Aerogel blanket and method for producing same

Patent metadata

Field	Value
Publication number	US-11926529-B2
Application number	US-202017414027-A
Country	US
Kind code	B2
Filing date	Aug 28, 2020
Priority date	Sep 18, 2019
Publication date	Mar 12, 2024
Grant date	Mar 12, 2024

Abstract

Provided is an aerogel blanket and a method for producing the same, wherein a catalyzed sol I sufficiently and uniformly impregnated into a blanket in an impregnation tank, and the catalyzed sol is allowed to stay in the impregnation tank for a specific time to control fluidity while achieving a viscosity at which the catalyzed sol can be easily introduced into the blanket, thereby forming a uniform aerogel in the blanket. As a result, the uniformity of pore structure and thermal insulation performance of an aerogel blanket are improved, the loss of raw materials is reduced through the impregnation process, the occurrence of process problems is reduced, and the generation of dust is reduced.

First claim

The invention claimed is:

1. A method for producing an aerogel blanket, the method comprising:
1) introducing a precursor solution and a catalyst solution comprising a base catalyst and a polar organic solvent into an impregnation tank to produce a catalyzed sol and allowing a catalyzed sol to stay in the impregnation tank to increase in viscosity;
2) passing a base material for a blanket through the impregnation tank to allow the catalyzed sol to penetrate into the base material for a blanket; and
3) subjecting the base material for a blanket into which the catalyzed sol has been penetrated to gelation on a conveyor belt of a device used for gel casting,
wherein a retention time of the catalyzed sol in the impregnation tank is 0.5 minutes to 40 minutes; and
the viscosity of the catalyzed sol when introduced into the base material is 1.2 to 6.0 times the viscosity of the catalyzed sol immediately after being produced.

2. The method of claim 1 , wherein the catalyzed sol is allowed to stay in the impregnation tank such that the viscosity of the catalyzed sol is 5.5 mPa·s to 100 mPa·s when introduced into the base material for a blanket.

3. The method of claim 1 , wherein the precursor solution and the catalyst solution are simultaneously introduced into the impregnation tank, or are mixed before being introduced into the impregnation tank and then introduced in the state of a catalyzed sol.

4. The method of claim 1 , wherein a temperature inside the impregnation tank is 1° C. to 30° C.

5. The method of claim 1 , wherein the catalyzed sol in the impregnation tank is stirred.

6. The method of claim 1 , wherein the catalyzed sol is a catalyzed silica sol.

7. The method of claim 1 , wherein the catalyzed sol is penetrated into the base material for a blanket using a roller.

Assignees

• Lg Chemical Ltd

Inventors

• Kim Young Hun
• Baek Se Won
• Yu Sung Min
• Min Kyung Seok
• Jeon Hyun Woo
• Park Sang Woo
• Kim Bong June

Classifications

• C01B33/1585 Primary

  Dehydration into aerogels · CPC title

• B01J13/0091

  Preparation of aerogels, e.g. xerogels · CPC title

• C04B30/02

  containing fibrous materials · CPC title

• D06M11/79

  with silicon dioxide, silicic acids or their salts · CPC title

• F16L59/028

  Compositions for or methods of fixing a thermally insulating material · CPC title