Honeycomb body manufacturing methods

Patent metadata

Field	Value
Publication number	US-11866375-B2
Application number	US-201917058507-A
Country	US
Kind code	B2
Filing date	May 30, 2019
Priority date	May 31, 2018
Publication date	Jan 9, 2024
Grant date	Jan 9, 2024

Abstract

Methods of firing ceramic-forming honeycomb bodies are disclosed that include heating the honeycomb bodies and blocking furnace gases from flowing through the honeycomb body by placing a layer selected from the group consisting of a graphite layer, a graphite-containing layer, an activated carbon layer, or an amorphous carbon layer adjacent an endface of the honeycomb body. Heating removes organic pore-forming material and graphite pore-forming material in the honeycomb body. The layer oxidizes to form a porous layer after firing to a first temperature, and furnace gases flow through the honeycomb body.

First claim

What is claimed is:

1. A method of firing a honeycomb body, the method comprising:
setting a ceramic-forming honeycomb body comprising pore-forming materials comprising organic pore-forming material and graphite pore-forming material on a cookie in a furnace containing gases comprising oxygen;
placing a layer selected from the group consisting of a graphite layer, a graphite-containing layer, an activated carbon layer, or an amorphous carbon layer between the cookie and the honeycomb body; and
heating the honeycomb body to a temperature that burns out and removes at least a portion of the organic pore-forming material and the graphite pore-forming material,
wherein the layer is configured to block gases from flowing through the honeycomb body when the honeycomb is heated to the temperature that burns out and removes the portion of the organic pore-forming material.

2. The method of claim 1 wherein heating the honeycomb body comprises heating the furnace to a temperature of up to 600° C. to remove at least a portion of the organic pore-forming material and heating the furnace to a temperature greater than 600° C. to remove the graphite pore-forming material.

3. The method of claim 2 wherein the layer blocks gases in the furnace from flowing through the honeycomb body.

4. The method of claim 2 wherein the layer is oxidized after removal of at least a portion of the organic pore-forming material.

5. The method of claim 4 wherein the layer that has been oxidized does not block furnace gases from flowing through the honeycomb body.

6. The method of claim 1 wherein the layer comprises a graphite sheet.

7. The method of claim 1 wherein the layer comprises a sheet.

8. The method of claim 1 wherein the cookie is placed on a flow-through setter.

9. The method of claim 8 wherein the flow-through setter comprises a ring-shaped setter.

10. The method of claim 9 wherein a second cookie is placed on the honeycomb body.

11. The method of claim 10 wherein a second layer selected from the group consisting of a graphite layer, a graphite-containing layer, an activated carbon layer, or an amorphous carbon layer is placed between the honeycomb body and the second cookie.

12. A method of firing a honeycomb body, the method comprising:
heating a ceramic-forming honeycomb body comprising a first endface and a second endface and organic pore-forming material and graphite pore-forming material in a furnace containing gases comprising oxygen; and
blocking the gases from flowing through the honeycomb body by placing a layer selected from the group consisting of a graphite layer, a graphite-containing layer, an activated carbon layer or an amorphous carbon layer adjacent the first endface or the second endface.

13. The method of claim 12 further comprising heating the furnace to a first temperature sufficient to burn out and remove the organic pore-forming material and heating the furnace to a second temperature that burns out and removes the graphite pore-forming material.

14. The method of claim 13 wherein during heating the honeycomb body to the second temperature burning out the graphite pore-forming material, furnace gases flow through the layer and the honeycomb body.

15. The method of claim 14 wherein the first temperature is less than or equal to 600° C. and the second temperature is greater than 600° C.

16. The method of claim 14 wherein the honeycomb body is placed upon the layer disposed upon a cookie.

17. The method of claim 16 wherein the cookie is place upon a setter.

18. The method of claim 17 wherein the setter comprises a flow-through setter.

19. The method of claim 18 wherein the flow-through setter comprises a ring-shaped setter.

20. The method of claim 18 wherein a second cookie is placed upon the honeycomb body.

Assignees

• Corning Inc

Inventors

• Chapman Thomas Richard
• Tepesch Patrick David
• Wing Douglas Richard

Classifications

• C04B35/64 Primary

  Burning or sintering processes (C04B33/32 takes precedence {; powder metallurgy B22F}) · CPC title

• B28B11/243

  Setting, e.g. drying, dehydrating or firing ceramic articles (B28B11/242 takes precedence) · CPC title

• B28B11/248

  Supports for drying · CPC title

• C04B38/0006

  Honeycomb structures (from one or more corrugated sheets by winding or stacking C04B38/0083) · CPC title

• C04B38/068

  Carbonaceous materials, e.g. coal, carbon, graphite, hydrocarbons · CPC title