Bench-top time of flight mass spectrometer

Patent metadata

Field	Value
Publication number	US-11879470-B2
Application number	US-201917057357-A
Country	US
Kind code	B2
Filing date	May 31, 2019
Priority date	May 31, 2018
Publication date	Jan 23, 2024
Grant date	Jan 23, 2024

Abstract

A mass spectrometer comprising: a vacuum housing comprising a first vacuum chamber having a first gas exhaust port; a gas pump ( 1700 ) having a first gas inlet port connected to the first gas exhaust port (H 1 ) by a first gas conduit for evacuating the first vacuum chamber; and a first apertured cover ( 2010 ) arranged over the first gas exhaust port (H 1 ) or first gas inlet port, or in the first gas conduit therebetween.

First claim

The invention claimed is:

1. A mass spectrometer comprising:
a vacuum housing comprising a first vacuum chamber having a first gas exhaust port;
a gas pump having a first gas inlet port connected to the first gas exhaust port by a first gas conduit for evacuating the first vacuum chamber; and
a first apertured cover arranged over the first gas exhaust port or first gas inlet port, or in the first gas conduit therebetween;
wherein the first apertured cover is electrically conductive so as to prevent electric fields passing therethrough and entering the first gas inlet port and/or first gas exhaust port, through the first gas conduit; and
wherein the first apertured cover comprises a main body portion having apertures through which said gas passes and a plurality of protrusions extending away from the main body portion to respective free ends that are arranged in contact with a housing of the gas pump and/or the vacuum housing.

2. The spectrometer of claim 1 , wherein the vacuum housing and/or pump housing is electrically grounded, thereby grounding the first apertured cover via the protrusions.

3. The spectrometer of claim 1 , wherein the protrusions are elongated fingers extending away from the main body portion.

4. The spectrometer of claim 1 , wherein the main body is substantially planar and extends in a first plane, and the protrusions are substantially planar and extend in one or more other plane angled relative to the plane of the main body.

5. The spectrometer of claim 1 , wherein the protrusions are flexible relative to the main body and/or relative to each other.

6. The spectrometer of claim 1 , wherein the first apertured cover is arranged substantially horizontally.

7. The spectrometer of claim 1 , wherein the gas pump is mounted to the vacuum housing and wherein the first apertured cover is provided at the interface between the gas pump and the vacuum housing.

8. The spectrometer of claim 7 , wherein the gas pump is removably mounted to the vacuum housing.

9. The spectrometer of claim 1 , wherein the first gas inlet port in the gas pump is arranged coaxially with the first gas exhaust port in the first vacuum chamber.

10. The spectrometer of claim 1 , wherein the vacuum housing comprises a second vacuum chamber having a second gas exhaust port;
wherein the gas pump has a second gas inlet port connected to the second gas exhaust port by a second gas conduit for evacuating the second vacuum chamber; and
a second apertured cover arranged over the second gas exhaust port or second gas inlet port, or in the second gas conduit therebetween.

11. The spectrometer of claim 10 , wherein the first and second vacuum chambers are adjacent one another and separated by a differential pumping aperture.

12. The spectrometer of claim 10 , wherein the gas pump housing has a first side, and the first and second gas inlet ports are provided in the first side.

13. The spectrometer of claim 1 , wherein the vacuum housing comprises a further vacuum chamber having a further gas exhaust port;
wherein the gas pump has a further gas inlet port connected to the further gas exhaust port by a further gas conduit for evacuating the further vacuum chamber; and
a further apertured cover arranged over the further gas exhaust port or further gas inlet port, or in the further gas conduit therebetween.

14. The spectrometer of claim 13 , wherein the gas pump housing has a first side in which the first gas inlet port is provided and a second side in which said further gas inlet port is provided.

15. The spectrometer of claim 13 , comprising a Time of Flight mass analyser in said further vacuum port.

16. A method of mass spectrometry comprising:
providing the spectrometer of claim 1 ;
operating the gas pump so as to draw gas from said first vacuum chamber, through said first gas exhaust port, through said first gas conduit, and into said first gas inlet port, wherein the gas passes through said first apertured cover.

Assignees

• Micromass Ltd

Inventors

• Marsh Cedric
• Carney Peter
• Wildgoose Jason Lee
• Wallis David
• Mciver Paul
• Chummar Soji
• Antoniades George Andreas
• Mistry Dipesh

Classifications

• F04D19/042 Primary

  Turbomolecular vacuum pumps · CPC title

• F04D29/122

  especially adapted for elastic fluid pumps · CPC title

• F04D29/701

  especially adapted for elastic fluid pumps · CPC title

• H01J49/24 Primary

  Vacuum systems, e.g. maintaining desired pressures · CPC title

• H01J49/405

  characterised by the reflectron, e.g. curved field, electrode shapes · CPC title