Systems and methods of forming and analyzing dissolvable articles

Patent metadata

Field	Value
Publication number	US-11884902-B2
Application number	US-202117527779-A
Country	US
Kind code	B2
Filing date	Nov 16, 2021
Priority date	May 16, 2018
Publication date	Jan 30, 2024
Grant date	Jan 30, 2024

Abstract

Systems and methods of forming and analyzing a dissolvable article are provided herein. In an embodiment, a method of analyzing a dissolvable article includes providing a dissolvable article comprising a water-soluble block copolymer and a fragrance, capturing a plurality of images of a surface of the dissolvable article using a three dimensional imaging device, wherein the plurality of images have different spatial properties and wherein the plurality of images are of a substantially similar viewing area of the three-dimensional imaging device, and determining a measurement of pore density and surface roughness of the surface of the dissolvable article.

First claim

What is claimed is:

1. A method of analyzing a dissolvable article, wherein the method comprises:
providing a dissolvable article comprising a water-soluble block copolymer and a fragrance;
capturing a plurality of images of a surface of the dissolvable article using a three dimensional imaging device,
wherein the plurality of images have different spatial properties and
wherein the plurality of images are of a substantially similar viewing area of the three-dimensional imaging device; and
determining a measurement of pore density and surface roughness of the surface of the dissolvable article.

2. The method of claim 1 , wherein the water-soluble block copolymer is solid at ambient conditions.

3. The method of claim 1 , wherein the dissolvable article is a solid at ambient conditions.

4. The method of claim 1 , wherein the dissolvable article has a flat surface and the step of capturing involves use the flat surface.

5. The method of claim 4 , wherein the flat surface has a surface area of at least 4 cm 2 .

6. The method of claim 1 , wherein the dissolvable article further comprises a glycol fatty acid ester.

7. The method of claim 1 , wherein the dissolvable article further comprises a filler.

8. The method of claim 1 , further comprising processing the plurality of images.

9. The method of claim 8 , wherein processing comprises processing at least one image using a contrast function to produce a data set representative of the surface roughness.

10. The method of claim 9 , wherein the step of processing comprises suppressing specular reflection from the surface of the dissolvable article.

11. The method of claim 10 , wherein suppressing specular reflection comprises one or more of polarization filtering or selective elimination of data from a data set that is attributable to specular reflection.

12. The method of claim 1 , further comprising producing a data set representative of roughness, pore volume, and optionally depression volume and elevation volume, with the images.

13. The method of claim 1 , further comprising determining elevation density, and depression density of the dissolvable article.

14. The method of claim 1 , further comprising determining dissolution of the dissolvable article.

15. The method of claim 14 , further comprising correlating pore density and surface roughness of the surface of the dissolvable article to dissolution.

16. The method of claim 15 , further comprising determining a threshold value of pore density and surface roughness that correlates to an acceptable dissolution performance of the dissolvable article.

17. A method of analyzing a solid dissolvable article, wherein the method comprises:
providing a solid dissolvable article comprising a water-soluble block copolymer;
capturing an image of a surface of the dissolvable article using a three dimensional imaging device;
processing the image using a contrast function;
producing a data set representative of at least one of roughness, pore volume, depression volume and elevation volume, with the processed image;
determining a measurement of at least one of pore density, surface roughness depression volume and elevation volume of the surface of the solid dissolvable article;
determining dissolution of the solid dissolvable article; and
correlating the determined measurement of at least one of pore density and surface roughness of the surface of the dissolvable article to the dissolution.

18. The method of claim 17 , further comprising determining a threshold value of pore density and surface roughness that correlates to an acceptable dissolution performance of the dissolvable article.

19. The method of claim 17 , wherein a plurality of images is captured.

20. The method of claim 19 , wherein capturing the plurality of images comprises capturing with a different illumination direction for each of the plurality of images with a constant viewing direction.

Assignees

• Henkel Ag & Co Kgaa

Inventors

• Piorkowski Daniel
• Dahlmeyer Jr Joseph D

Classifications

• C11D3/3707 Primary

  Polyethers, e.g. polyalkyleneoxides · CPC title

• C11D3/2093

  Esters; Carbonates · CPC title

• C11D3/50

  Perfumes · CPC title

• C11D3/505

  encapsulated or adsorbed on a carrier, e.g. zeolite or clay · CPC title

• G01N21/84

  Systems specially adapted for particular applications · CPC title