Superconductor comprising magnesium diboride and manufacturing method therefor

Patent metadata

Field	Value
Publication number	US-11903332-B2
Application number	US-201816962923-A
Country	US
Kind code	B2
Filing date	Feb 6, 2018
Priority date	Feb 6, 2018
Publication date	Feb 13, 2024
Grant date	Feb 13, 2024

Abstract

The present disclosure relates to a superconductor including magnesium diboride and a production method therefor. A superconductor having a high critical current density at a certain temperature and under a certain magnetic field may be obtained by doping magnesium diboride with liquid chloroform during the production of the superconductor.

First claim

The invention claimed is:

1. A superconductor comprising: carbon-doped magnesium diboride; and chlorine atoms present in grains of the carbon-doped magnesium diboride, wherein the superconductor comprises 0.05 at. % to 0.11 at. % of chlorine atoms.

2. The superconductor of claim 1 , wherein the carbon-doped magnesium diboride comprises more than 0 wt. % and 2 wt. % or less of carbon atoms.

3. A method for producing the superconductor according to claim 1 , the method comprising:
mixing boron powder with a liquid chlorinated hydrocarbon compound to form an amorphous carbon layer on the surface of the boron powder;
mixing magnesium powder with the boron powder having the amorphous carbon layer formed thereon to produce mixture;
press shaping the mixture; and
sintering a product resulting from the press shaping,
wherein the liquid chlorinated hydrocarbon compound is mixed with the boron powder in an amount of 0.03 mL to 0.4 mL per mg of the boron powder.

4. The method of claim 3 , wherein the liquid chlorinated hydrocarbon compound is chloroform or carbon tetrachloride.

5. The method of claim 3 , wherein the mixing of magnesium powder comprises mixing the magnesium powder with the boron powder having the amorphous carbon layer formed thereon at a stoichiometric ratio.

6. The method of claim 3 , wherein the amorphous carbon layer has a thickness of 1 nm to 10 nm.

7. The method of claim 3 , wherein the sintering is performed at a temperature of 600° C. to 1,000° C.

8. The method of claim 3 , wherein the sintering is performed for 10 minutes to 10 hours.

Assignees

• Korea Inst Mach & Materials

Inventors

• Chung Kook Chae
• Oh Young Seok
• Kang Seong Hoon
• Shinde Kiran Prakash
• Ranot Mahipal

Classifications

• H10N60/85 Primary

  Superconducting active materials · CPC title

• C01B7/01

  Chlorine; Hydrogen chloride · CPC title

• C01B35/04 Primary

  Metal borides · CPC title

• H10N60/0856

  of devices comprising metal borides, e.g. MgB2 · CPC title

• H10N60/20

  Permanent superconducting devices · CPC title