CLC facility comprising a solid/solid separator with means for distributing a gas-solid mixture

Patent metadata

Field	Value
Publication number	US-11885488-B2
Application number	US-201917261509-A
Country	US
Kind code	B2
Filing date	Jul 18, 2019
Priority date	Jul 23, 2018
Publication date	Jan 30, 2024
Grant date	Jan 30, 2024

Abstract

The invention relates to a CLC plant for the combustion of solid hydrocarbon feedstocks generating particles of unburnt residues, comprising a solid/solid separator above the combustion reactor in order to efficiently separate the particles of the oxygen-carrying solid from the particles of unburnt residues contained in the gas/solid mixture (14) exiting from the combustion reactor. The chamber (1) of the solid/solid separator, the combustion reactor and the inlet (2) for the gas/solid mixture (14) of the chamber have a parallelepiped shape. The inlet (2) is equipped at its top with means (3) for distribution of said gas/solid mixture in the chamber which extend over the entire length of the inlet, improving the solid/solid separation.

First claim

The invention claimed is:

1. A plant for chemical looping combustion of a solid hydrocarbon feedstock generating particles of unburnt residues and employing particles of an oxygen-carrying solid, the plant comprising:
a reduction reactor operating as fluidized bed in order to carry out the combustion of the solid hydrocarbon feedstock in contact with the particles of the oxygen-carrying solid, the reactor having a parallelepiped shape;
an oxidation reactor operating as fluidized bed in order to oxidize the reduced particles of the oxygen-carrying solid originating from the reduction reactor by bringing into contact with an oxidizing gas; and
a solid/solid separator surmounting the reduction reactor in order to separate the particles of the oxygen-carrying solid from particles of unburnt residues contained in a gas/solid mixture resulting from the reduction reactor, the solid/solid separator comprising:
a chamber of parallelepipedal shape comprising
a lower part operating as dense phase and an upper part operating as dilute phase;
at least one inlet of parallelepipedal shape for the gas/solid mixture originating from the reduction reactor, the at least one inlet emerging in the upper part of the chamber and being equipped at a top of the at least one inlet with means for distribution of the gas/solid mixture in the chamber which extend over the entire length of the at least one inlet;
at least one drain placed in the lower part of the chamber;
at least one outlet located in the upper part of the chamber.

2. The plant as claimed in claim 1 , additionally comprising a gas/solid separator fed by the at least one outlet of the chamber of the solid/solid separator, the gas/solid separator comprising a pipe for discharge of a gas depleted in light particles of unburnt residues, and a transportation pipe in communication with the reduction reactor in order to recycle a stream containing the particles of unburnt residues to the reduction reactor.

3. The plant as claimed in claim 1 , in which the chamber of the solid/solid separator and the at least one inlet have a rectangular parallelepipedal shape.

4. The plant as claimed in claim 1 , in which the reduction reactor has a rectangular parallelepipedal shape.

5. The plant as claimed in claim 1 , in which the at least one drain comprises two drains positioned at a bottom of the chamber on either side of the at least one inlet.

6. The plant as claimed in claim 1 , in which the at least one inlet is centered in the chamber.

7. The plant as claimed in claim 1 , in which the means for distribution of the gas/solid mixture in the chamber of the solid/solid separator comprise a beam of V-shaped section open toward the top of the chamber.

8. The plant as claimed in claim 7 , in which an opening angle α of the V-shaped section of the beam is between 10° and 150°.

9. The plant as claimed in claim 7 , in which the top of the beam is at a distance H from the top of the at least one inlet of between 0.5×L 2 and 5×L 2 , L 2 being a width of the internal space of the at least one inlet.

10. The plant as claimed in claim 7 , in which the top of the beam has a width L 1 of between 0.1×L 2 , L 2 being a width of the internal space of the at least one inlet.

11. The plant as claimed in claim 7 , in which the solid/solid separator additionally comprises means for cooling the at least one inlet and the beam.

12. The plant as claimed in claim 11 , in which the means for cooling are metal tubes for the passage of a heat-exchange fluid, the tubes being fixed to an external surface of the walls forming the at least one inlet and to an internal surface of the walls forming the beam.

13. The plant as claimed in claim 1 , in which the means for distribution of the gas/solid mixture in the chamber of the solid/solid separator comprise a curved plate with a concavity facing a bottom of the chamber, the curved plate being connected to two walls forming the at least one inlet and being provided with at least two slots positioned on either side of a central part of the curved plate for the passage of the gas/solid mixture and distribution of the gas/solid mixture toward a periphery of the chamber.

14. The plant as claimed in claim 13 , in which the solid/solid separator additionally comprises means for cooling the at least one inlet and the curved plate.

15. The plant as claimed in claim 1 , in which the means for distribution of the gas/solid mixture in the chamber of the solid/solid separator comprise a cylindrical beam.

16. The plant as claimed in claim 7 , in which an opening angle α of the V-shaped section of the beam is between 10° and 90°.

17. The plant as claimed in claim 7 , in which an opening angle α of the V-shaped section of the beam is between 10° and 40°.

18. The plant as claimed in claim 7 , in which the top of the beam is at a distance H from the top of the at least one inlet of between 0.5×L 2 and 3×L 2 , L 2 being a width of the internal space of the at least one inlet.

19. The plant as claimed in claim 7 , in which the top of the beam is at a distance H from the top of the at least one inlet of between 0.5×L 2 and 1×L 2 , L 2 being a width of the internal space of the at least one inlet.

20. The plant as claimed in claim 7 , in which the top of the beam has a width L1 of between 0.2×L2 and 1×L2, L2 being a width of the internal space of the at least one inlet.

Assignees

• Ifp Energies Now
• Total Raffinage Chimie

Inventors

• Bertholin Stephane
• Cloupet Ann
• Guillou Florent
• Tilland Airy
• Amblard Benjamin
• Tebianian Sina
• Yazdanpanah Mahdi

Classifications

• F23C10/18

  Details; Accessories · CPC title

• F23C10/10 Primary

  the separation apparatus being located outside the combustion chamber · CPC title

• F23C10/01 Primary

  in a fluidised bed of catalytic particles · CPC title

• F23C10/02

  with means specially adapted for achieving or promoting a circulating movement of particles within the bed or for a recirculation of particles entrained from the bed · CPC title

• F23C10/08

  characterised by the arrangement of separation apparatus, e.g. cyclones, for separating particles from the flue gases · CPC title