from a processing stream, the method comprising:
receiving a process stream from a production facility, the process stream comprising a mixture of one or more liquids and one or more solids;
adding a non-condensable media to the mixture to change a density of each of differential between the one or more solids and the one or more liquids:
separating the one or more solids from the one or more liquids in the mixture based on a difference in density between the one or more solids and the one or more liquids, to provide a separated solids stream and a light emulsion phase;
processing the light emulsion phase with a separation device comprising an open channel membrane filter to recover oil from a protein-containing stream; and
producing at least a portion of the separated solids stream as a feed product comprising protein.

13. The method of claim 12 , wherein the separated solids stream comprises approximately 15% to approximately 39% total solids.

14. The method of claim 12 , wherein the separated solids stream comprises at least one of zein, germ, insoluble fiber, insoluble starch, inorganic acids, non-fermentable carbohydrates, oil, or a combination thereof.

15. The method of claim 12 , wherein the light emulsion phase comprises approximately 4% to approximately 12% total solids.

16. The method of claim 12 , wherein the separating of the one or more solids from the one or more liquids comprises using centrifugal force in a range of from approximately 3,000 g force to approximately 10,000 g force.

17. A method comprising: receiving a process stream comprising a mixture of one or more liquids and one or more solids;
adding non-condensable media to the mixture to change a density differential between the one or more liquids and the one or more solids; and
separating the one or more liquids from the one or more solids in the process stream using a first separation device to provide a separated liquids stream and a separated solids stream, wherein the separated solids stream has at least approximately 38% protein;
wherein the first separation device includes a sedicanter centrifuge, a decanter centrifuge, an air flotation device, a disk stack centrifuge, a cyclone, or a settling tank; and
processing the separated liquids stream with a second separation device to separate oil from a protein-containing stream, the second separation device comprising an open channel membrane filter.

18. The method of claim 17 , further comprising evaporating at least a portion of the separated liquids stream to provide a condensed stream.

19. The method of claim 17 , wherein the separated liquids stream comprises from about 20% to about 55% total solids.

20. A method comprising:
receiving a process stream comprising a mixture of one or more liquids and one or more solids; and
separating the one or more liquids from the one or more solids in the process stream with a first separation device to provide a separated liquids stream and a separated solids stream, the first separation device including a sedicanter centrifuge, a decanter centrifuge, a disk stack centrifuge, an air floatation device, a cyclone, or a settling tank;
wherein the separated solids stream has at least 38% protein; and
processing the separated liquids stream with a membrane-based separation device to provide a stream comprising a protein content of about 7% to about 27%.

21. The method of claim 20 , wherein the membrane-based separation device comprises an open channel membrane filter.

Assignees

• Icm Inc

Inventors

• Gallop Charles C
• Gerken Christopher Riley William

Classifications

• A23K10/10 Primary

  obtained by microbiological or biochemical processes (using chemicals or microorganisms for ensilaging of green fodder A23K30/15) · CPC title

• A23J1/005

  from vegetable waste materials · CPC title

• A23J1/12

  from cereals, wheat, bran, or molasses · CPC title

• A23J1/125

  by treatment involving enzymes or microorganisms (enzymatic hydrolysis of proteins A23J3/34) · CPC title

• A23J1/16

  from waste water of starch-manufacturing plant or like wastes · CPC title