Methods for forming peroxyformic acid and uses thereof
US-9845290-B2 · Dec 19, 2017 · US
US11873273B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11873273-B2 |
| Application number | US-201916981666-A |
| Country | US |
| Kind code | B2 |
| Filing date | Mar 28, 2019 |
| Priority date | Mar 29, 2018 |
| Publication date | Jan 16, 2024 |
| Grant date | Jan 16, 2024 |
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A method of producing an organic peroxide includes introducing an organic solution and a peroxide solution into a mixing tank to form a mixture. The method further includes circulating the mixture over a fixed catalyst bed to form the organic peroxide and measuring a concentration of the organic peroxide in the mixture. Further, the method includes removing at least a portion of the mixture when the concentration reaches a set value.
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What is claimed is: 1. A method of producing an organic peroxide comprising: introducing an organic solution and a peroxide solution into a mixing tank to form a mixture; circulating the mixture over a fixed catalyst bed to form the organic peroxide; measuring a concentration of the organic peroxide in the mixture; and removing at least a portion of the mixture when the concentration reaches a set value. 2. The method according to claim 1 , wherein the peroxide solution comprises hydrogen peroxide and water. 3. The method according to claim 2 , wherein the peroxide solution comprises 10 to 50 wt % of hydrogen peroxide based on a total weight of the peroxide solution. 4. The method according to claim 1 , wherein the organic solution comprises water and an organic acid having 1 to 8 carbon atoms. 5. The method according to claim 4 , wherein the organic solution comprises 10 to 50 wt % of the organic acid based on a total weight of the organic solution. 6. The method according to claim 4 , wherein the organic acid is acetic acid. 7. The method according to claim 5 , wherein the organic acid is acetic acid. 8. The method according to claim 1 , wherein the fixed catalyst bed comprises an acid resin. 9. The method according to claim 1 , wherein the set value is between 50 and 2000 ppm of the organic peroxide.
Preparation of peroxy compounds · CPC title
Feed or outlet control devices · CPC title
Controlling catalytic processes (B01J8/1809 takes precedence) · CPC title
Feeding reactive fluids (for solid material B01J8/0015) · CPC title
the outlet side being of particular interest · CPC title
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