Gypsum-based investment material composition for casting, and method for manufacturing gypsum-based investment material composition for casting

Patent metadata

Field	Value
Publication number	US-11844660-B2
Application number	US-201816652865-A
Country	US
Kind code	B2
Filing date	Oct 1, 2018
Priority date	Oct 5, 2017
Publication date	Dec 19, 2023
Grant date	Dec 19, 2023

Abstract

The present invention provides a gypsum-based embedding material composition for casting useful for forming a rapid-heating type gypsum-based embedding material and a method for producing the same. The gypsum-based embedding material is formed of the gypsum-based powdery embedding material composition by adding a malaxation liquid into the composition and heating the mixture in a high-temperature furnace. The gypsum-based embedding material composition contains as main components, at least one co-pulverized material selected from a co-pulverized material of calcined gypsum and quartz, that of calcined gypsum and cristobalite, and that of calcined gypsum, quartz, and cristobalite. The composition further contains a powdery moisture-retaining component or a liquid moisture-retaining component having a low water content, and has an average particle diameter of 30 μm or less.

First claim

The invention claimed is:

1. A gypsum-based embedding material composition for casting, the gypsum-based embedding material composition for casting comprising, as main components:
calcined gypsum in an amount from 25 to 50 parts by mass;
quartz in an amount from 40 to 65 parts by mass; and
cristobalite in an amount from 10 to 35 parts by mass, relative to a total amount of the main components as 100 parts by mass, and

the composition further comprising:
a moisture-retaining component in an amount from 0.2 to 1.0 part by mass relative to the total amount of the main components as 100 parts by mass, the moisture-retaining component comprising a powdery moisture-retaining component or a liquid moisture-retaining component and having a water content in a range of 1.5 or less,
wherein the composition comprises at least one co-pulverized material selected from the group consisting of a co-pulverized material of calcined gypsum and quartz, a co-pulverized material of calcined gypsum and cristobalite, and a co-pulverized material of calcined gypsum, quartz, and cristobalite,
the composition has an average particle diameter in a range of 30 μm or less, and
the composition is configured to form a gypsum-based embedding material with a leaving time in a range from 8 to 15 minutes when the gypsum-based embedding material is formed by adding a malaxation liquid to the composition so as to form a mixture of the composition and the malaxation liquid, setting the mixture, and heating the resulting set product of the mixture, wherein the leaving time is a time from the adding of the malaxation liquid to starting of the heating of the set product of the mixture.

2. The gypsum-based embedding material composition for casting according to claim 1 ,
wherein the moisture-retaining component comprises at least one polyhydric alcohol.

3. The gypsum-based embedding material composition for casting according to claim 2 ,
wherein the at least one polyhydric alcohol is at least one material selected from the group consisting of glycerin, propylene glycol, ethylene glycol, 1,3-butylene glycol, polymers thereof, and copolymers thereof.

4. The gypsum-based embedding material composition for casting according to claim 3 ,
wherein the glycerin is glycerin having a purity in a range of 98.5% or more.

5. The gypsum-based embedding material composition for casting according to claim 1 , wherein the leaving time is in a range from 8 to 10 minutes.

6. The gypsum-based embedding material composition for casting according to claim 1 , wherein the leaving time is 8 minutes.

7. The gypsum-based embedding material composition for casting according to claim 1 , wherein the gypsum-based embedding material is a dental article.

8. The gypsum-based embedding material composition for casting according to claim 1 , further comprising gypsum dihydrate.

9. The gypsum-based embedding material composition for casting according to claim 8 ,
wherein the gypsum dihydrate is contained in the at least one co-pulverized material.

10. The gypsum-based embedding material composition for casting according to claim 1 ,
wherein the composition has a coefficient of setting expansion at two hours after the adding of the malaxation liquid in a range from 0.2% to 3.0%.

11. The gypsum-based embedding material composition for casting according to claim 1 ,
wherein the composition has a total coefficient of expansion in a range from 1.3% to 3.0%.

12. The gypsum-based embedding material composition for casting according to claim 1 ,
wherein the composition has the average particle diameter in a range from 15 μm to 30 μm.

13. A method for producing a gypsum-based embedding material composition for casting, the method comprising:
mixing at least one co-pulverized material and a moisture-retaining component,
wherein the at least one co-pulverized material is selected from the group consisting of a co-pulverized material of calcined gypsum and quartz, a co-pulverized material of calcined gypsum and cristobalite, and a co-pulverized material of calcined gypsum, quartz, and cristobalite,
the composition comprises, as main components: calcined gypsum in an amount from 25 to 50 parts by mass, quartz in an amount from 40 to 65 parts by mass, and cristobalite in an amount from 10 to 35 parts by mass, relative to a total amount of the main components as 100 parts by mass,
the composition further comprises the moisture-retaining component in an amount from 0.2 to 1.0 part by mass relative to the total amount of the main components as 100 parts by mass,
the moisture-retaining component is a powdery moisture-retaining component or a liquid moisture-retaining component, and has a water content in a range of 1.5% or less,
if quartz or cristobalite is absent from the at least one co-pulverized material, the absent quartz or the absent cristobalite is pulverized separately and added to the at least one co-pulverized material, so that the gypsum-based embedding material composition in a powder form having an average particle diameter in a range of 30 μm or less is prepared, and
the composition is configured to form a gypsum-based embedding material with a leaving time in a range from 8 to 15 minutes when the gypsum-based embedding material is formed by adding a malaxation liquid to the composition so as to form a mixture of the composition and the malaxation liquid, setting the mixture, and heating the resulting set product of the mixture, wherein the leaving time is a time from the adding of the malaxation liquid to starting of the heating of the set product of the mixture.

14. The method for producing a gypsum-based embedding material composition for casting according to claim 13 , wherein in the mixing, gypsum dihydrate is further present.

15. The method for producing a gypsum-based embedding material composition for casting according to claim 13 ,
wherein each of the co-pulverized materials in the at least one co-pulverized material comprises gypsum dehydrate and is co-pulverized with the gypsum dehydrate.

16. A gypsum-based embedding material formed of the gypsum-based embedding material composition according to claim 1
wherein the gypsum-based embedding material is the heated product comprising the mixture of the composition and the malaxation liquid.

17. A method for producing a gypsum-based embedding material, the method comprising:
adding malaxation liquid into the gypsum-based embedding material composition according to claim 1 ;
forming the mixture of the composition and the malaxation liquid;
setting the mixture; and
heating the resulting set product in a furnace,
wherein the gypsum-based embedding material is formed with the leaving time in the range from 8 to 15 minutes.

Assignees

• Yoshino Gypsum Co

Inventors

• Horiuchi Tatsuya
• Sugano Kenichi

Classifications

• A61C13/20 Primary

  Methods or devices for soldering, casting, moulding or melting {(A61C13/04, A61C13/081 take precedence)} · CPC title

• B22C1/08 Primary

  for decreasing shrinkage of the mould, e.g. for investment casting · CPC title

• B22C1/18

  of inorganic agents {(B22C1/162 takes precedence)} · CPC title

• B22C7/02

  Lost patterns · CPC title

• C04B14/06

  Quartz; Sand · CPC title