Apparatus for mixing materials dissolved in a high-pressure working fluid

Patent metadata

Field	Value
Publication number	US-11931709-B2
Application number	US-201816760650-A
Country	US
Kind code	B2
Filing date	Oct 24, 2018
Priority date	Nov 7, 2017
Publication date	Mar 19, 2024
Grant date	Mar 19, 2024

Abstract

The present invention relates to a mixing apparatus. A production unit produces a working fluid that is in a supercritical state or a subcritical state. A storage unit stores a material. A dissolving unit dissolves the material in the working fluid. A mixer mixes the material together in the presence of the working fluid. A material feed valve opens or closes a flow passage through which the material is to pass to be fed from the storage unit into the dissolving unit. A working fluid inflow valve opens or closes a flow passage through which the working fluid is to pass to flow into the dissolving unit from the production unit. A mixer inflow valve opens or closes a flow passage through which the working fluid and the material are to pass to flow into the mixer from the dissolving unit.

First claim

The invention claimed is:

1. A mixing apparatus comprising:
a production unit configured to produce a working fluid that is in a supercritical state or a subcritical state;
a storage unit configured to store materials including a main material and an auxiliary material different from the main material;
a dissolving unit into which the working fluid and the materials are fed, the dissolving unit configured to dissolve the materials in the working fluid;
a mixer configured to mix the materials together in the presence of the working fluid;
material feed valves each configured to open or close a flow passage through which one of the materials is to pass to be fed from the storage unit into the dissolving unit;
a working fluid inflow valve configured to open or close a flow passage through which the working fluid is to pass to flow into the dissolving unit from the production unit;
a mixer inflow valve configured to open or close a flow passage through which the working fluid and the materials are to pass to flow into the mixer from the dissolving unit; and
a control unit for setting pressures in the production unit and the mixer such that the working fluid is kept in the supercritical or subcritical state, and for setting a pressure in the dissolving unit lower than the pressures in the production unit and the mixer.

2. The mixing apparatus according to claim 1 , comprising:
a branch flow passage that is a passage through which the working fluid produced in the production unit is to flow, that branches off the production unit on the upstream side of the working fluid inflow valve, and that merges into the mixer at a position on the downstream side of the mixer inflow valve and on the upstream side of the mixer; and
a branch flow passage opening/closing valve configured to open or close the branch flow passage.

3. The mixing apparatus according to claim 2 , configured to execute at least one of a step of reducing a pressure in the dissolving unit and a step of feeding the materials from the storage unit into the dissolving unit at the same time as a step of mixing the material together in the mixer.

4. The mixing apparatus according to claim 1 , configured to execute at least one of a step of reducing a pressure in the dissolving unit and a step of feeding the materials from the storage unit into the dissolving unit at the same time as a step of mixing the material together in the mixer.

5. The mixing apparatus according to claim 1 ,
wherein the dissolving unit is configured to repeatedly execute:
a step of feeding the material from the storage unit into the dissolving unit;
a step of dissolving the material in the working fluid;
a step of allowing the working fluid and the materials to flow into the mixer from the dissolving unit; and
a step of reducing a pressure in the dissolving unit.

6. The mixing apparatus according to claim 5 ,
wherein the dissolving unit comprises:
a dissolving unit entrance pressure gauge configured to detect a pressure at an entrance-side portion of the dissolving unit; and
a dissolving unit exit pressure gauge configured to detect a pressure at an exit-side portion of the dissolving unit.

7. The mixing apparatus according to claim 5 ,
wherein the mixer comprises:
a mixer entrance pressure gauge configured to detect a pressure at an entrance-side portion of the mixer; and
a mixer exit pressure gauge configured to detect a pressure at an exit-side portion of the mixer.

8. The mixing apparatus according to claim 5 ,
wherein the mixer comprises:
a mixer pressure gauge configured to detect a pressure inside the mixer; and
a mixer thermometer configured to detect a temperature inside the mixer.

9. The mixing apparatus according to claim 1 ,
wherein the dissolving unit comprises:
a dissolving unit entrance pressure gauge configured to detect a pressure at an entrance-side portion of the dissolving unit; and
a dissolving unit exit pressure gauge configured to detect a pressure at an exit-side portion of the dissolving unit.

10. The mixing apparatus according to claim 9 ,
wherein the mixer comprises:
a mixer entrance pressure gauge configured to detect a pressure at an entrance-side portion of the mixer; and
a mixer exit pressure gauge configured to detect a pressure at an exit-side portion of the mixer.

11. The mixing apparatus according to claim 9 ,
wherein the mixer comprises:
a mixer pressure gauge configured to detect a pressure inside the mixer; and
a mixer thermometer configured to detect a temperature inside the mixer.

12. The mixing apparatus according to claim 1 ,
wherein the mixer comprises:
a mixer entrance pressure gauge configured to detect a pressure at an entrance-side portion of the mixer; and
a mixer exit pressure gauge configured to detect a pressure at an exit-side portion of the mixer.

13. The mixing apparatus according to claim 12 ,
wherein the mixer comprises:
a mixer pressure gauge configured to detect a pressure inside the mixer; and
a mixer thermometer configured to detect a temperature inside the mixer.

14. The mixing apparatus according to claim 1 ,
wherein the mixer comprises:
a mixer pressure gauge configured to detect a pressure inside the mixer; and
a mixer thermometer configured to detect a temperature inside the mixer.

15. The mixing apparatus according to claim 14 , comprising:
a degree-of-opening adjustment valve configured to adjust a degree of opening of a flow passage through which the working fluid and the materials ejected from the mixer are to pass,
wherein the mixing apparatus is configured to adjust the degree of opening of the degree-of-opening adjustment valve according to detection results of the mixer pressure gauge and the mixer thermometer.

16. The mixing apparatus according to claim 15 ,
wherein the production unit comprises a pump configured to send out the working fluid, and
the mixing apparatus is configured to adjust a rotation speed of the pump according to detection results of the mixer pressure gauge and the mixer thermometer.

17. The mixing apparatus according to claim 14 ,
wherein the production unit comprises a pump configured to send out the working fluid, and
the mixing apparatus is configured to adjust a rotation speed of the pump according to detection results of the mixer pressure gauge and the mixer thermometer.

18. The mixing apparatus according to claim 1 , comprising:
a pressure adjustment valve configured to adjust a degree of opening of a flow passage through which the working fluid separated from the materials is to pass.

19. The mixing apparatus according to claim 1 ,
wherein at least one of the dissolving unit and the mixer has a portion that is inclined respect to a horizontal direction so that the materials go material goes down from an upstream side to a downstream side of the materials.

20. The mixing apparatus according to claim 1 , comprising:
a pressure reduction pump configured to reduce a pressure in the dissolving unit.

Assignees

• Kobe Steel Ltd

Inventors

• Higashi Kosuke
• Fukutani Kazuhisa

Classifications

• B01F35/71805 Primary

  using valves, gates, orifices or openings · CPC title

• B01F21/20

  using flow mixing · CPC title

• B01F23/09

  Mixing systems, i.e. flow charts or diagrams for components having more than two different of undetermined agglomeration states, e.g. supercritical states · CPC title

• B01F35/71

  Feed mechanisms (with proportioning B01F35/80) · CPC title

• B01F35/7547

  using valves, gates, orifices or openings · CPC title