System and method for polymerization
US-9382348-B2 · Jul 5, 2016 · US
US11845047B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11845047-B2 |
| Application number | US-201815980025-A |
| Country | US |
| Kind code | B2 |
| Filing date | May 15, 2018 |
| Priority date | May 15, 2018 |
| Publication date | Dec 19, 2023 |
| Grant date | Dec 19, 2023 |
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Systems and methods for improved mixing, including baffle systems, reactor systems, and methods of using the same are provided herein. These baffle systems include a ring having an exterior surface defining an outer diameter and an outer circumference, an interior surface defining an inner diameter and an inner circumference, a top surface, a bottom surface, and an axis; and one or more substantially vertical baffles extending from the interior surface of the ring toward the axis.
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What is claimed is: 1. A baffle system for improved mixing in a cylindrical reactor, the cylindrical reactor defining a reactor axis extending along a height of the cylindrical reactor, the baffle system comprising: a cylindrical ring having an exterior surface defining an outer diameter and an outer circumference, an interior surface defining an inner diameter and an inner circumference, a top surface, a bottom surface opposite and parallel to the top surface, and an axis extending through an axial center alignable with the reactor axis; and one or more substantially vertical baffles extending from the interior surface of the ring toward the axis, wherein the ring is a compression ring which is discontinuous along both the outer circumference and the inner circumference thereby defining two opposing and non-overlying edges and a gap therebetween, wherein the ring defines a height extending between the top surface and the bottom surface in a direction along the axis, wherein the ring defines a width extending between the outer diameter and the inner diameter in a direction transverse to the axis, wherein the height of the ring is greater than the width of the ring, wherein the one or more substantially vertical baffles has a length of from about 0.1 times to about 10 times the outer diameter of the ring, wherein the one or more substantially vertical baffles has a length which extends vertically above the top surface of the cylindrical ring, vertically below the bottom surface of the cylindrical ring, or both, and wherein the one or more substantially vertical baffles are planar. 2. The baffle system of claim 1 , wherein the one or more substantially vertical baffles comprise: a first planar surface and a second planar surface, each of which is substantially perpendicular to the interior surface of the ring and extend in an axial direction; and at least one lateral surface connecting the first planar surface and the second planar surface. 3. The baffle system of claim 2 , wherein the first planar surface and the second planar surface are polygonal in shape. 4. The baffle system of claim 1 , wherein the top surface of the ring is configured to support a mixing motor housing. 5. The baffle system of claim 1 , wherein the ring further comprises one or more openings extending from the exterior surface of the ring to the interior surface of the ring and located along the outer circumference of the ring to correspond to one or more feed inlet ports, outlet ports, or measuring device ports of the reactor. 6. The baffle system of claim 1 , wherein the ring further comprises one or more projections extending outwardly from the exterior surface of the ring, each projection comprising an aperture extending through the projection to the interior surface of the ring, and located along the outer circumference of the ring to correspond to and extend into one or more feed inlet ports, outlet ports, or measuring device ports of the reactor. 7. The baffle system of claim 1 , comprising at least two vertical baffles. 8. The baffle system of claim 1 , comprising at least four vertical baffles. 9. The baffle system of claim 1 , wherein the ring is further configured to be attached to the cylindrical reactor in one or more of: a bearing housing, or a motor seal block. 10. A reactor system comprising: the cylindrical reactor having an inner surface and an outer surface and defining the reactor axis; and the baffle system of claim 1 installed inside the reactor, such that the exterior surface of the ring is in contact with the inner surface of the reactor, wherein the cylindrical reactor is a high pressure LDPE reactor. 11. The reactor system of claim 10 , wherein the reactor is a tubular reactor. 12. The reactor system of claim 10 , further comprising: a motor comprising an axial shaft extending vertically through the center and along the axis of the ring and comprising at least two vanes extending from the axial shaft; a feed inlet port; an outlet port; and a measuring device port. 13. The reactor system of claim 12 , wherein the at least two vanes are located vertically along the axial shaft such that at least a portion of the vanes is between the top surface and the bottom surface of the ring. 14. The reactor system of claim 12 , wherein the ring further comprises one or more openings extending from the exterior surface of the ring to the interior surface of the ring and located along the outer circumference of the ring to correspond to the feed inlet port, the outlet port, or the measuring device port. 15. The reactor system of claim 12 , wherein the ring further comprises one or more projections extending outwardly from the exterior surface of the ring, each projection comprising an aperture extending through the projection to the interior surface of the ring, and located along the outer circumference of the ring to correspond to and extend into one or more feed inlet ports, outlet ports, or measuring device ports of the reactor. 16. The reactor system of claim 10 , wherein the ring is further attached to the cylindrical reactor in one or more of: a bearing housing, or a motor seal block. 17. A method of improving mixing in a gas phase, a liquid phase, a supercritical, or a slurry process, the method comprising: installing a baffle system inside a substantially cylindrical reactor having an outer surface and an inner surface and defining a reactor axis extending along a height of the cylindrical reactor, wherein the baffle system comprises: (a) a cylindrical ring having an exterior surface defining an outer diameter and an outer circumference, an interior surface defining an inner diameter and an inner circumference, a top surface, a bottom surface, and an axis extending through an axial center aligned with the reactor axis, wherein the ring is a compression ring which is discontinuous along both the outer circumference and the inner circumference thereby defining two opposing and non-overlying edges and a gap therebetween, and (b) one or more substantially vertical baffles extending from the interior surface of the ring toward the axis, wherein the ring defines a height extending between the top surface and the bottom surface in a direction along the axis, wherein the ring defines a width extending between the outer diameter and the inner diameter in a direction transverse to the axis, wherein the one or more substantially vertical baffles has a length of from about 0.1 times to about 10 times the outer diameter of the ring, wherein the one or more substantially vertical baffles has a length which extends vertically above the top surface of the cylindrical ring, vertically below the bottom surface of the cylindrical ring, or both, wherein the one or more substantially vertical baffles are planar, and wherein the height of the ring is greater than the width of the ring, and wherein, when installed, the exterior surface of the ring is in contact with the inner surface of the reactor; and under gas phase, liquid phase, supercritical phase, or slurry process conditions, stirring the contents of the cylindrical reactor. 18. The method of claim 17 , wherein the one or more substantially vertical baffles comprise: a first planar surface and a second planar surface, each of which is substantially perpendicular to the interior surface of the ring; and at least one lateral surface connecting the first planar surface and the second planar surface. 19. The method of claim 18 , wherein the first planar surface and
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