Fine bubble elimination method and fine bubble elimination device, and bubble size distribution measuring method and bubble size distribution measuring device

Patent metadata

Field	Value
Publication number	US-11898949-B2
Application number	US-201816769239-A
Country	US
Kind code	B2
Filing date	Nov 29, 2018
Priority date	Dec 4, 2017
Publication date	Feb 13, 2024
Grant date	Feb 13, 2024

Abstract

By irradiating target liquid L containing fine bubbles with ultrasonic waves from an ultrasonic irradiation device 102 , the fine bubbles in the target liquid L is reduced. By irradiating the target liquid L with ultrasonic waves, fine bubbles in the target liquid L can be reduced effectively. By using ultrasonic waves, bubbles with small diameters, particularly fine bubbles, can be effectively reduced, so that fine bubbles in the target liquid L can be efficiently reduced.

First claim

The invention claimed is:

1. A fine bubble elimination method comprising
a target liquid acquiring step of acquiring a target liquid containing ultrafine bubbles by restoring a lyophilized target object;
a container installing step of installing a container containing the target liquid at an installation position; and
an ultrasonic irradiation step of irradiating the target liquid containing the ultrafine bubbles having a bubble diameter of less than 1 μm with an ultrasonic wave from an ultrasonic irradiation device to reduce the ultrafine bubbles in the target liquid,
wherein the ultrasonic irradiation step irradiates the target liquid installed at the installation position with an ultrasonic wave having a frequency of 430 kHz or more, and
a lower part of the container installed at the installation position is always fixed at an antinode in a standing wave of the ultrasonic wave emitted from the ultrasonic irradiation device.

2. The fine bubble elimination method according to claim 1 , wherein
a gap is formed above the target liquid in the container.

3. The fine bubble elimination method according to claim 1 further comprising a standing step of allowing the target liquid to stand for a certain period of time after the ultrasonic irradiation step irradiates the target liquid with the ultrasonic wave.

4. The fine bubble elimination method according to claim 1 , wherein
an additive having high solubility is added to the target liquid.

5. The fine bubble elimination method according to claim 1 , wherein
the ultrasonic irradiation step irradiates the target liquid having a reduced surface tension due to inclusion of the ultrafine bubbles with the ultrasonic wave to reduce the ultrafine bubbles in the target liquid, so that a surface tension of the target liquid is increased.

6. The fine bubble elimination method according to claim 1 , wherein
the ultrasonic irradiation step adjusts a reduction amount of the ultrafine bubbles in the target liquid by adjusting at least one of a frequency, an irradiation time, and an irradiation intensity of the ultrasonic wave emitted from the ultrasonic irradiation device.

7. A bubble size distribution measuring method comprising a step of measuring bubble size distribution of ultrafine bubbles contained in a target liquid based on data on particle size distribution of the target liquid having the ultrafine bubbles reduced by the fine bubble elimination method according to claim 1 , and the data on the particle size distribution of the target liquid before the ultrafine bubbles are reduced.

8. A bubble size distribution measuring device configured to measure bubble size distribution of ultrafine bubbles contained in a target liquid based on data on particle size distribution of the target liquid having the ultrafine bubbles reduced by the fine bubble elimination method according to claim 1 , and the data on the particle size distribution of the target liquid before the ultrafine bubbles are reduced.

Assignees

• Shimadzu Corp
• National Institute Of Tech And Evaluation
• Fine Bubble Ind Association

Inventors

• Ohuchi Seika
• Tanaka Mitsuru
• Shimaoka Haruo

Classifications

• G01N15/0205 Primary

  by optical means · CPC title

• G01N2015/0011

  in liquids, e.g. bubbles · CPC title

• G01N2015/0283

  using control of suspension concentration · CPC title

• G01N15/0211 Primary

  Investigating a scatter or diffraction pattern · CPC title

• B01D19/00

  Degasification of liquids · CPC title