System and method for detecting concentration of free SiO2 in coal dust

Patent metadata

Field	Value
Publication number	US-11940376-B2
Application number	US-202218147236-A
Country	US
Kind code	B2
Filing date	Dec 28, 2022
Priority date	Mar 29, 2022
Publication date	Mar 26, 2024
Grant date	Mar 26, 2024

Abstract

A system for detecting a concentration of free SiO 2 in coal dust includes a first sampling tube and a second sampling tube for sampling the coal dust, a three-way control valve communicated with the first sampling tube and the second sampling tube respectively, a photoacoustic spectrometry detection device communicated with the three-way control valve through a connecting pipeline, and a SiO 2 reaction tube for reacting SiO 2 in the coal dust; and the SiO 2 reaction tube is disposed on the second sampling tube. In the present disclosure, a coal dust sampling line is convenient to change by disposing the three-way control valve, and the first sampling tube and the second sampling tube are respectively communicated with the photoacoustic spectrometry detection device, so as to perform a differential accurate detection of the reacted CO content, and to obtain the SiO 2 content.

First claim

What is claimed is:

1. A system for detecting a concentration of free SiO 2 in coal dust, comprising a first sampling tube and a second sampling tube for sampling the coal dust, a three-way control valve communicated with the first sampling tube and the second sampling tube respectively, a photoacoustic spectrometry detection device communicated with the three-way control valve through a connecting pipeline, and a SiO 2 reaction tube for reacting SiO 2 in the coal dust; and the SiO 2 reaction tube is disposed on the second sampling tube;
wherein the SiO 2 reaction tube comprises a carbon tube and an air inlet heating tape from inside to outside, the carbon tube is heated through the air inlet heating tape, the SiO 2 in the coal dust delivered by the second sampling tube reacts with the heated carbon tube, and reacted gas is delivered into the photoacoustic spectrometry detection device through the three-way control valve;
the photoacoustic spectrometry detection device comprises a photoacoustic cavity communicated with the connecting pipeline, a laser device, a signal modulator, a reflector, quartz windows disposed at two ends of the photoacoustic cavity, a rheomicrophone disposed at a middle of the photoacoustic cavity, a lock-in amplifier for collecting and amplifying a photoaccoustic signal generated by the rheomicrophone and a detection software; and the laser device outputs laser through the signal modulator, and after the reflector reflects the laser, the laser enters the photoacoustic cavity through the quartz windows;
the photoacoustic spectrometry detection device further comprises a sampling pump for extracting gas and a flowmeter disposed on the sampling pump;
the system further comprises a tail gas treatment device, which comprises a tail gas conversion tube communicated with an air outlet of the sampling pump and a NaOH liquid bottle communicated with the tail gas conversion tube, and the NaOH liquid bottle is provided with an air outlet tube for discharging the processed tail gas.

2. The system for detecting the concentration of the free SiO 2 in the coal dust according to claim 1 , wherein a first insulation layer is disposed outside the air inlet heating tape, and the first insulation layer comprises an air inlet high temperature resistant quartz felt, an air inlet high temperature resistant quartz fiber and an air inlet high temperature resistant insulation cotton from inside to outside.

3. The system for detecting the concentration of the free SiO 2 in the coal dust according to claim 1 , wherein the tail gas conversion tube comprises an oxidized copper tube and an air outlet heating tape for heating the oxidized copper tube from inside to outside.

4. The system for detecting the concentration of the free SiO 2 in the coal dust according to claim 3 , wherein a second insulation layer is disposed outside the air outlet heating tape, and the second insulation layer comprises an air outlet high temperature resistant quartz felt, an air outlet high temperature resistant quartz fiber and an air outlet high temperature resistant insulation cotton from inside to outside.

5. The system for detecting the concentration of the free SiO 2 in the coal dust according to claim 1 , wherein temperature probes are respectively disposed on the SiO 2 reaction tube and the tail gas conversion tube.

Assignees

• Univ Anhui Sci & Technology

Inventors

• Jin Huawei
• Yan Fangzheng
• Fang Lei

Classifications

• G01N21/1702 Primary

  with opto-acoustic detection, e.g. for gases or analysing solids · CPC title

• G01N1/24

  Suction devices {(G01N1/22 - G01N1/2294 take precedence)} · CPC title

• G01N33/0027 Primary

  concerning the detector · CPC title

• G01N2021/1704

  in gases · CPC title

• G01N2201/06113

  Coherent sources; lasers · CPC title